欢迎登录材料期刊网

材料期刊网

高级检索

采用反应热压烧结法制备了TaC/Ti3SiC2复合材料,借助XRD、SEM、能谱仪以及热重分析等,研究了TaC含量对TaC/Ti3SiC2复合材料的相组成、显微结构、力学性能和抗氧化性的影响.结果表明:采用反应热压烧结法可以制备出致密的TaC/Ti3SiC2复合材料,该复合材料的主晶相为Ti3SiC2和TaTiC2,还含有少量的TiC;随着TaC含量的增加,TaC/Ti3SiC2复合材料的弯曲强度和断裂韧性呈现先增大后降低的变化趋势,当TaC含量为30wt%时,二者均达到最大值,此时弯曲强度为404 MPa,断裂韧性为4.10 MPa·m1/2;TaC的引入,使TaC/Ti3SiC2复合材料抗氧化性能明显优于Ti3SiC2材料.

参考文献

[1] Ngai T L;Kuang Y H;Li Y Y.Impurity control in pressureless reactive synthesis of Ti3SiC2 pure bulk from elemental powders[J].Ceramics International,201238(01):463-469.
[2] Radoivc M;Barsoum M W;Ganguly A.On the elastic properties and mechanical damping of Ti3SiC2,Ti3GeC2,Ti3Si0.5Al0.5C2 and Ti2AlC in the 300-1573 K[J].Acta Materialia,200654(10):2757-2767.
[3] Zhang Z F;Sun Z M;Hashimoto H.Deformation and fracture behavior of ternary compound Ti3SiC2 at 25-1300 ℃[J].Materials Letters,200357(07):1295-1299.
[4] Li S B;Xie J X;Zhao J Q.Mechanical properties and mechanism of damage tolerance for Ti3SiC2[J].Materials Letters,200257(01):119-123.
[5] Zhang J F;Wu T;Wang L J.Microstructure and properties of Ti3SiC2/SiC nanocomposites fabricated by spark plasma sintering[J].Composites Science and Technology,200868(02):499-505.
[6] 尹洪峰;任 耘;范 强.反应热压烧结法制备SiC/Ti3SiC2复合材料及其性能[J].复合材料学报,201128(03):69-73.
[7] Wu B T;Sun Z M;Hashimoto H.Microstructural evolution and mechanical properties of Ti3SiC2-TiC composites[J].Journal of Alloys and Compounds,2010502(01):49-53.
[8] Zhu J F;Ye L;He L H.Effect of Al2O3 on the microstructure and mechanical properties of Ti3SiC2/Al2O3 in situ composites synthesized by reactive hot pressing[J].Ceramics International,201238(07):5475-5479.
[9] 陈盼军;尹洪峰;潘丽青.热压制备Ti3SiC2/MgAl2O4 复合材料及其性能研究[J].兵器材料科学与工程,201134(05):53-56.
[10] Wang Y;Xu Y D;Wang Y G.Effects of TaC addition on the ablation resistance of C/SiC[J].Materials Letters,201064(19):2068-2071.
[11] Chen Z K;Xiong X;Li G D.Ablation behaviors of carbon/carbon composites with C-SiC-TaC multi-interlayers[J].Applied Surface Science,2009255(22):9217-9219.
上一张 下一张
上一张 下一张
计量
  • 下载量()
  • 访问量()
文章评分
  • 您的评分:
  • 1
    0%
  • 2
    0%
  • 3
    0%
  • 4
    0%
  • 5
    0%