硅酸盐通报 , 2011, 30(2): 312-315.
汝官瓷、钧官瓷和刘家门窑青瓷的多元统计分析
肖朋飞 1, , 赵红梅 2, , 李融武 3, , 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"},"keywords":[{"id":"8624d21b-a96e-41e7-adc6-a38cba2250bd","keyword":"残铝量","originalKeyword":"残铝量"},{"id":"ccb12170-14a8-4d6c-b23a-cf48e5e985cd","keyword":"晶粒度","originalKeyword":"晶粒度"},{"id":"21ad2b5e-06fd-430a-a822-440ae2cd22df","keyword":"钢","originalKeyword":"钢"}],"language":"zh","publisherId":"bqclkxygc200205005","title":"残铝对35CrNiMoV钢晶粒度的影响","volume":"25","year":"2002"},{"abstractinfo":"建立了西洋参中人参皂苷Rg1、Re及Rb1同时分离测定的胶束电动毛细管色谱新方法,以解决西洋参样品中难溶于水的3种人参皂苷的准确定量问题.以40.2 cm(有效长度30 cm)×50 μm的熔融石英毛细管柱为分离柱,分离缓冲液的组成为V(15 mmol/L Na2B4O7 + 30 mmol/L H3BO3(pH 9.0)+100 mmol/L十二烷基硫酸钠(SDS)+30 g/L聚乙二醇35 000)∶V(甲醇)∶V(异丙醇)=2∶1∶1,于214 nm下检测.详细研究了影响分离的因素.Rg1、Re及Rb1检出限(信噪比(S/N)为3)分别为30、40及30 mg/L,定量限(S/N=9)分别为90、120及90mg/L,加标回收率为87.4%～95.2%.用该法测定了西洋参标准物质,并与高效液相色谱法的检测结果进行了比对,结果吻合.应用该方法分别测定了中国、加拿大及美国的西洋参,获得满意的结果.","authors":[{"authorName":"李佳","id":"4ec745f0-cde6-451d-bba1-e948550d46ef","originalAuthorName":"李佳"},{"authorName":"丁晓静","id":"b38ae2d7-0976-4335-996a-42b6e4bd04cf","originalAuthorName":"丁晓静"},{"authorName":"李芸","id":"65f3c490-5910-47de-97ad-826af5d7153c","originalAuthorName":"李芸"},{"authorName":"杨媛媛","id":"d55148e0-604e-442b-801f-f9882cbdd892","originalAuthorName":"杨媛媛"},{"authorName":"刘军","id":"69dbd4b4-ebea-454d-a73d-18b1a3f0d438","originalAuthorName":"刘军"},{"authorName":"王志","id":"5f2cc096-b792-4c51-bf99-53c1ba5e2857","originalAuthorName":"王志"}],"doi":"10.3724/SP.J.1123.2011.00259","fpage":"259","id":"4078194e-b3bc-4dbf-86de-1c90f7d6446e","issue":"3","journal":{"abbrevTitle":"SP","coverImgSrc":"journal/img/cover/SP.jpg","id":"58","issnPpub":"1000-8713","publisherId":"SP","title":"色谱 "},"keywords":[{"id":"2ad0b20e-385c-454d-b88b-7b9d7b38907f","keyword":"胶柬电动毛细管色谱","originalKeyword":"胶柬电动毛细管色谱"},{"id":"915c18c5-1280-4941-b6ef-d4c1aff2a363","keyword":"高效液相色谱","originalKeyword":"高效液相色谱"},{"id":"1da1654e-4aba-4f19-ad57-7cea19474830","keyword":"人参皂苷","originalKeyword":"人参皂苷"},{"id":"0260f00d-9624-4da9-ac53-aa63abd89b9b","keyword":"西洋参","originalKeyword":"西洋参"}],"language":"zh","publisherId":"sp201103014","title":"胶束电动毛细管色谱法同时测定西洋参中人参皂苷Rg1、Re和Rb1","volume":"29","year":"2011"},{"abstractinfo":"采用滴涂和电聚合法制备了聚L-半胱氨酸/乙炔黑修饰玻碳电极(L-Cys/AB/GCE).用电化学交流阻抗法和计时库仑法研究了该修饰电极表面的界面性质.此外,还通过循环伏安法(CV)研究了对苯二酚(HQ)在该修饰电极上的电化学行为.阻抗图谱说明L-Cys/ AB/GCE修饰膜的存在能够增加电子转移速度;计时库仑分析表明,L-Cys/AB/GCE的比表面积是裸电极的6倍;CV行为表明,L-Cys/AB/GCE对HQ氧化还原具有良好的电催化作用,响应的峰电流为裸电极的4倍,提高了检测HQ的灵敏度且峰电流与电位扫描速度的平方根呈良好的线性关系,相关系数R2为0.995～0.998,说明HQ在L-Cys/ AB/GCE上的电化学反应过程是受扩散速度控制的过程.在支持电解质为0.1 mol/L磷酸盐缓冲溶液(pH 7.0)的优化条件下,用差分脉冲伏安法(DPV)分析,HQ浓度在0.5～1 000 μmol/L范围内,氧化峰的峰电流(Ipa)与浓度(c)呈良好的线性关系,相关系数R2为0.998,方法检出限为0.08 μ mol/L,由此建立了一种测定水样中HQ的方法.按照实验方法对环境水样中HQ进行测定,结果与高效液相色谱法基本一致,相对标准偏差(RSD,n=8)为2.3％～2.6％.","authors":[{"authorName":"许春萱","id":"b188a6d3-e475-4029-a1be-dbbd5a527b5c","originalAuthorName":"许春萱"},{"authorName":"丁婷婷","id":"4233101e-4a11-4a29-8816-9665f6a7aaed","originalAuthorName":"丁婷婷"},{"authorName":"杨媛媛","id":"4b85e69c-ff83-4990-b1a8-a04eedbaa603","originalAuthorName":"杨媛媛"},{"authorName":"钟翔","id":"2a3cc5c3-095d-4a82-a290-c23e4aaac69f","originalAuthorName":"钟翔"},{"authorName":"卢先春","id":"eeae4ae4-564d-4269-afa8-b88ef0935075","originalAuthorName":"卢先春"}],"doi":"10.13228/j.boyuan.issn1000-7571.009836","fpage":"19","id":"8f791c15-09d2-473a-9d27-73f376334b37","issue":"9","journal":{"abbrevTitle":"YJFX","coverImgSrc":"journal/img/cover/YJFX.jpg","id":"71","issnPpub":"1000-7571","publisherId":"YJFX","title":"冶金分析 "},"keywords":[{"id":"475b2cb9-a486-4664-881d-01e56c3c36b2","keyword":"L-半胱氨酸","originalKeyword":"L-半胱氨酸"},{"id":"e427f864-0e1e-4b07-b279-fb4eda5f9721","keyword":"乙炔黑","originalKeyword":"乙炔黑"},{"id":"86a03af9-84fe-4f4a-9b10-d92a6820b07b","keyword":"对苯二酚","originalKeyword":"对苯二酚"},{"id":"5925e681-8318-4eb3-a7a5-f0ef1688a84d","keyword":"传感器","originalKeyword":"传感器"},{"id":"5c39e238-30b0-49a9-b09a-4a8d818c7406","keyword":"玻碳电极","originalKeyword":"玻碳电极"}],"language":"zh","publisherId":"yjfx201609003","title":"聚L-半胱氨酸/乙炔黑修饰玻碳电极测定水样中对苯二酚","volume":"36","year":"2016"},{"abstractinfo":"采用基于密度泛函理论和Hartree-Fork的第一性原理方法,计算了CdS、CdSe、CdTe、HgTe等Ⅱ-Ⅵ族化合物中原子间的两体及三体相互作用势,分析了基组及计算方法的选择对计算结果的影响.采用Lennard-Jones、Born-Mayer和Morse势函数对两体相互作用势进行拟合,得到相应的拟合参数及误差值,结果表明普遍应用于共价分子的Morse势也同样适用于Ⅱ-Ⅵ族原子二聚体.考虑到多体相互作用势必须考虑角度因素,采用Stilling-Weber势函数对三体势进行了拟合研究,结果亦较为理想.","authors":[{"authorName":"杨媛媛","id":"3bc22a80-092b-415f-8ccd-7c4d2605e214","originalAuthorName":"杨媛媛"},{"authorName":"王新强","id":"a5180c4e-b57c-4131-9335-b7498c4fa8e7","originalAuthorName":"王新强"},{"authorName":"何阿玲","id":"0539fcbb-e186-476e-a896-813b8c3a9d25","originalAuthorName":"何阿玲"}],"doi":"","fpage":"1234","id":"8e7041b8-bd06-4115-bc7d-595403370d26","issue":"8","journal":{"abbrevTitle":"GNCL","coverImgSrc":"journal/img/cover/GNCL.jpg","id":"33","issnPpub":"1001-9731","publisherId":"GNCL","title":"功能材料"},"keywords":[{"id":"278e7d1b-62cb-4ecb-ac4e-8d21fce7520c","keyword":"Ⅱ-Ⅵ族化合物","originalKeyword":"Ⅱ-Ⅵ族化合物"},{"id":"9b694459-adfb-4d72-9000-c7ba3ec307d3","keyword":"原子间作用势","originalKeyword":"原子间作用势"},{"id":"0571dbff-7f74-49aa-b434-4688fb31ac21","keyword":"第一性原理","originalKeyword":"第一性原理"},{"id":"42502243-5e37-4187-a149-53191a8a21ca","keyword":"势能拟合","originalKeyword":"势能拟合"}],"language":"zh","publisherId":"gncl200708005","title":"Ⅱ-Ⅵ族化合物中原子间两体及三体相互作用势的理论研究","volume":"38","year":"2007"},{"abstractinfo":"采用Woods-Saxon形成的密度函数，按照杨立铭方法以及稍微修改的方法进行估算都得出，紧接126的幻数应该接近于184．","authors":[{"authorName":"李先卉","id":"de0a8216-5ace-4a39-a9c2-dc0e4635868d","originalAuthorName":"李先卉"},{"authorName":"周治宁","id":"fb0bee5a-b978-479d-a348-7cfeb81683ff","originalAuthorName":"周治宁"},{"authorName":"钟毓澍","id":"7e1c646a-9dd6-4099-a1dd-48a38d24785c","originalAuthorName":"钟毓澍"},{"authorName":"杨泽森","id":"dac8f638-c051-480c-899f-55daa616b078","originalAuthorName":"杨泽森"}],"doi":"10.3969/j.issn.1007-4627.2000.01.009","fpage":"39","id":"24ab9145-669e-473f-940c-46aafa41541e","issue":"1","journal":{"abbrevTitle":"YZHWLPL","coverImgSrc":"journal/img/cover/YZHWLPL.jpg","id":"78","issnPpub":"1007-4627","publisherId":"YZHWLPL","title":"原子核物理评论 "},"keywords":[{"id":"a56c609f-1561-4216-adb0-fc937f323b42","keyword":"超重核幻数","originalKeyword":"超重核幻数"},{"id":"bc154b1b-0f42-4d6f-9e65-64cf1cf70b5f","keyword":"杨立铭方法","originalKeyword":"杨立铭方法"},{"id":"913e281b-2cf2-4469-99de-7758f327a0c2","keyword":"Thomas-Fermi近似","originalKeyword":"Thomas-Fermi近似"}],"language":"zh","publisherId":"yzhwlpl200001009","title":"用杨立铭方法估算大于126的幻数","volume":"17","year":"2000"},{"abstractinfo":"杨坪金矿床赋存于下古生界丹凤群大草坝组变火山—沉积建造中,金矿化严格受层间挤压破碎(片理化)带控制,赋矿岩性为蚀变的二云石英片岩、绢云母石英片岩、绿泥石英片岩等变质岩及黄铁矿化石英脉,金矿化受变质、构造及次生氧化三重作用控制.对杨坪金矿床的地质特征及控矿特征进行了系统的研究,总结了找矿标志,并指出了找矿方向.","authors":[{"authorName":"张银斗","id":"8764fff0-6afd-4f47-8cbb-a0bc3aebc5e3","originalAuthorName":"张银斗"}],"doi":"","fpage":"24","id":"7c98a968-7112-4917-9271-e00b77970427","issue":"1","journal":{"abbrevTitle":"HJ","coverImgSrc":"journal/img/cover/HJ.jpg","id":"44","issnPpub":"1001-1277","publisherId":"HJ","title":"黄金"},"keywords":[{"id":"5034aee0-cb40-4bd0-b883-2eb1d15eac4b","keyword":"地质特征","originalKeyword":"地质特征"},{"id":"5f6b6235-c284-4a52-a713-e0bb3ac50aa3","keyword":"控矿特征","originalKeyword":"控矿特征"},{"id":"1e4733d3-52c3-4c63-9072-ff2e17cf002e","keyword":"找矿标志","originalKeyword":"找矿标志"},{"id":"f0b2ed2b-45f9-4bad-aba9-8b696a60102b","keyword":"找矿方向","originalKeyword":"找矿方向"},{"id":"abe0bc7e-b8e2-4095-a867-8c7cbb45a24f","keyword":"杨坪金矿床","originalKeyword":"杨坪金矿床"}],"language":"zh","publisherId":"huangj201301006","title":"甘肃杨坪金矿床控矿特征及找矿方向","volume":"","year":"2013"},{"abstractinfo":"杨砦峪金矿床为河南灵宝小秦岭地区一重要大型石英脉型金矿床,矿床空间产出受太华群变质地层、岩浆岩及断裂构造控制,层间断裂为主要容矿构造.矿脉内矿体产出表现出\"尖灭再现\"、\"尖灭侧现\"规律.综合研究表明,小秦岭地区金矿床深部具有存在第二矿化富集段的可能性,在杨砦峪矿区,矿脉东段深部仍存在较好的成矿远景和找矿潜力.","authors":[{"authorName":"张庆超","id":"bab17d0e-bafb-4b0d-a46c-af63e0f92041","originalAuthorName":"张庆超"}],"doi":"10.3969/j.issn.1001-1277.2004.10.006","fpage":"19","id":"a5e01dd1-9aa0-45a0-bbfc-dc367c2a13db","issue":"10","journal":{"abbrevTitle":"HJ","coverImgSrc":"journal/img/cover/HJ.jpg","id":"44","issnPpub":"1001-1277","publisherId":"HJ","title":"黄金"},"keywords":[{"id":"96b81f72-8929-4e32-a794-35b0f3908133","keyword":"杨砦峪金矿床","originalKeyword":"杨砦峪金矿床"},{"id":"6027da23-6ddc-4696-b051-89c13227848a","keyword":"石英脉型","originalKeyword":"石英脉型"},{"id":"0cb416f8-b21f-4ff8-b599-e31978de5af7","keyword":"地质特征","originalKeyword":"地质特征"},{"id":"1379a96f-cb9d-492f-9621-dd980419d399","keyword":"深部成矿远景","originalKeyword":"深部成矿远景"}],"language":"zh","publisherId":"huangj200410006","title":"杨砦峪金矿床地质特征及深部成矿远景评价","volume":"25","year":"2004"},{"abstractinfo":"本文研究了应用稀土保水剂对干旱地区新疆杨育苗的效应,结果表明:应用稀土保水剂能极大地提高苗木成活率,加速苗木的生长发育,根系数量、株高、地茎等生长量指标均明显高于对照.因此,应用稀土保水剂对育苗的成功率、培育壮苗都有一定的作用.","authors":[{"authorName":"王永刚","id":"38361a45-f110-4aeb-a580-2436cf6c6956","originalAuthorName":"王永刚"},{"authorName":"张宇生","id":"083931f0-09cd-4490-8ade-f310257d5949","originalAuthorName":"张宇生"},{"authorName":"张宏江","id":"22614210-1ed9-46b4-94f5-e83cfbf53d69","originalAuthorName":"张宏江"}],"doi":"10.3969/j.issn.1004-0277.2000.05.011","fpage":"38","id":"f2fb53ae-860a-4080-930b-25c1c781692f","issue":"5","journal":{"abbrevTitle":"XT","coverImgSrc":"journal/img/cover/XT.jpg","id":"65","issnPpub":"1004-0277","publisherId":"XT","title":"稀土"},"keywords":[{"id":"d6121fd6-2f0c-4b38-8415-0809dff7b660","keyword":"稀土保水剂","originalKeyword":"稀土保水剂"},{"id":"dbb6825d-5ea8-42fb-a3b7-faaa66286cd7","keyword":"育苗","originalKeyword":"育苗"},{"id":"5354a5b7-84ad-4b44-90af-4de66e718826","keyword":"成活率","originalKeyword":"成活率"},{"id":"9145b6d2-c58c-44ca-9db8-3924c802ab04","keyword":"生长量","originalKeyword":"生长量"}],"language":"zh","publisherId":"xitu200005011","title":"稀土保水剂在新疆杨育苗上的应用研究","volume":"21","year":"2000"}],"totalpage":4,"totalrecord":33}