以C18TAB为模板剂,氧氯化锆和四氯化锡为原料,采用共沉淀法成功合成了不同掺锡量的有序多孔氧化锆.通过XRD、N2吸-脱附、FT-IR等技术表征材料的孔结构.结果表明,掺锡氧化锆孔排布为六方有序,材料的热稳定性、比表面积均高,与C16TAB为模板剂合成的结果相比,d100值、孔容明显增大,S(5)Zd100增大了0.22 nm.
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