以Na3VO4 ·12H2O,AgNO3和Y(NO3)3·6H2O为原料,采用浸渍法制备了Y2O3/Ag3VO4复合可见光催化剂,并用XRD,SEM,XPS,UV-Vis等测试手段表征了试样的结构和性能.结果显示,Y2O3/Ag3VO4复合可见光催化剂为单斜结构,Y以Y2O3的形式分散在Ag3VO4晶体的表面.UV-Vis测试结果表明,Y2O3/Ag3VO4较纯Ag3VO4吸收带边发生了红移,在可见光区的吸收增强;以金属卤灯(波长大于400 nm)为光源,研究了Y2O3/Ag3VO4催化剂对甲基橙(MO)的可见光催化降解性能.结果发现,Y2O3/Ag3VO4复合可见光催化剂的光催化活性较纯Ag3VO4均有大幅提高,其中Y掺杂量为4%时活性最高.
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