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以干燥的B粉和Mg粉为原料,采用分步反应法制备了SiC(40~45μm)掺杂的MgB2/Nb/Cu超导线材.通过X射线衍射仪(XRD)、扫描电子显微镜(SEM)研究了在650℃热处理温度下不同掺杂量对所制备样品的相组成、微观结构的影响.采用标准四引线法测定了样品的电阻温度曲线,结果表明,当该工艺第二步热处理温度为650℃时,反应不完全,应适当升高温度;同时高SiC掺杂量有利于在MgB2线材中引入更多B位C掺杂,表现为Tc略有降低,从而提高了其磁通钉扎特性.

参考文献

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