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用磁控溅射技术在钢基片上沉积出具有T区结构的TiB2薄膜,研究基片偏压对薄膜的影响.使用X射线衍射技术和扫描电镜分析薄膜的特性.发现在本研究工艺条件下,所有的薄膜均呈(001)晶面择优生长.当基片偏压在-50 V时,薄膜的硬度为50 GPa,抗塑性变形的能力为0.65 GPa.加大基片偏压,导致薄膜晶粒尺寸减小,同时薄膜的硬度和抗塑性变形的能力也下降.扫描电镜分析显示,基片温度对T区结构的影响是明显的,提高基片温度,当Ts/Tm=0.18时.薄膜中出现"等轴"结构.

参考文献

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[4] Microstructural evolution during film growth[J].Journal of Vacuum Science & Technology, A. Vacuum, Surfaces, and Films,2003(5):S117-S128.
[5] W.C. Oliver;G.M. Pharr .Measurement of hardness and elastic modulus by instrumented indentation: Advances in understanding and refinements to methodology[J].Journal of Materials Research,2004(1):3-20.
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