{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":5,"startPagecode":1},"records":[{"abstractinfo":"以四氯化钛为反应前驱体,用低温水热法制备纯金红石相纳米TiO2,研究了反应温度和反应时间对TiO2微结构和形貌的影响.X-射线衍射分析表明,所有产物均为纯金红石型纳米TiO2,晶粒尺寸范围4.0～11.5 nm.红外光谱和热重分析表明,产物TiO2存在表面羟基和表面水.TEM分析表明,反应温度为60-80℃的TiO2样品呈梭形,且彼此聚集呈束状,但反应温度高于120℃时呈粒状,且粒径增加.随着反应时间(4-40 h)的延长,TiO2呈棒状,梭状及颗粒状.","authors":[{"authorName":"周利民","id":"3d283c95-a3d4-4195-9103-dc0429de3b0e","originalAuthorName":"周利民"},{"authorName":"梁喜珍","id":"0389c10a-23b1-436a-b070-f14d1d0ef8b1","originalAuthorName":"梁喜珍"},{"authorName":"<span style=\"color:red\">蔡</span><span style=\"color:red\">俊</span><span style=\"color:red\">青</span>","id":"2d0d9307-8c3c-4d0f-8d09-876fc2c84f2a","originalAuthorName":"蔡俊青"}],"doi":"","fpage":"208","id":"478cd80c-f8c4-4304-a104-6af8ec5539ef","issue":"2","journal":{"abbrevTitle":"CLYJXB","coverImgSrc":"journal/img/cover/CLYJXB.jpg","id":"16","issnPpub":"1005-3093","publisherId":"CLYJXB","title":"材料研究学报"},"keywords":[{"id":"f1b6ebfa-0ca3-4be2-b080-2eb4b4e88bc0","keyword":"无机非金属材料","originalKeyword":"无机非金属材料"},{"id":"ae7dd84d-2d3a-4035-a6e8-639fd9fe256a","keyword":"金红石型TiO2","originalKeyword":"金红石型TiO2"},{"id":"ef23df98-4906-4ff9-b34f-a374ba785bc9","keyword":"低温水热法","originalKeyword":"低温水热法"},{"id":"039bb812-4188-4640-851c-a16174a9c01a","keyword":"形貌","originalKeyword":"形貌"},{"id":"075ea415-c4d3-4c90-89e8-37ee06bd55a9","keyword":"反应温度","originalKeyword":"反应温度"},{"id":"9bb82f2b-48a5-4bde-afa9-3164f6638e23","keyword":"反应时间","originalKeyword":"反应时间"}],"language":"zh","publisherId":"clyjxb201002018","title":"用低温水热法制备可控形貌金红石型纳米TiO2","volume":"24","year":"2010"},{"abstractinfo":"介绍了<span style=\"color:red\">青</span>钢第二炼钢厂实现炼钢-连铸全工序负能炼钢的现状和在生产中为降低能耗所采取的技术措施,并对炼钢工艺流程和负能炼钢工序构成进行了改进.","authors":[{"authorName":"刘树海","id":"0a06c2ad-7798-4b06-9b2d-0aa009a6e5a3","originalAuthorName":"刘树海"},{"authorName":"牛锡云","id":"a30e4136-58d8-4865-9500-a3ceae2dbfac","originalAuthorName":"牛锡云"},{"authorName":"朱珉","id":"73d115d8-2175-4e8f-9ee8-99e5fff01bda","originalAuthorName":"朱珉"}],"doi":"","fpage":"14","id":"dd0cc474-c0a9-4a8a-b6a3-36b366d6d288","issue":"1","journal":{"abbrevTitle":"LZ","coverImgSrc":"journal/img/cover/LZ.jpg","id":"52","issnPpub":"1005-4006","publisherId":"LZ","title":"连铸"},"keywords":[{"id":"b5ffd402-0132-4db3-b764-908b0519149a","keyword":"转炉","originalKeyword":"转炉"},{"id":"c0092434-c8cf-4aff-ab31-72cd465a1172","keyword":"工艺优化","originalKeyword":"工艺优化"},{"id":"310903c1-3356-4340-8c42-dc86c7bc284b","keyword":"负能炼钢","originalKeyword":"负能炼钢"}],"language":"zh","publisherId":"lz200801005","title":"<span style=\"color:red\">青</span>钢负能炼钢概述","volume":"","year":"2008"},{"abstractinfo":"以1-羟基-N-[4-(2,4--特戊基-苯氧基-丁基)-2-萘甲酰胺为母体,以2,5-二巯基-1,3,4-噻二唑为吸附基团,分别以1-甲酰基-2-(4-氨基)苯肼,1-乙酰基-2-(4-氨基)苯肼和1-三氟乙酰基-2-(4-氨基)苯肼为增强基团合成了3种DAR<span style=\"color:red\">青</span>成色剂.结构经IR、1H NMR、MS及元素分析等检测确证.","authors":[{"authorName":"刘玉婷","id":"caa97f67-8f05-4c9c-8803-57e40b3fc206","originalAuthorName":"刘玉婷"},{"authorName":"吕峰","id":"37e69a53-c80b-46e7-a23c-18207a6f03df","originalAuthorName":"吕峰"},{"authorName":"邹竞","id":"8e449132-76d0-40d2-8e8e-67682e376c4c","originalAuthorName":"邹竞"},{"authorName":"张大德","id":"5196469c-c75d-464e-9281-0b253b6e1b39","originalAuthorName":"张大德"},{"authorName":"姚祖光","id":"7299efd3-5156-4877-af56-1c62bdc4c883","originalAuthorName":"姚祖光"}],"doi":"10.3969/j.issn.1000-0518.2004.06.016","fpage":"609","id":"32bea755-a47c-4bc3-be35-36deb4dbf8bf","issue":"6","journal":{"abbrevTitle":"YYHX","coverImgSrc":"journal/img/cover/YYHX.jpg","id":"73","issnPpub":"1000-0518","publisherId":"YYHX","title":"应用化学"},"keywords":[{"id":"747c9319-04a6-4f54-a730-3a1943717530","keyword":"DAR成色剂","originalKeyword":"DAR成色剂"},{"id":"2bb576f2-4aaf-425a-943b-8ac19757d32d","keyword":"合成","originalKeyword":"合成"}],"language":"zh","publisherId":"yyhx200406016","title":"DAR<span style=\"color:red\">青</span>成色剂的合成","volume":"21","year":"2004"},{"abstractinfo":"分析<span style=\"color:red\">青</span>钢小方坯连铸的现状及存在的问题,介绍高效连铸设备改造的方案和目标以及改造后的效果.","authors":[{"authorName":"吴晓文","id":"69f57e50-63a3-446b-bb68-8402dd1e3254","originalAuthorName":"吴晓文"}],"doi":"10.3969/j.issn.1005-4006.2001.06.006","fpage":"18","id":"4bb26ca7-20a7-4372-a578-41b56f6dae0e","issue":"6","journal":{"abbrevTitle":"LZ","coverImgSrc":"journal/img/cover/LZ.jpg","id":"52","issnPpub":"1005-4006","publisherId":"LZ","title":"连铸"},"keywords":[{"id":"6ae98429-35d9-4147-ac07-b8fbd62e9ede","keyword":"","originalKeyword":""}],"language":"zh","publisherId":"lz200106006","title":"<span style=\"color:red\">青</span>钢小方坯连铸高效改造","volume":"","year":"2001"},{"abstractinfo":"矿山金属平衡通过矿山金属产量实现了地质资源储量模型与矿山实际生产数据有机的结合,它涉及到储量评估、采矿计划、品位控制、矿山测量、选矿流程和产品销售等各个矿山生产环节.以<span style=\"color:red\">蔡</span>家营矿为例详细介绍了矿山金属平衡的操作步骤,实施矿山金属平衡不但可以评估矿山生产运作过程中财务现金流的风险,而且更重要的是运用实际品位数据来检验矿体矿块模型对采矿品位预计的可信度.","authors":[{"authorName":"梁涛","id":"4db6c0b4-2849-48c9-8284-1924cd18346c","originalAuthorName":"梁涛"},{"authorName":"卢仁","id":"12f6c54d-476c-4ec6-9349-0d1d5b907b04","originalAuthorName":"卢仁"},{"authorName":"吕胜利","id":"798ec94f-56a6-4a6b-b2b1-4d7b2dba45bf","originalAuthorName":"吕胜利"},{"authorName":"王书军","id":"1eb66d1f-a26a-46ac-bb0f-17754796659f","originalAuthorName":"王书军"},{"authorName":"刘明月","id":"db9462e3-990f-49cc-869b-2eb9e19d8516","originalAuthorName":"刘明月"},{"authorName":"张四维","id":"9704dcd6-3761-42e1-90a9-abd06a6f03c3","originalAuthorName":"张四维"}],"doi":"10.3969/j.issn.1001-1277.2010.09.008","fpage":"33","id":"276f67c7-9926-4144-b980-ca476b438ce6","issue":"9","journal":{"abbrevTitle":"HJ","coverImgSrc":"journal/img/cover/HJ.jpg","id":"44","issnPpub":"1001-1277","publisherId":"HJ","title":"黄金"},"keywords":[{"id":"59adb483-d722-4ab6-a33e-869876754a12","keyword":"矿山金属平衡","originalKeyword":"矿山金属平衡"},{"id":"b70fda73-0fee-4ebe-8ee1-5edf570404b1","keyword":"Micromine软件","originalKeyword":"Micromine软件"},{"id":"5eac0457-2b20-4ee9-9e7b-46993907204e","keyword":"<span style=\"color:red\">蔡</span>家营矿","originalKeyword":"蔡家营矿"}],"language":"zh","publisherId":"huangj201009008","title":"矿山金属平衡的应用——以<span style=\"color:red\">蔡</span>家营矿为例","volume":"31","year":"2010"},{"abstractinfo":"在工艺矿物学研究的基础上对含金0.084 g/t、硫2.74％的陕西<span style=\"color:red\">蔡</span>川铜尾矿进行了金的强化回收技术研究.结果表明,含金铜尾矿经过一次粗选、一次精选、一次扫选闭路流程可获得硫品位43.34％、回收率44.30％的硫精矿,其中金品位为1.26g/t、回收率为42.06％,达到计价标准.另外矿石中的银和镓元素也得到了一定程度的回收.理论分析结果显示,组合药剂的使用可大幅度提高含金矿物的选别效果,Y-89和丁基铵黑药的组合属于正—负型协同药剂,药剂基团中硫原子的Mulliken电荷分布是影响捕收剂选别性能的关键因素.","authors":[{"authorName":"刘明宝","id":"56fb3e34-3b54-4489-9bf7-82c08366462d","originalAuthorName":"刘明宝"},{"authorName":"杨超普","id":"e833885d-42ff-4dd3-a39e-666936e47fe5","originalAuthorName":"杨超普"},{"authorName":"阎赞","id":"1bea5843-bdd1-4e40-96d2-d451a868d4ee","originalAuthorName":"阎赞"},{"authorName":"印万忠","id":"c641e8f4-946b-41d9-94d4-78e7fb636315","originalAuthorName":"印万忠"}],"doi":"10.3969/j.issn.2095-1744.2016.05.013","fpage":"61","id":"0e228049-8998-421c-9974-9b7ac7be17a9","issue":"5","journal":{"abbrevTitle":"YSJSGC","coverImgSrc":"journal/img/cover/YSJSGC.jpg","id":"76","issnPpub":"2095-1744","publisherId":"YSJSGC","title":"有色金属工程"},"keywords":[{"id":"a81e098e-e47c-4fb2-8b06-a6e17609a946","keyword":"铜尾矿","originalKeyword":"铜尾矿"},{"id":"3deeda17-63a5-42a6-b747-abf688732cc2","keyword":"协同药剂","originalKeyword":"协同药剂"},{"id":"8c0e1c8f-f808-4870-91e6-fa75ff442474","keyword":"Mulliken电荷","originalKeyword":"Mulliken电荷"}],"language":"zh","publisherId":"ysjs201605013","title":"陕西<span style=\"color:red\">蔡</span>川铜矿含金铜尾矿中金的回收","volume":"6","year":"2016"},{"abstractinfo":"以含磺酸基离子液体1-(4-磺酸基)丁基-3-甲基咪唑四氟硼酸盐([4-sulfbmim][BF4])为酸性催化剂,由乙缩醛和苯甲醇合成了叶<span style=\"color:red\">青</span>素. 采用正交实验方法考察了合成条件的影响,固定反应温度为20 ℃条件下,确定优化合成条件为:n(苯甲醇):n(乙缩醛)=1:8,反应时间60 min,催化剂用量为每摩尔苯甲醇4 g,产率为92.2%. 与H2SO4催化剂相比[4-sulfbmim][BF4]的催化活性相对较弱,但综合效果优于H2SO4. [4-sulfbmim][BF4]循环使用6次,催化活性基本不变.","authors":[{"authorName":"易封萍","id":"4e14b741-bf29-4af7-8720-03b9b0ff842e","originalAuthorName":"易封萍"},{"authorName":"孙海洋","id":"49e433f9-5df5-4408-97ad-78e7009c98c9","originalAuthorName":"孙海洋"}],"doi":"10.3724/SP.J.1095.2010.90633","fpage":"860","id":"138e589f-df92-4166-a4ab-50c9439efcd0","issue":"7","journal":{"abbrevTitle":"YYHX","coverImgSrc":"journal/img/cover/YYHX.jpg","id":"73","issnPpub":"1000-0518","publisherId":"YYHX","title":"应用化学"},"keywords":[{"id":"8f011997-6b13-4709-8006-b94f8554f44c","keyword":"酸性功能化离子液体","originalKeyword":"酸性功能化离子液体"},{"id":"c77c609c-398f-4b9a-9c7a-64f1a9c7cc0d","keyword":"叶<span style=\"color:red\">青</span>素","originalKeyword":"叶青素"},{"id":"66716fe2-313e-48df-9ed6-8b80f748ab01","keyword":"乙醛乙基苄基缩醛","originalKeyword":"乙醛乙基苄基缩醛"},{"id":"8b20366d-5084-49d5-9653-ae04ed582c5b","keyword":"催化剂","originalKeyword":"催化剂"}],"language":"zh","publisherId":"yyhx201007022","title":"磺酸型离子液体催化合成叶<span style=\"color:red\">青</span>素","volume":"27","year":"2010"},{"abstractinfo":"采用离子交换色谱法对世界上分布最广、危害最重且最难防治的植物致病菌<span style=\"color:red\">青</span>枯菌进行了色谱表征.在以0.02 mol/L哌嗪-盐酸缓冲液(pH 8.0)为流动相、梯度洗脱条件下,<span style=\"color:red\">青</span>枯菌在SuperQ-650 C色谱柱(200 mm×4.6 mm i.d.)上被分离为3个不同的色谱峰.根据这3个组分的形态和生理生化性质,确定<span style=\"color:red\">青</span>枯菌原液和分离得到的3个组分都属于<span style=\"color:red\">青</span>枯菌的生化型Ⅲ型.通过2,3,4-三苯基氯化四氮唑(TTC)平板鉴定两个洗脱峰菌体的致病性及电镜观察二者的运动性,发现第一洗脱峰菌体的致病性弱于第二洗脱峰菌体而运动性强于后者.实验表明,通过离子交换色谱可以把常规微生物方法无法分离的<span style=\"color:red\">青</span>枯菌的不同状态区分出来.分离结果将为阐明<span style=\"color:red\">青</span>枯菌的多态性及传代培养过程中致病性逐渐减弱的内在机理,最终研制出特效的<span style=\"color:red\">青</span>枯菌抗菌剂具有重要意义.","authors":[{"authorName":"张洋","id":"9d97bb5c-3c4e-4d0a-8834-fb4d601f07bf","originalAuthorName":"张洋"},{"authorName":"温腾","id":"716e0146-57af-4093-8a94-3a349e769647","originalAuthorName":"温腾"},{"authorName":"林娟","id":"75c78616-51e9-468a-bf12-047261dde8c1","originalAuthorName":"林娟"},{"authorName":"谢智","id":"3e0826e6-d047-4413-8b3e-1e492b2acd86","originalAuthorName":"谢智"},{"authorName":"刘树滔","id":"3860dde4-eb91-4865-90fd-b901064c4da8","originalAuthorName":"刘树滔"},{"authorName":"饶平凡","id":"6ceb7f09-6b0f-4f6e-9e1e-b09151920e0e","originalAuthorName":"饶平凡"}],"doi":"10.3321/j.issn:1000-8713.2005.04.021","fpage":"418","id":"80e60727-9561-4c3f-aeef-495aabff1e9e","issue":"4","journal":{"abbrevTitle":"SP","coverImgSrc":"journal/img/cover/SP.jpg","id":"58","issnPpub":"1000-8713","publisherId":"SP","title":"色谱 "},"keywords":[{"id":"b39cb445-a806-473f-9b0c-c13e444bc66e","keyword":"离子交换色谱","originalKeyword":"离子交换色谱"},{"id":"3c40f935-a17e-42b7-8353-751064a6c6a1","keyword":"<span style=\"color:red\">青</span>枯菌","originalKeyword":"青枯菌"},{"id":"04437d81-a98f-4930-9cca-c817516e5ac9","keyword":"生化鉴定","originalKeyword":"生化鉴定"},{"id":"649b139e-0dfe-4fc4-9cad-cf0e2c00b699","keyword":"多态性","originalKeyword":"多态性"}],"language":"zh","publisherId":"sp200504021","title":"离子交换色谱法分离<span style=\"color:red\">青</span>枯菌及其色谱峰的鉴定","volume":"23","year":"2005"},{"abstractinfo":"应用高效离子交换色谱和激光光散射仪在线检测,快速分离定量不同致病力的<span style=\"color:red\">青</span>枯菌.<span style=\"color:red\">青</span>枯菌经过高效离子交换色谱分离得到3个特征峰,通过2,3,5-三苯基氯化四氮唑(TTC)平板鉴定和采用剪叶法回接番茄组培苗感染试验,发现这3个色谱峰所对应的<span style=\"color:red\">青</span>枯菌在致病力方面存在差异;其中峰3组分的致病力最强,峰1组分的致病力最弱.通过对<span style=\"color:red\">青</span>枯菌进样量与激光光散射仪的响应信号(峰面积)之间的线性关系研究,发现当<span style=\"color:red\">青</span>枯菌进样菌数为9×106～9×108时,菌数与色谱峰面积之间呈现出良好的线性关系,相关系数r=0.99.该项应用研究为不同致病力<span style=\"color:red\">青</span>枯菌的快速定量提供了一种新的分析方法.","authors":[{"authorName":"林娟","id":"8112c1d4-38bc-4a6b-8ef9-858ecf8e7b99","originalAuthorName":"林娟"},{"authorName":"马骋","id":"0e250cf7-57e0-431d-ac87-c2e484a86ab8","originalAuthorName":"马骋"},{"authorName":"刘树滔","id":"da7551a2-e12c-4955-b55f-93554cdd3842","originalAuthorName":"刘树滔"},{"authorName":"吴玲玲","id":"d21479a7-bf71-4345-b4f7-b026ef788c6d","originalAuthorName":"吴玲玲"},{"authorName":"饶平凡","id":"af9bd11f-fe80-46b3-b8ec-8b27c9393d97","originalAuthorName":"饶平凡"}],"doi":"10.3321/j.issn:1000-8713.2007.01.014","fpage":"70","id":"ad0d561c-9fdc-49ae-bb3e-8ff6cb217b06","issue":"1","journal":{"abbrevTitle":"SP","coverImgSrc":"journal/img/cover/SP.jpg","id":"58","issnPpub":"1000-8713","publisherId":"SP","title":"色谱 "},"keywords":[{"id":"35192a0a-5186-4de9-9e2e-4ecba644f0be","keyword":"高效离子交换色谱","originalKeyword":"高效离子交换色谱"},{"id":"b3b6a855-aac4-4102-925e-57ae76d8ad79","keyword":"激光光散射仪","originalKeyword":"激光光散射仪"},{"id":"3d600c9d-e6b7-4505-a7f4-3b55d03e0ce5","keyword":"<span style=\"color:red\">青</span>枯菌","originalKeyword":"青枯菌"},{"id":"f4ad49db-d1b9-4e03-aba4-83bc14034a47","keyword":"致病力","originalKeyword":"致病力"},{"id":"8cc7ecaf-f6ed-48e8-a201-67b80d62587f","keyword":"分离","originalKeyword":"分离"},{"id":"7e5ee153-852f-4b6f-91f3-66f955e84ccd","keyword":"定量","originalKeyword":"定量"}],"language":"zh","publisherId":"sp200701014","title":"应用高效离子交换色谱快速分离定量不同致病力的<span style=\"color:red\">青</span>枯菌","volume":"25","year":"2007"},{"abstractinfo":"建立了高效离子交换色谱和紫外检测系统快速分离<span style=\"color:red\">青</span>枯雷尔氏菌的细菌色谱方法.通过比较<span style=\"color:red\">青</span>枯雷尔氏菌悬浮在哌嗪-HCl缓冲体系和双蒸水后的菌体数变化及细胞形态变化,分析该缓冲液对<span style=\"color:red\">青</span>枯雷尔氏菌生长活性及细胞表面特性的影响.结果表明,<span style=\"color:red\">青</span>枯雷尔氏菌悬浮在乎衡缓冲液、洗脱缓冲液和双蒸水中的菌体数量无明显差异,分别为6.467× 109、6.267× 109和6.233× 109 cfu/mL.透射电镜观察发现,3种溶液处理后,<span style=\"color:red\">青</span>枯雷尔氏菌均保持完整的细胞结构研究了缓冲液pH值、流速及菌体细胞浓度对<span style=\"color:red\">青</span>枯雷尔氏菌色谱分离效果的影响,确定<span style=\"color:red\">青</span>枯雷尔氏菌的最佳色谱分离条件为:缓冲液pH值为8.0,流速为2 mL/min,菌体浓度大于1.0× 108 cfu/mL且小于1.0× 1010cfu/mL.该分离条件缩短了分离时间,提高了分离效率,为快速分离<span style=\"color:red\">青</span>枯雷尔氏菌提供了一种有效的手段,同时也为细菌等微生物的分离提供了新途径.","authors":[{"authorName":"郑雪芳","id":"907ee62c-28b3-4325-a2f4-aea6a26488dd","originalAuthorName":"郑雪芳"},{"authorName":"刘波","id":"7b47ae6a-ad67-480c-b51d-b6918a864235","originalAuthorName":"刘波"},{"authorName":"朱育菁","id":"b9952f82-94d5-4c37-be07-402a2792101a","originalAuthorName":"朱育菁"},{"authorName":"陈德局","id":"be26aac8-6ec0-4c4c-a3b6-4b85cdf7b49e","originalAuthorName":"陈德局"}],"doi":"10.3724/SP.J.1123.2016.06044","fpage":"1091","id":"24aac966-5573-476b-962a-6a4211c989ec","issue":"11","journal":{"abbrevTitle":"SP","coverImgSrc":"journal/img/cover/SP.jpg","id":"58","issnPpub":"1000-8713","publisherId":"SP","title":"色谱 "},"keywords":[{"id":"f0f84c50-e3f7-4689-8ac4-62421666b585","keyword":"高效离子交换色谱","originalKeyword":"高效离子交换色谱"},{"id":"25b2cf27-fc1a-450d-816a-5aaebf69732f","keyword":"分离","originalKeyword":"分离"},{"id":"27393040-9df5-45df-9b69-9af420d98220","keyword":"<span style=\"color:red\">青</span>枯雷尔氏菌","originalKeyword":"青枯雷尔氏菌"},{"id":"58f11eb5-6a94-4566-9b66-7779b03dc09b","keyword":"细胞表面特性","originalKeyword":"细胞表面特性"}],"language":"zh","publisherId":"sp201611011","title":"<span style=\"color:red\">青</span>枯雷尔氏菌特征菌株高效离子交换色谱快速分离条件的优化","volume":"34","year":"2016"}],"totalpage":7,"totalrecord":68}