利用透射电镜对冷轧变形所致纳米结构金属镍的微结构组织演变特征进行了研究.结果表明,经过轧制变形后,纳米晶的平均晶粒尺寸为50~70 mm,有少量位错结构,但没有发现位错堆积缠结;在晶界处及附近有台阶界面结构,以及与台阶形状相对应的应力场衬度.在变形后期,可以靠晶界发射不全位错从而促使层错生成,并依赖层错尺寸长大(即层错界面位错)的运动进行.而当层错尺寸长大时,其前沿局部变形应力逐渐变大,直至该应力大到一定值时,位错停止运动,层错尺寸也不再长大,并留下了台阶结构.
参考文献
[1] | Legros M.;Rittner MN.;Weertman JR.;Hemker KJ.;Elliott BR. .Microsample tensile testing of nanocrystalline metals[J].Philosophical Magazine.A.Physics of condensed matter, defects and mechanical properties,2000(4):1017-1026. |
[2] | van Swygenhoven H;Weertman J R .Preface to the viewpoint set on:mechanical properties of fully dense nanocrystalline metals[J].Scripta Materialia,2003,49:625-627. |
[3] | Mingwei Chen;En Ma;Kevin J. Hemker;Hongwei Sheng;Yinmin Wang;Xuemei Cheng .Deformation Twinning in Nanocrystalline Aluminum[J].Science,2003(5623):1275-1277. |
[4] | K. S. Kumar;S. Suresh;M. F. Chisholm;J. A. Horton;P. Wang .Deformation of electrodeposited nanocrystalline nickel[J].Acta materialia,2003(2):387-405. |
[5] | Wang Y;Chen M;Zhou F;Ma E .High tensile ductility in a nanostructured metal.[J].Nature,2002(6910):912-915. |
[6] | J. Sort;A. Zhilyaev;M. Zielinska .Microstructural effects and large microhardness in cobalt processed by high pressure torsion consolidation of ball milled powders[J].Acta materialia,2003(20):6385-6393. |
[7] | Lu L;Sui M L;Lu K .Superplastic extensibility of nanocrystalline copper at room temperature[J].Science,2000,287:1463-1466. |
[8] | B. Cai;Q.P. Kong;P. Cui .Creep behavior of cold-rolled nanocrystalline pure copper[J].Scripta materialia,2001(12):1407-1413. |
[9] | K. S. Kumar;S. Suresh;M. F. Chisholm;J. A. Horton;P. Wang .Deformation of electrodeposited nanocrystalline nickel[J].Acta materialia,2003(2):387-405. |
[10] | R. C. Hugo;H. Kung;J. R. Weertman;R. Mitra;J. A. Knapp;D. M. Follstaedt .In-situ TEM tensile testing of DC magnetron sputtered and pulsed laser deposited Ni thin films[J].Acta materialia,2003(7):1937-1943. |
[11] | Budrovic Z;Van Swygenhoven H;Derlet PM;Van Petegem S;Schmitt B .Plastic deformation with reversible peak broadening in nanocrystalline nickel[J].Science,2004(5668):273-276. |
[12] | M. Yu. Gutkin;I. A. Ovid'ko;N. V. Skiba .Crossover from grain boundary sliding to rotational deformation in nanocrystalline materials[J].Acta materialia,2003(14):4059-4071. |
[13] | A.A. Fedorov;M.Yu. Gutkin;I.A. Ovid'ko .Transformations of grain boundary dislocation pile-ups in nano-and polycrystalline materials[J].Acta materialia,2003(4):887-898. |
[14] | V. Yamakov;D. Wolf;S. R. Phillpot;H. Gleiter .Dislocation-dislocation and dislocation-twin reactions in nanocrystalline Al by molecular dynamics simulation[J].Acta materialia,2003(14):4135-4147. |
[15] | Van Swygenhoven H .Polycrystalline materials - Grain boundaries and dislocations[J].Science,2002(5565):66-67. |
[16] | Schiotz J;Jacobsen KW .A maximum in the strength of nanocrystalline copper[J].Science,2003(5638):1357-1359. |
[17] | Van Swygenhoven H.;Derlet PM.;Hasnaoui A. .Atomic mechanism for dislocation emission from nanosized grain boundaries - art. no. 024101[J].Physical Review.B.Condensed Matter,2002(2):4101-0. |
[18] | P. M. Derlet;A. Hasnaoui;H. Van Swygenhoven .Atomistic simulations as guidance to experiments[J].Scripta materialia,2003(7):629-635. |
[19] | A. Froseth;H. Van Swygenhoven;P.M. Derlet .The influence of twins on the mechanical properties of nc-Al[J].Acta materialia,2004(8):2259-2268. |
[20] | Morris D G;Morris M A .Microstructure and strength of nanocrystalline copper alloy prepared by mechanical alloying[J].Acta Musicologica,1991,39:1763-1767. |
[21] | Derlet P M;van Swygenhoven H .Fracture of nanolamellar materials:continuum and atomistic models with application to titanium aluminides[J].Philosophical Magazine A:Physics of Condensed Matter:Structure,Defects and Mechanical Properties,2002,82(12):2397-2417. |
[22] | Farkas D.;Van Swygenhoven H.;Derlet PM. .Intergranular fracture in nanocrystalline metals - art. no. 060101[J].Physical Review.B.Condensed Matter,2002(6):101-0. |
[23] | Mullner P;Solenthaler C .On the effect of deformation twinning on defect densities[J].Materials Science and Engineering A,1997,230:107-115. |
上一张
下一张
上一张
下一张
计量
- 下载量()
- 访问量()
文章评分
- 您的评分:
-
10%
-
20%
-
30%
-
40%
-
50%