欢迎登录材料期刊网

材料期刊网

高级检索

采用CaCO3和CaHPO·2HO的混合物为前驱物,通过水热合成得到晶粒完整、分散性好、端面粒度在100nm以下的HA粉体,并借助XRD和SEM分析讨论了前驱物配比、水热温度、反应时间与物相组成、粒度变化和晶体形貌的关系.

Hydroxyapatite(HA) was synthesized by using CaCO3 and CaHPO4·2H2O as raw materials under hydrothermal condition. The relation between ratio of raw materials, hydrothermal temperature, reaction time and the resultant phases, changes of granularity, crystal appearance were studied by using SEM and XRD. This HA synthesized has a good crystal appearance, good dispersity, its end plane granularity is less than 100 nm.

参考文献

[1] Gricial R, Doremus R H. J. Mat. Sci.:Mat. in Medicine, 1992, 3: 154--156.
[2] Gottfredsen K, et al. J. Biomed Mater. Res., 1995, 29: 1223--1231.
[3] Daculsi G, et al. J. Biomed Mater. Res., 1990, 24: 379--396.
[4] 张德正, 王保峰, 纪元玉, 等. 中国陶瓷, 1998, 34(6): 24--26.
[5] 邬鸿彦, 朱明刚, 孔令宜, 等. 河北轻化工学院学报, 1998, 19(1): 36--38.
[6] 施尔畏, 夏长泰,王步国, 等(SHI Er-Wei, et al). 无机材?料学报(Journal of Inorganic Materials),1996, 11(2): 193--206.
[7] Laudise R A. In: Dryburgh P M ed. Advanced Crystal Growth.New York, London, Sydney,Tokyo: Prentice Hall,1987. 267.
[8] Pham M, Reuther H. Journal of Materials Science-materials in Medicine, 2000, 11: 383--391.
[9] Toyama T, Oshima A. Journal of the Ceramic Society of Japan, 2001, 109: 232--237.
上一张 下一张
上一张 下一张
计量
  • 下载量()
  • 访问量()
文章评分
  • 您的评分:
  • 1
    0%
  • 2
    0%
  • 3
    0%
  • 4
    0%
  • 5
    0%