通过加入不同的有机添加剂，以电沉积一热氧化法制备了3种不同形貌的多孔SnO2薄膜，再电沉积Pt，制备得到不同形貌的多孔Pt／SnO2薄膜。通过扫描电镜（SEM）、x射线衍射（XRD）和循环伏安（CV）法分析了薄膜的形貌、结构和电催化氧化甲醇的活性。结果表明，不同形貌的多孔Pt／SnO2薄膜具有不同的电催化性能：SnO2镀液中添加聚乙二醇辛基苯基醚（OP，1．0mL／L）和苯甲醛（25mg／L），制得的SnO2薄膜呈一定规则排列的长条状，经氧化和电沉积Pt后的多孔Pt／SnO2薄膜具有良好的电催化氧化甲醇的活性及耐CO的性能。
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