为了制备性能优良的Al基Pb—WC—CeO：惰性阳极材料，考察了WC、CeO：颗粒浓度对阴极极化的影响，正向脉冲参数、温度和搅拌对沉积速率以及复合镀层表面形貌的影响，并研究了其在锌电解液中的耐蚀性能，确定了脉冲电沉积制备Al基Pb-WC-C02复合镀层的最佳工艺条件：基础镀铅液中添加40g／LWC（粒径1斗m），30g／LCe02（粒径20～30nm），0．5一1．0g／L十六烷基三甲基溴化铵（CTAB-CDS），正向占空比30％，正向脉冲工作时间400ms，正向脉冲平均电流密度0．8A／dm。，温度40℃，搅拌速度300r／min。结果表明：所获镀层在锌电解液中较纯铅和Pb．WC镀层有较好的耐蚀性；脉冲镀层比直流镀层表面颗粒排列更平整、有序、致密，粒度较大，基质金属对颗粒的包覆程度更好，有更好的耐蚀性。
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