欢迎登录材料期刊网

材料期刊网

高级检索

采用场发射电镜观察了FGH97合金经过不同时效温度和时效时间后不同形态γ′相的演化规律。结果表明:不同温度下一次γ′相和二次γ′相平均尺寸随时效时间的增加存在最大值,三次γ′相平均尺寸随时效时间延长呈线性增长;550℃时效后二次γ′相由立方形长大为不规则形,分裂成为田字花瓣形或蝶形,而后沿〈100〉方向分解为小立方形;在750℃时效后期,二次γ′相出现边界融合现象,且小三次γ′相消失。时效后硬度值的变化与γ′相尺寸有关。

The γ′ phase evolution in FGH97 P/M alloy after aging at different temperatures for different time was observed by FESEM. The results show that the sizes of primary γ′ phase and seeondary γ′ phase exist maximum values with increasing aging time at different temperatures. The average sizes of tertiary γ′ phase increases linearly with increasing aging time. The euboidal seeondary γ′ phase grows irregularly and changes to the shape of four-leaf clover or butterfly, then breaks up into small cube along 〈 100 〉 at 550 ℃. But the boundary of second γ′ phase becomes merged and the tertiary γ′ phase becomes vanished at 750 ℃. The hardness relates to the size of precipitated phase.

参考文献

[1] 席文君,邢洁,张义文.FGH95粉末冶金高温合金长期时效的组织稳定性[J].稀有金属材料与工程,2011(08):1397-1401.
[2] 李红宇,宋西平,王艳丽,陈国良.FGH95合金中γ'相稳定性研究[J].稀有金属材料与工程,2009(01):64-67.
[3] John Radavich,Tadeu Carneiro,David Furrer,Joseph Lemsky,Anthony Banik.Effect of Processing and Composition on the Structure and Properties of P/M EP741NP Type Alloys[J].中国航空学报(英文版),2007(02):97-106.
[4] 张莹,张义文,张娜,贾建.FGH97粉末冶金高温合金热处理工艺和组织性能的研究[J].航空材料学报,2008(06):5-9.
[5] 陈大钦,郑子樵,李世晨,刘祖耀,李剑,周明,陈志国.共格沉淀析出过程的模拟Ⅰ--微观结构演化[J].中国有色金属学报,2005(12):1945-1952.
[6] 吕俊英;杨洪才;王志兴 等.一种高温合金的γ'相析出初期长大动力学[J].东北大学学报,1994,15(02):184-188.
[7] 李玉清;刘锦岩.高温合金晶界间隙相[M].北京:冶金工业出版社,1990
[8] Qiu YY. .The splitting behavior of gamma ' particles in Ni-based alloys[J].Journal of Alloys and Compounds: An Interdisciplinary Journal of Materials Science and Solid-state Chemistry and Physics,1998(1/2):145-153.
[9] 宋西平,李红宇,盖靖峰,陈国良.U720LI合金高温析出γ′相的失稳分解[J].金属学报,2005(11):1233-1236.
上一张 下一张
上一张 下一张
计量
  • 下载量()
  • 访问量()
文章评分
  • 您的评分:
  • 1
    0%
  • 2
    0%
  • 3
    0%
  • 4
    0%
  • 5
    0%