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以氯化铁(FeCl3·6H2O)和氨水(NH3·H2O)为原料,以十六烷基三甲基溴化铵(CTAB)为表面活性剂,采用共沉淀法制备了氧化铁磁性微球.利用X射线衍射(XRD)、扫描电镜(SEM)和磁性测量系统(SQUID-VSM)对样品成分、形貌和磁学性能进行了表征分析.结果表明:所得氧化铁磁性微球为类球形斜方六面体结构,其粒径大小在0.8-1.Oum左右,剩余磁感应强度为0.13emu/g,矫顽力为1960Oe,表现出一定的铁磁性.

参考文献

[1] Jain G;Balasubramanian M;Xu JJ .Structural studies of lithium intercalation in a nanocrystalline alpha-Fe2O3 compound[J].Chemistry of Materials: A Publication of the American Chemistry Society,2006(2):423-434.
[2] Reddy MV;Yu T;Sow CH;Shen ZX;Lim CT;Rao GVS;Chowdari BVR .alpha-Fe2O3 nanoflakes as an anode material for Li-ion batteries[J].Advanced functional materials,2007(15):2792-2799.
[3] Zeng SY;Tang KB;Li TW;Liang ZH;Wang D;Wang YK;Qi YX;Zhou WW .Facile route for the fabrication of porous hematite nanoflowers: Its synthesis, growth mechanism, application in the lithium ion battery, and magnetic and photocatalytic properties[J].The journal of physical chemistry, C. Nanomaterials and interfaces,2008(13):4836-4843.
[4] Cheng F;Tao Z;Liang J;Chen J .Template-directed materials for rechargeable lithium-ion batteries[J].Chemistry of Materials: A Publication of the American Chemistry Society,2008(3):667-681.
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