欢迎登录材料期刊网

材料期刊网

高级检索

为了进一步探讨Q235A钢电沉积镍层残余应力、力学性能与镀覆工艺参数的关系,以瓦特镀镍液为基础,采用直流电沉积法,在Q235A钢表面电镀镍.采用X射线衍射仪、纳米力学测试系统、表面轮廓测量仪测试了镍镀层的残余应力、显微硬度、弹性模量及表面粗糙度;探讨了电流密度、温度、pH值对镍镀层力学性能的影响规律,以正交试验法优选了最佳工艺.结果表明:电流密度3.0 A/dm2,温度45℃,pH值3.5时,镍镀层的性能最佳,晶粒粒径为34.8 nm,镀层显微硬度达到3.86 GPa,弹性模量达到238 GPa,表面粗糙度为0.182 μm.

参考文献

[1] Nasirpouri F;Sanaeian M R;Samardak A S .An investigation on the effect of surface morphology and crystalline texture on corrosion behavior,structural and magnetic properties of electrodeposited nanocrystalline nickel rims[J].Applied Surface Science,2014,292:795-805.
[2] S. E. Hadian;D. R. Gabe .Residual stresses in electrodeposits of nickel and nickel-iron alloys[J].Surface & Coatings Technology,1999(2/3):118-135.
[3] 周楠,丁毅,马立群.Q235钢表面电镀镍及其性能的研究[J].电镀与环保,2013(01):4-6.
[4] 蒋艳平,赵冠湘,潘勇,周益春.用纳米压痕法测量电沉积镍镀层的力学性能[J].湘潭大学自然科学学报,2005(03):50-58.
[5] Chen JS.;Duh JG. .Indentation behavior and Young's modulus evaluation in electroless Ni modified CrN coating on mild steel[J].Surface & Coatings Technology,2001(1):6-13.
[6] 朱立群.功能膜层的电沉积理论与技术[M].北京:北京航空航天大学出版社,2005:24-28.
[7] 许姣姣 .电沉积制备纳米晶镍及其电化学研究[D].昆明:昆明理工大学,2007.
[8] 吕镖,胡振峰,汪笑鹤,徐滨士.电流密度对镍镀层结构和性能的影响[J].中国表面工程,2013(04):66-71.
[9] Milstein F.;Chantasiriwan S. .Theoretical study of the response of 12 cubic metals to uniaxial loading[J].Physical Review.B.Condensed Matter,1998(10):6006-6018.
[10] Mohammadreza Baghbanan;Uwe Erb;Gino Palumbo .Towards the application of nanocrystalline metals in MEMS[J].Physica Status Solidi, A. Applied Research,2006(6):1259-1264.
[11] Oliver W C;Pharr G M .An improved technique for determining hardness and elastic modulus using load and displacement sensing indentation experiments[J].Journal of Materials Researoh,1992,7(06):1564-1583.
[12] S.-H.Kim;J.-Y.Kim;J.Yu;t.Y.Lee .Residual Stress and Interfacial Reaction of the Electroplated Ni-Cu Alloy Under Bump Metallurgy in the Flip-Chip Solder Joint[J].Journal of Electronic Materials,2004(9):948-957.
[13] Bolshakov A;Oliver W C;Pharr G M .Infuences of stress on the measurement of mechanical properties using nanoindentation:Part Ⅱ.Finite element simulations[J].Journal of Materials Research,1996,11(03):760-768.
上一张 下一张
上一张 下一张
计量
  • 下载量()
  • 访问量()
文章评分
  • 您的评分:
  • 1
    0%
  • 2
    0%
  • 3
    0%
  • 4
    0%
  • 5
    0%