采用动态力学分析(dynamic mechanical analysis)方法研究了纳米羟基磷灰石(nano-hydroxyapatite, n-HA)增强聚酰胺66(polyamide 66, PA66)生物复合材料的动态力学性能.结果表明,复合材料中纳米羟基磷灰石组分的含量、生理盐水和振动频率对n-HA/PA66复合材料的动态力学性能和玻璃化转变过程都有一定程度的影响.随着纳米羟基磷灰石含量的增加,其复合材料的力学损耗峰温度移向高温区,峰值降低;复合材料吸水后其储能模量和损耗模量都有所降低,且玻璃化温度向低温区移动;振动频率对复合材料的动态力学性能也有一定的影响, 随着振动频率的增加,复合材料的储能模量也有所提高.
参考文献
[1] | Xian Mo D;Jian Yuan H;Chang Sheng W .[J].Biomaterials,2001,22:2867-2873. |
[2] | Sang-Soo K;Min-Sun P;Oju J et al.[J].Biomaterials,2006,27:1399-1409. |
[3] | Bonfield W;Grynpas M D;Tully A E et al.[J].BIOMATERIALS,1981,2:185-186. |
[4] | Wang Xuejiang;Li Yubao;Wei Jie .[J].Biomaterials,2002,23:4787. |
[5] | Wei Jie;Li Yubao;Chen Weiqun et al.[J].Journal of Materials Science,2003,38:3303. |
[6] | Wei Jie;Li Yubao .[J].European Polymer Journal,2004,40:509. |
[7] | Joshi M;Maiti S N;Misra A .[J].Polymer,1994,35:17. |
[8] | George S;Neelakantan N R;Varghese K T et al.[J].J Poly Sci Part B Polymer Physics,1997,35:2309. |
[9] | Pothan L A;Oommen Z;Thomas S .[J].Composites Science and Technology,2003,63:283. |
[10] | Diéz-Gutiérrez S;Rodríguez-Pérez M A;De Saja J A et al.[J].Polymer,1999,40:5345. |
[11] | Lakes R S;Katz J L;Sternstein S S .[J].Journal of Biomechanics,1979,12:657. |
[12] | Lakes R S;Katz J L .[J].Journal of Biomechanics,1979,12:679. |
[13] | Garner E B;Lakes R S;Lee L et al.[J].Journal of Biomechanical Engineering,2000,122:166. |
[14] | Buechner,PM;Lakes,RS;Swan,C;Brand,RA .A broadband viscoelastic spectroscopic study of bovine bone: implications for fluid flow.[J].Annals of Biomedical Engineering,2001(8):719-728. |
[15] | Richardson M O W.Polymer Engineering Composite[M].London:Applied Science Publishers,1977 |
[16] | Nielsen L E.Mechanical Properties of Polymers and Composites[M].New York:marcel Dekker,inc,1974 |
[17] | 张翔;李玉宝;吕国玉 等.[J].功能材料,2006,36(06):896-899. |
[18] | 赵彦生,刘永梅,卢建军,叶峻岭,王克智.纳米CaCO3改性β成核聚丙烯的研究[J].中国塑料,2006(05):25-28. |
[19] | Zhang X;Li Y B;L G Y et al.[J].Polymer Stability and Stability,2006,91(05):1202-1207. |
[20] | Murayama T.Dynamic Mechanical Analysis of Polymeric Materials[M].Amsterdam:elsevier,1978 |
[21] | 杨建 .[J].中国塑料,1989,3(04):80-95. |
[22] | Men Yongfeng;Reiger J .[J].European Polymer Journal,2004,40:2629. |
[23] | Loo LS.;Gleason KK.;Cohen RE. .Correlation times of motion of deuterium oxide in polyamide 6 rods[J].Macromolecules,1998(25):8907-8911. |
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