欢迎登录材料期刊网

材料期刊网

高级检索

采用Gleeble?3500热力模拟试验机在变形温度300~450℃、应变速率0.001~1 s?1条件下进行单轴压缩试验,研究ZX115(Mg-1.0%Zn-1.5%Ca(质量分数))合金热压缩过程中的组织演变及再结晶形核机制。结果表明:ZX115合金在热压缩过程中发生了明显的动态再结晶,再结晶晶粒尺寸随着变形温度的升高或应变速率的降低而增大。合金在不同变形条件下的动态再结晶机制有所差异,主要有孪生动态再结晶、不连续动态再结晶和第二相粒子促进动态再结晶等方式。

The microstructure evolution and dynamic recrystallization (DRX) of ZX115 (Mg-1.0%Zn-1.5%Ca (mass fraction)) magnesium alloy during hot compression were studied. The uniaxial compression was conducted on a Gleeble-3500 simulator at different deformation temperatures (300?450℃) and strain rates (0.001?1 s?1). The results show that the DRX can be found in compressed ZX115 alloy during hot compressing. With the increase of the deformation temperatures or the decreases of the strain rates, the recrystallized grain size increases. Under different deformation conditions, the nucleation mechanism of dynamic recrystallization including twin induced nucleation, discontinuous nucleation, the second phase particle stimulated nucleation of DRX, and so on, can be found.

参考文献

[1] 丁文江.镁合金科学与技术[M].北京:科学出版社, 2007. DING Wen-jiang. Science and technology of magnesium alloys[M]. Beijing:Science Press, 2007.,2007.
[2] 余琨,黎文献,王日初,马正青.变形镁合金的研究、开发及应用[J].中国有色金属学报,2003(02):277-288.
[3] 曾荣昌,柯伟,徐永波,韩恩厚,朱自勇.Mg合金的最新发展及应用前景[J].金属学报,2001(07):673-685.
[4] PÉREZ-PRADO M T, DEL VALLE J A, CONTRERAS J M, RUANO O A. Microstructural evolution during large strain hot rolling of an AM60 Mg alloy[J]. Scripta Materialia, 2004, 50(5):661-665.,2004.
[5] 汪凌云,黄光胜,范永革,黄光杰.变形AZ31镁合金的晶粒细化[J].中国有色金属学报,2003(03):594-598.
[6] 刘楚明,刘子娟,朱秀荣,周海涛.镁及镁合金动态再结晶研究进展[J].中国有色金属学报,2006(01):1-12.
[7] 付雪松,陈国清,王中奇,周文龙.AZ31镁合金热轧变形的动态再结晶机制[J].稀有金属材料与工程,2011(08):1473-1477.
[8] 任政,张兴国,邱月,隋里,张涛,金俊泽.电磁场和钙微合金化对变形镁合金AZ61组织和力学性能的影响[J].中国有色金属学报,2010(02):182-188.
[9] HRADILOVÁ M, VOJTĚCH D, KUBÁSEK J, ČAPEK J, VLACH M. Structural and mechanical characteristics of Mg-4Zn and Mg-4Zn-0.4 Ca alloys after different thermal and mechanical processing routes[J]. Materials Science and Engineering A, 2013, 586:284-291.,2013.
[10] OH-ISHI K, WATANABE R, MENDIS C L, HONO K. Age-hardening response of Mg-0.3 at.% Ca alloys with different Zn contents[J]. Materials Science and Engineering A, 2009, 526(1):177-184.,2009.
[11] BETTLES C J, GIBSON M A, VENKATESAN K. Enhanced age-hardening behaviour in Mg-4wt.%Zn micro-alloyed with Ca[J]. Scripta Materialia, 2004, 51(3):193-197.,2004.
[12] ZHANG B P, WANG Y, GENG L, LU C X. Effect of calcium on texture and mechanical properties of hot-extruded Mg-Zn-Ca alloys[J]. Material Science and Engineering A, 2012, 539:56-60.,2012.
[13] OH J C, OHKUBO T, MUKAI T, HONO K. TEM and 3DAP characterization of an age-hardened Mg-Ca-Zn alloy[J]. Scripta Materialia, 2005, 53(6):675-679.,2005.
[14] LEVI G, AVRAHAM S, ZILBEROV A, BAMBERGER M. Solidification, solution treatment and age hardening of a Mg-1.6 wt.% Ca-3.2 wt.% Zn alloy[J]. Acta Materialia, 2006, 54(2):523-530.,2006.
[15] LARIONOVA T V, PARK W W, YOU B S. A ternary phase observed in rapidly solidified Mg-Ca-Zn alloys[J]. Scripta Materialia, 2001, 45(1):7-12.,2001.
[16] ISHIKAWA K, WATANABE H, MUKAI T. High temperature compressive properties over a wide range of strain rates in an AZ31 magnesium alloy[J]. Journal of Materials Science, 2005, 40(7):1577-1582.,2005.
[17] GALIYEV A, KAIBYSHEV R, GOTTESTEIN G. Correlation of plastic deformation and dynamic recrystallization in magnesium alloy ZK60[J]. Acta Materialia, 2001, 49(7):1199-1207.,2001.
[18] AL-SAMMAN T, GOTTSTEIN G. Dynamic recrystallization during high temperature deformation of magnesium[J]. Material Science and Engineering A, 2008, 490:411-420.,2008.
[19] 刘庆.镁合金塑性变形机理研究进展[J].金属学报,2010(11):1458-1472.
[20] KAIBYSHEV R O, SITDIKOV O S. On the role of twinning in dynamic recrystallization[J]. Physics of Metals and Metallography C, 2000, 89(4):384-390.,2000.
[21] 郭强,严红革,陈振华,张辉.AZ31镁合金高温热压缩变形特性[J].中国有色金属学报,2005(06):900-906.
[22] PARK S H, YU H, BAE J H, YIM C D, YOU B S. Microstructural evolution of indirect-extruded ZK60 alloy by adding Ce[J]. Journal of Alloy Compounds, 2012, 545:139-143.,2012.
上一张 下一张
上一张 下一张
计量
  • 下载量()
  • 访问量()
文章评分
  • 您的评分:
  • 1
    0%
  • 2
    0%
  • 3
    0%
  • 4
    0%
  • 5
    0%