{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":5,"startPagecode":1},"records":[{"abstractinfo":"采用微弧氧化工艺分别在钨酸盐和磷酸盐电解液中制备了WO_3/TiO_2复合薄膜和单一的TiO_2膜(P-TiO_2),利用X射线衍射、扫描电子显微镜、紫外-可见光谱和荧光光谱对这两种膜层的结构及光物理特性进行了表征.结果表明,P-TiO_2膜由锐钛矿与金红石混合相组成,而WO_3/TiO_2膜中除锐钛矿与金红石混合相外,还含有W0O相.两种膜层表面粗糙多孔,WO_3/TiO_2膜的孔洞数量更多,分布更均匀.WO_3/TiO_2膜的光吸收范围较P-TiO_2膜略宽,但后者在紫外光区的光吸收性能更好.WO_3O/TiO_2膜的荧光发光强度比P-TiO_2的小,光生电子-空穴之间的分离效果好.与P-TiO_2膜相比,WO_3/TiO_2膜的表面酸度高,吸附有机物和羟基的能力更强.紫外光下照射2 h,WO_3/TiO_2能够降解85%罗丹明,而P-TiO_2膜只能降解23%.WO_3/Ti0_2膜的高光催化活性源于它较高的比表面积、较优的电子.空穴分离效果和较高的表面酸度.","authors":[{"authorName":"何剑","id":"ec5d650e-a61c-44fa-b3d4-22cdf5160c3c","originalAuthorName":"何剑"},{"authorName":"蔡启舟","id":"0fbb3b99-d0a9-4b65-81da-54e6e371df81","originalAuthorName":"蔡启舟"},{"authorName":"<span style=\"color:red\">肖</span><span style=\"color:red\">枫</span>","id":"0c564948-75d5-47d3-a9d9-d917274f1933","originalAuthorName":"肖枫"},{"authorName":"罗强","id":"749e56b5-7677-4637-b781-7b45eaabba8e","originalAuthorName":"罗强"},{"authorName":"王丽娟","id":"1c4c19fa-957e-4d81-a9fa-eaed174d2b7f","originalAuthorName":"王丽娟"},{"authorName":"祝迪","id":"401ddefb-fc01-406e-b8d3-c6ff9f0ef034","originalAuthorName":"祝迪"}],"doi":"","fpage":"1137","id":"39451b37-1d35-478c-ba61-4e23b83ae7ca","issue":"11","journal":{"abbrevTitle":"CHXB","coverImgSrc":"journal/img/cover/CHXB.jpg","id":"18","issnPpub":"0253-9837","publisherId":"CHXB","title":"催化学报   "},"keywords":[{"id":"ff267be5-44f5-42e1-ae47-e428a787f139","keyword":"钨","originalKeyword":"钨"},{"id":"bb360925-903e-4a9c-ab52-39826c5dd1e5","keyword":"钛","originalKeyword":"钛"},{"id":"61e3e4b8-7aec-4ed5-8cc8-f8cfebc6cf9d","keyword":"微弧氧化","originalKeyword":"微弧氧化"},{"id":"d4e61a64-9aa8-4b48-9d65-8b56f21528f1","keyword":"电解液","originalKeyword":"电解液"},{"id":"d866b9be-0c33-4c1c-a49b-f6d52e541918","keyword":"二氧化钛膜","originalKeyword":"二氧化钛膜"},{"id":"35e07bf8-e73b-4d36-81fe-e1f9b87d3a0e","keyword":"光催化","originalKeyword":"光催化"}],"language":"zh","publisherId":"cuihuaxb200911012","title":"微弧氧化法制备WO_3/TiO_2复合薄膜的结构及光催化性能","volume":"30","year":"2009"},{"abstractinfo":"为了推动SnO2光催化的实际应用,采用微弧氧化工艺在锡酸盐电解液中制备了SnO2薄膜,利用扫描电子显微镜、X射线衍射、紫外-可见分光光度计对膜层的结构及光物理特性进行表征.结果表明:膜层由单一SnO2相组成,表面粗糙多孔,沉积的SnO2如树根状向四周延伸;内部致密,无孔洞,与基体结合良好.SnO2膜在紫外区吸光性能良好,光吸收截止边缘为390 nm.紫外光下照射10 h,SnO2能够降解83%罗丹明.SnO2膜的高光催化活性源于其开放的表面结构和良好的吸光性能.","authors":[{"authorName":"何剑","id":"e1ee0e6c-5762-4ece-86cd-a664bca042ed","originalAuthorName":"何剑"},{"authorName":"蔡启舟","id":"87a16a5a-00a2-40a1-93c9-8842ffae6927","originalAuthorName":"蔡启舟"},{"authorName":"<span style=\"color:red\">肖</span><span style=\"color:red\">枫</span>","id":"2dcdd716-d054-4e2b-bd0d-32dd73d55a8b","originalAuthorName":"肖枫"},{"authorName":"罗强","id":"7cfc839e-bc91-4487-9ad5-77655d969457","originalAuthorName":"罗强"},{"authorName":"张丹青","id":"837a2222-4c11-452c-8d81-24a43258af64","originalAuthorName":"张丹青"},{"authorName":"陈喜娣","id":"6220447d-ca9e-4010-b54b-ee6a36ce2cdf","originalAuthorName":"陈喜娣"}],"doi":"","fpage":"38","id":"7a9a26e3-cee8-4bb5-8a33-b5f33ee1daf3","issue":"2","journal":{"abbrevTitle":"CLKXYGY","coverImgSrc":"journal/img/cover/CLKXYGY.jpg","id":"14","issnPpub":"1005-0299","publisherId":"CLKXYGY","title":"材料科学与工艺"},"keywords":[{"id":"93aa742c-19db-4042-ab9c-a4cc1c497675","keyword":"锡","originalKeyword":"锡"},{"id":"a4814237-d163-4404-a6e6-3ce40fd17d72","keyword":"钛","originalKeyword":"钛"},{"id":"602e3a44-f120-4362-a680-2af7f078f13b","keyword":"微弧氧化","originalKeyword":"微弧氧化"},{"id":"702d458b-6b32-4d57-8522-a7ed5752c551","keyword":"电解液","originalKeyword":"电解液"},{"id":"099c880f-5738-4ddc-b24f-82ebacb16b92","keyword":"光催化","originalKeyword":"光催化"}],"language":"zh","publisherId":"clkxygy201102009","title":"多孔SnO2薄膜的微弧氧化制备及光催化性能研究","volume":"19","year":"2011"},{"abstractinfo":"剖析了邯钢7号高炉配套的比<span style=\"color:red\">肖</span>夫式煤气洗涤塔的结构特点,运行状况与噪声超标、挂板脱落、橡胶补偿器易损坏、液压伺服阀堵塞、鲎口自动闭合堵塞气、液通道问题的具体原因,制定了相应的技术改造方案.实施后,取得了能够满足高炉与TRT正常生产和发电的需要,噪声也达到了国标要求,效果良好.","authors":[{"authorName":"杨子彬","id":"93e441ad-f505-4ff4-a99a-a92d98209107","originalAuthorName":"杨子彬"},{"authorName":"杨殿卿","id":"a38008b8-68d1-474a-97cc-61119b7b4d89","originalAuthorName":"杨殿卿"}],"doi":"10.3969/j.issn.1006-9356.2008.12.008","fpage":"32","id":"e61bd9c8-1aa7-4834-875e-e66cd2e05f8f","issue":"12","journal":{"abbrevTitle":"ZGYJ","coverImgSrc":"journal/img/cover/ZGYJ.jpg","id":"87","issnPpub":"1006-9356","publisherId":"ZGYJ","title":"中国冶金"},"keywords":[{"id":"3283fdb8-1c01-403c-865c-2bb880916cd3","keyword":"比<span style=\"color:red\">肖</span>夫式高炉煤气洗涤塔","originalKeyword":"比肖夫式高炉煤气洗涤塔"},{"id":"d6ca729c-7309-427c-9f38-db0d52663bb3","keyword":"结构技术改造","originalKeyword":"结构技术改造"}],"language":"zh","publisherId":"zgyj200812008","title":"比<span style=\"color:red\">肖</span>夫式高炉煤气洗涤塔的技术改造","volume":"18","year":"2008"},{"abstractinfo":"杏<span style=\"color:red\">枫</span>山金矿床位于湘中白马山—龙山东西向构造带与古台山—新宁南北向构造带的交汇部位,是一典型的石英细脉带型金矿床.在研究矿区地质特征基础上,通过对矿体特征、矿石成分、成矿作用过程等分析研究,提出该矿床成矿模式.认为该矿床的形成主要经历了4个阶段:第一阶段,青白口系高涧群初始矿源层的形成；第二阶段,区域深大断裂,变质作用阶段,金元素聚集、分解、化合、氧化、还原、沉淀、再循环,形成矿化富集层；第三阶段,多次岩浆活动,成矿热液形成,断裂构造活动,形成运移通道；第四阶段,岩浆活动,旧断裂复活,新断裂产生,金富集成矿.","authors":[{"authorName":"陈武","id":"e10115ae-dafb-46b5-a11a-507d5fcd8f9d","originalAuthorName":"陈武"},{"authorName":"张寿庭","id":"1c45581a-d164-4eaf-b196-439448a3766e","originalAuthorName":"张寿庭"},{"authorName":"伦生平","id":"0f004897-ddf7-41f1-aa28-daedd2b6b727","originalAuthorName":"伦生平"}],"doi":"10.11792/hj20130205","fpage":"16","id":"9980d6cd-0f02-4999-a020-7213819003e1","issue":"2","journal":{"abbrevTitle":"HJ","coverImgSrc":"journal/img/cover/HJ.jpg","id":"44","issnPpub":"1001-1277","publisherId":"HJ","title":"黄金"},"keywords":[{"id":"a27a477a-b91b-4820-87c2-fb503e457da6","keyword":"杏<span style=\"color:red\">枫</span>山金矿床","originalKeyword":"杏枫山金矿床"},{"id":"3683ebfb-731d-4b05-ba8e-28d2da9ee3ab","keyword":"地质特征","originalKeyword":"地质特征"},{"id":"d4ffb169-0777-4d9a-9d9c-dec3c5a5f763","keyword":"成矿模式","originalKeyword":"成矿模式"},{"id":"e748319d-15d5-4ab9-806a-b76016d305be","keyword":"湖南","originalKeyword":"湖南"}],"language":"zh","publisherId":"huangj201302005","title":"湖南省隆回县杏<span style=\"color:red\">枫</span>山金矿床地质特征及成矿模式探讨","volume":"34","year":"2013"},{"abstractinfo":"建立了基于液相色谱-离子阱飞行时间串联质谱(LC-IT-TOF MS/MS)的酚酸类分析方法,对6种共18批次的石斛<span style=\"color:red\">枫</span>斗药材中的酚类化合物进行了研究,其中18种酚酸类化合物得到初步定性.在共有化合物中选择杓唇石斛素和石斛酚作为质量控制的目标化合物.在此基础上,采用响应面法(RSM)确定了提取溶剂为60%甲醇、提取时间为65 min的超声提取杓唇石斛素和石斛酚的最佳条件,建立了石斛<span style=\"color:red\">枫</span>斗中杓唇石斛素、石斛酚的高效液相色谱(HPLC)含量测定方法.定量线性优于0.999 8,检出限(LOD)分别为0.18 mg/L 和0.09 mg/L,重复性的相对标准偏差(RSD)小于3% ,加标回收率均值分别为97.1%和101.4% .这些结果表明本研究建立的方法可用于石斛<span style=\"color:red\">枫</span>斗药材中酚酸类化学成分研究及质量控制.","authors":[{"authorName":"周婧","id":"067cb7e8-095c-40fc-8ecb-c08d377f8c8f","originalAuthorName":"周婧"},{"authorName":"许志良","id":"4b98e4e2-43ba-4491-90bd-b0229a9a86fe","originalAuthorName":"许志良"},{"authorName":"孔宏伟","id":"382243e4-e058-4a55-a253-789791aef19e","originalAuthorName":"孔宏伟"},{"authorName":"路鑫","id":"54ea0da4-e9a8-49cd-9f2f-2d6da90c5570","originalAuthorName":"路鑫"},{"authorName":"许国旺","id":"f00dafb0-cfdd-4af2-9106-9e1956277234","originalAuthorName":"许国旺"}],"doi":"10.3724/SP.J.1123.2010.00566","fpage":"566","id":"86c11be2-2c95-4665-a82b-8da6eaa9c95f","issue":"6","journal":{"abbrevTitle":"SP","coverImgSrc":"journal/img/cover/SP.jpg","id":"58","issnPpub":"1000-8713","publisherId":"SP","title":"色谱 "},"keywords":[{"id":"9cacd447-3042-4773-b8b5-edfa1d879917","keyword":"液相色谱-离子阱飞行时间串联质谱","originalKeyword":"液相色谱-离子阱飞行时间串联质谱"},{"id":"7e8da7a8-b7a1-4016-9785-09397dc229b3","keyword":"含量","originalKeyword":"含量"},{"id":"255b5145-2ae0-4496-b5e8-af6d7c36757b","keyword":"酚酸类物质","originalKeyword":"酚酸类物质"},{"id":"6b62b59f-8b15-47bb-b404-9f44f2ed1a21","keyword":"杓唇石斛素","originalKeyword":"杓唇石斛素"},{"id":"ce7e68d3-5e3d-438c-9be8-52d175dbc4b8","keyword":"石斛酚","originalKeyword":"石斛酚"},{"id":"77826760-45f4-4cd4-ae05-bc1e1ec9dfeb","keyword":"石斛<span style=\"color:red\">枫</span>斗","originalKeyword":"石斛枫斗"}],"language":"zh","publisherId":"sp201006009","title":"不同石斛<span style=\"color:red\">枫</span>斗中酚酸类活性成分的比较及杓唇石斛素和石斛酚含量的测定","volume":"28","year":"2010"},{"abstractinfo":"","authors":[{"authorName":"王光雍","id":"1129dcae-ced5-4d4c-a4d9-3db047f5cafb","originalAuthorName":"王光雍"}],"doi":"","fpage":"4","id":"553920b6-77df-4efa-8106-15360a4a033c","issue":"10","journal":{"abbrevTitle":"CLDB","coverImgSrc":"journal/img/cover/CLDB.jpg","id":"8","issnPpub":"1005-023X","publisherId":"CLDB","title":"材料导报"},"keywords":[{"id":"acfc091b-2d2e-499a-a3de-68caac9ccfd3","keyword":"","originalKeyword":""}],"language":"zh","publisherId":"cldb200010002","title":"<span style=\"color:red\">肖</span>纪美先生简介","volume":"14","year":"2000"},{"abstractinfo":"","authors":[{"authorName":"尚成嘉","id":"d7e1874a-7cbd-49b9-a205-592594f882b6","originalAuthorName":"尚成嘉"}],"doi":"10.3969/j.issn.1000-6826.2014.03.01","fpage":"1","id":"8734de45-7ba1-4157-b7f7-e8407fd32c5d","issue":"3","journal":{"abbrevTitle":"JSSJ","coverImgSrc":"journal/img/cover/3abe017a-2574-4821-8152-4ae974ef0471.jpg","id":"47","issnPpub":"1000-6826","publisherId":"JSSJ","title":"金属世界"},"keywords":[{"id":"ce9e716e-8048-4e12-8029-8e8a00e3eb61","keyword":"","originalKeyword":""}],"language":"zh","publisherId":"jssj201403001","title":"斯人远去 风范长存——缅怀<span style=\"color:red\">肖</span>纪美先生","volume":"","year":"2014"},{"abstractinfo":"","authors":[{"authorName":"尚成嘉","id":"5920da76-f5e0-48a6-bb79-2b2d7006db68","originalAuthorName":"尚成嘉"}],"doi":"10.3969/j.issn.1000-6826.2014.03.02","fpage":"3","id":"a6f74bed-caa0-40e0-8409-6621dea960e3","issue":"3","journal":{"abbrevTitle":"JSSJ","coverImgSrc":"journal/img/cover/3abe017a-2574-4821-8152-4ae974ef0471.jpg","id":"47","issnPpub":"1000-6826","publisherId":"JSSJ","title":"金属世界"},"keywords":[{"id":"474df513-2829-4474-bc2b-eaedc2a19b24","keyword":"","originalKeyword":""}],"language":"zh","publisherId":"jssj201403002","title":"<span style=\"color:red\">肖</span>纪美教授教学与科技活动概览","volume":"","year":"2014"},{"abstractinfo":"","authors":[{"authorName":"王晶莹","id":"a2b0f8be-f760-4d84-9531-cd3f3fa349df","originalAuthorName":"王晶莹"}],"doi":"10.3969/j.issn.2095-1744.2011.03.001","fpage":"5","id":"162b6dac-f1cf-4ea2-bd88-56f37312bb6c","issue":"3","journal":{"abbrevTitle":"YSJSGC","coverImgSrc":"journal/img/cover/YSJSGC.jpg","id":"76","issnPpub":"2095-1744","publisherId":"YSJSGC","title":"有色金属工程"},"keywords":[{"id":"9506fa5a-dadf-4291-856b-b5cdb43187ed","keyword":"","originalKeyword":""}],"language":"zh","publisherId":"ysjs201103001","title":"从金属学到断裂学科的研究变革及学科交叉的思想探寻——访中国科学院院士<span style=\"color:red\">肖</span>纪美","volume":"","year":"2011"},{"abstractinfo":"以1,4-双(4-氨基-2-三氟甲基苯氧基)苯(6FAPB)为含氟二胺单体,均苯四甲酸二酐(PMDA)和1,2,3,4-环丁烷四酸二酐(CBDA)为二酐单体,经低温溶液缩聚反应得到聚酰胺酸,再经热酰亚胺化处理制备出含氟共聚聚酰亚胺(CPI)薄膜.采用红外(IR)、紫外(UV-Vis)、溶解性测试等对CPI进行结构与性能表征,考察两种二酐单体的不同物质的量之比对共聚聚酰亚胺光学性能和溶解性的影响.结果表明:随着脂环二酐CBDA摩尔配比的增加,CPI薄膜在410 nm处的光透过率逐渐增加,薄膜颜色逐渐变浅,溶解性有所改善.","authors":[{"authorName":"鲁云华","id":"09c92763-7a3d-4860-aac7-8c0672f668bd","originalAuthorName":"鲁云华"},{"authorName":"赵洪斌","id":"e79d0f1c-bcd6-4a61-b298-1e6a823e69ff","originalAuthorName":"赵洪斌"},{"authorName":"迟海军","id":"4d06d6df-470b-4836-9e14-6a9e68a798fb","originalAuthorName":"迟海军"},{"authorName":"董岩","id":"65896635-a332-4856-ad38-77ddf2d37753","originalAuthorName":"董岩"},{"authorName":"<span style=\"color:red\">肖</span>国勇","id":"6738b002-e0b1-4cb3-831f-bed85cb05445","originalAuthorName":"肖国勇"},{"authorName":"胡知之","id":"7c4d40f4-1977-435e-ab13-ebd318d5c61d","originalAuthorName":"胡知之"}],"doi":"","fpage":"1","id":"e73a30ed-13db-43ea-bea4-6581231b1334","issue":"1","journal":{"abbrevTitle":"JYCL","coverImgSrc":"journal/img/cover/JYCL.jpg","id":"50","issnPpub":"1009-9239","publisherId":"JYCL","title":"绝缘材料"},"keywords":[{"id":"6a5dd4f9-b106-4267-949f-792555f6ac67","keyword":"聚酰亚胺","originalKeyword":"聚酰亚胺"},{"id":"81daa9c0-a188-4bf7-becd-eb9025259934","keyword":"共缩聚","originalKeyword":"共缩聚"},{"id":"4fa37438-567f-4a66-bd23-7b745ed05d4e","keyword":"含氟","originalKeyword":"含氟"},{"id":"e0608fa6-5b7a-44b4-9f6c-533a67987ef0","keyword":"结构与性能","originalKeyword":"结构与性能"}],"language":"zh","publisherId":"jycltx201301001","title":"含氟共聚聚酰亚胺的合成与性能研究鲁云华,赵洪斌,迟海军,董岩,<span style=\"color:red\">肖</span>国勇,胡知之","volume":"","year":"2013"}],"totalpage":5,"totalrecord":43}