材料科学与工艺, 2010, 18(1): 51-55.
催化乳酸铵酯化的改性树脂的制备与表征
赵文军 1, , 汪群慧 2, , 滕云 3, {"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":5,"startPagecode":1},"records":[{"abstractinfo":"硫化锡(SnS)具有很高的光吸收系数和合适的禁带宽度,又无毒性,因此在太阳电池等光电器件中具有潜在应用价值.本文用真空蒸发法制备掺杂的SnS薄膜,掺杂源有Sb、Sb2O3、Se、Te、In、In2O3、Se和In2O3的混合物.对各种掺杂SnS薄膜的厚度、电流-电压(I-V)特性等进行了表征,并计算了其电阻率和光电导与暗电导的比值(Gphoto/Gdark).结果表明较有效的掺杂源是Sb,Sb掺杂的薄膜电阻率比纯薄膜的电阻率降低四个数量级,Gphoto/Gdark增加约一倍.同时,研究了Sb掺杂量对SnS薄膜电学性能的影响,表明Sb的最佳掺入量约为1.3wt%～1.5wt%.","authors":[{"authorName":"郭余英","id":"0646b948-c0ad-467b-ae7a-d8813165a396","originalAuthorName":"郭余英"},{"authorName":"史伟民","id":"69d38ca6-57a1-4199-953f-9b72aca80412","originalAuthorName":"史伟民"},{"authorName":"魏光普","id":"2dd0a5d6-c325-4e67-816f-60b367abdba7","originalAuthorName":"魏光普"},{"authorName":"邱永华","id":"e3414774-69e8-4b8c-b72d-78a27537d14f","originalAuthorName":"邱永华"},{"authorName":"夏义本","id":"7d45a049-9db4-469e-b5c9-6a848b21df82","originalAuthorName":"夏义本"}],"doi":"10.3969/j.issn.1007-4252.2007.06.026","fpage":"651","id":"3d123a41-2493-483c-8b09-0810f886d55e","issue":"6","journal":{"abbrevTitle":"GNCLYQJXB","coverImgSrc":"journal/img/cover/GNCLYQJXB.jpg","id":"34","issnPpub":"1007-4252","publisherId":"GNCLYQJXB","title":"功能材料与器件学报 "},"keywords":[{"id":"b66e256f-0d9c-4f53-a845-2d03482330f8","keyword":"硫化锡","originalKeyword":"硫化锡"},{"id":"986fb101-9acc-4648-b8f3-87f3ffa1d0e7","keyword":"太阳电池","originalKeyword":"太阳电池"},{"id":"46e9f1d2-fbc6-4386-8f5b-81eb83cef845","keyword":"掺杂","originalKeyword":"掺杂"},{"id":"136ff642-27fd-4068-a7af-8157d82a8d93","keyword":"真空蒸发","originalKeyword":"真空蒸发"},{"id":"6963ad02-670d-4f2f-b319-4e68bb6c71de","keyword":"电阻率","originalKeyword":"电阻率"}],"language":"zh","publisherId":"gnclyqjxb200706026","title":"掺杂SnS薄膜的制备及电学性能","volume":"13","year":"2007"},{"abstractinfo":"采用电沉积法制备了CdS薄膜.分别用XRD及SEM分析了薄膜的结构和表面形貌.研究了不同温度和不同沉积电压对薄膜表面硫与镉的化学成分比的影响.最佳的沉积电压为2.5～3V之间.制作了ITO/n-CdS/p-SnS/Ag结构的太阳能电池,在100mW/cm2的光强下其开路电压0.2V,短路电流13.2mA/cm2,填充因子0.31,转换效率0.81%.","authors":[{"authorName":"葛艳辉","id":"cc8d4ed8-f082-4e26-8414-842143987874","originalAuthorName":"葛艳辉"},{"authorName":"史伟民","id":"48b22eae-d484-4666-bed7-c237765bb1ab","originalAuthorName":"史伟民"},{"authorName":"魏光普","id":"11838e85-c31f-4349-a193-4265d226b942","originalAuthorName":"魏光普"},{"authorName":"徐菁","id":"7fdf3e75-1ba4-484a-9f8f-7fbc8ca932b1","originalAuthorName":"徐菁"},{"authorName":"邱永华","id":"4d11b765-1407-440b-9794-015cf5b1f2d5","originalAuthorName":"邱永华"}],"doi":"10.3969/j.issn.1000-985X.2006.04.043","fpage":"867","id":"4d75f74e-e312-4206-8a9b-2c79d8c62997","issue":"4","journal":{"abbrevTitle":"RGJTXB","coverImgSrc":"journal/img/cover/RGJTXB.jpg","id":"57","issnPpub":"1000-985X","publisherId":"RGJTXB","title":"人工晶体学报"},"keywords":[{"id":"5d178a3b-0d52-4014-a7db-28c888ac8835","keyword":"CdS","originalKeyword":"CdS"},{"id":"98d1f6b3-6306-4d96-96c1-6cb69b6284ea","keyword":"电沉积","originalKeyword":"电沉积"},{"id":"c40e2066-ce96-4f16-8710-a303451afa04","keyword":"太阳能电池","originalKeyword":"太阳能电池"}],"language":"zh","publisherId":"rgjtxb98200604043","title":"电沉积法制备CdS薄膜及其性能研究","volume":"35","year":"2006"},{"abstractinfo":"采用真空蒸发法在玻璃衬底上沉积硫化亚锡(SnS)薄膜,并对不同衬底温度沉积的薄膜性能进行了探讨.对薄膜的结构、表面形貌、成份、电学特性和光学特性进行了表征.实验发现,最佳的衬底温度为150℃;制备的SnS薄膜为多晶的斜方晶系,晶粒大小约为0.5 μm,Sn和S元素的化学计量比接近1,导电类型为P型,暗电导率、光电导率分别为 0.01 Ω-1·cm-1 和 0.08Ω-1·cm-1,禁带宽度为1.402 eV.","authors":[{"authorName":"郭余英","id":"09d7d073-a5bc-42e8-8b4d-b8f31f652fed","originalAuthorName":"郭余英"},{"authorName":"史伟民","id":"82992b4d-4efc-4de4-8016-0b3f105347c4","originalAuthorName":"史伟民"},{"authorName":"魏光普","id":"fb296a26-f71c-4c01-a6d4-c5c8f5c0c745","originalAuthorName":"魏光普"},{"authorName":"夏义本","id":"943dc2c9-24b1-489c-9ee9-200c6f6a55b1","originalAuthorName":"夏义本"}],"doi":"","fpage":"666","id":"53de8247-7c46-4ba2-8408-d2e6f86423e0","issue":"3","journal":{"abbrevTitle":"RGJTXB","coverImgSrc":"journal/img/cover/RGJTXB.jpg","id":"57","issnPpub":"1000-985X","publisherId":"RGJTXB","title":"人工晶体学报"},"keywords":[{"id":"a971dbdd-e3a7-46a4-8eb8-aeb9da99c6f9","keyword":"太阳能电池","originalKeyword":"太阳能电池"},{"id":"2565e082-504d-4338-adfe-f999978a222f","keyword":"硫化亚锡薄膜","originalKeyword":"硫化亚锡薄膜"},{"id":"3c9c3982-c2ef-4c14-9697-3a39c473d4a1","keyword":"真空蒸发","originalKeyword":"真空蒸发"},{"id":"e20fddc1-d52c-4d46-a911-c29cccc9f13a","keyword":"衬底温度","originalKeyword":"衬底温度"}],"language":"zh","publisherId":"rgjtxb98200803033","title":"衬底温度对SnS薄膜性能的影响","volume":"37","year":"2008"},{"abstractinfo":"普光气田净化厂胺液(MDEA溶液)系统大量采用了316L不锈钢材料,设计之初预计集输流程会分离所有氯离子,但实际使用过程中,发现胺液中的氯离子含量逐渐升高,最高达到8 000 μg/g.为评估普光气田胺液系统中316L不锈钢的使用安全性,通过模拟工况应力腐蚀试验研究了316L不锈钢在含氯胺液中的应力腐蚀开裂行为.结果表明:胺液具有很好的保护性能,316L钢在高含硫含氯胺液环境中具有很好的韧性,未发生应力腐蚀开裂.研究认为,胺液中的特殊环境,使得具有毒化功能的硫离子被络合,从而避免了发生硫化物应力腐蚀开裂的可能性.而胺液的碱性环境,也使得发生氯化物应力腐蚀开裂的门槛值显著上升.","authors":[{"authorName":"张诚","id":"05c0350e-cecb-4aec-a170-d3d829f16eb6","originalAuthorName":"张诚"}],"doi":"10.11973/fsyfh-201611009","fpage":"900","id":"10b1edc7-1f59-483c-a209-0f16cacdf11e","issue":"11","journal":{"abbrevTitle":"FSYFH","coverImgSrc":"journal/img/cover/FSYFH.jpg","id":"25","issnPpub":"1005-748X","publisherId":"FSYFH","title":"腐蚀与防护"},"keywords":[{"id":"d2e2f9a0-3e0a-4b03-9676-6e7b30953cee","keyword":"奥氏体不锈钢","originalKeyword":"奥氏体不锈钢"},{"id":"6bc2901f-85c3-4641-8f28-705de476eeb4","keyword":"胺液","originalKeyword":"胺液"},{"id":"f0a88620-6609-4733-b704-06a763df4433","keyword":"高含硫气田","originalKeyword":"高含硫气田"},{"id":"456dc8cd-8dd1-43d1-aa17-3fa1608a6d4d","keyword":"应力腐蚀开裂","originalKeyword":"应力腐蚀开裂"},{"id":"ab4ebaef-0b33-43f2-94d2-b96b559d4eb6","keyword":"氯离子","originalKeyword":"氯离子"}],"language":"zh","publisherId":"fsyfh201611009","title":"316L不锈钢在普光净化厂含氯胺液中的应力腐蚀开裂","volume":"37","year":"2016"},{"abstractinfo":"研究了45Mn2钢魏氏组织对其力学性能的影响.结果表明,一定量的魏氏组织有利于提高其强韧性.","authors":[{"authorName":"钟长文","id":"62a16d0c-647d-4cd1-95c5-e9a0024bb029","originalAuthorName":"钟长文"},{"authorName":"刘建华","id":"65af211a-2b3a-4d98-bb14-ae0cd3fbf4d5","originalAuthorName":"刘建华"}],"doi":"10.3969/j.issn.1001-0777.2002.03.001","fpage":"1","id":"18b0cbfb-b0d9-411b-a60d-94b38294e6bf","issue":"3","journal":{"abbrevTitle":"WLCS","coverImgSrc":"journal/img/cover/WLCS.jpg","id":"64","issnPpub":"1001-0777","publisherId":"WLCS","title":"物理测试"},"keywords":[{"id":"afb278f0-6870-4db2-995e-06fbac281ece","keyword":"45Mn2钢","originalKeyword":"45Mn2钢"},{"id":"89737183-39e7-4780-b887-349bf67b57c8","keyword":"魏氏组织","originalKeyword":"魏氏组织"},{"id":"f2acd931-7e20-4358-a158-e22dadf7929c","keyword":"力学性能","originalKeyword":"力学性能"}],"language":"zh","publisherId":"wlcs200203001","title":"45Mn2钢魏氏组织对其力学性能的影响","volume":"","year":"2002"},{"abstractinfo":"用扫描隧道显微镜（STM）观察了Fe-0．37C（质量分数，％）合金中魏氏组织铁素体的表面浮突，发现其浮突形状为帐篷型和复杂形态.切变机制不能解释魏氏组织表面浮突的形成过程，而扩散控制的台阶机制可合理地解释.魏氏组织的浮突高度为70—450nm，最大形状变形约0．36.","authors":[{"authorName":"薄祥正","id":"beaa42e9-dc0e-42f9-8a34-38fef2f47bc0","originalAuthorName":"薄祥正"},{"authorName":"方鸿生","id":"16034f00-e8d6-4d86-9f9e-b9c1b34d148b","originalAuthorName":"方鸿生"},{"authorName":"王家军","id":"1aaa85d3-c77a-402b-adc8-ea11a9f782eb","originalAuthorName":"王家军"},{"authorName":"王峥华","id":"83fd7fe5-0e2f-4c92-b887-907e3b37c8e2","originalAuthorName":"王峥华"}],"categoryName":"|","doi":"","fpage":"345","id":"17606cac-47f6-4a25-bb8b-33ab41ad3402","issue":"4","journal":{"abbrevTitle":"JSXB","coverImgSrc":"journal/img/cover/JSXB.jpg","id":"48","issnPpub":"0412-1961","publisherId":"JSXB","title":"金属学报"},"keywords":[{"id":"333be36e-8063-45f3-88ec-d320451b4720","keyword":"表面浮凸","originalKeyword":"表面浮凸"},{"id":"1a353ff0-f6bd-4c79-80c9-cd059e832cde","keyword":" Widmanstatten ferrite","originalKeyword":" Widmanstatten ferrite"},{"id":"1ae96154-0cf9-4d1e-8212-bff6ee843aa8","keyword":" scanning tunneling microscopy","originalKeyword":" scanning tunneling microscopy"},{"id":"05b95277-919a-400c-9769-09973ad81bbf","keyword":" shapede formation","originalKeyword":" shapede formation"}],"language":"zh","publisherId":"0412-1961_1998_4_6","title":"魏氏组织表面浮突的扫描隧道显微镜研究","volume":"34","year":"1998"},{"abstractinfo":"本文合成了萘普生稀土(Ce、Gd)配合物,测定了配合物配位数并依据徐光宪关于水溶液中配合物的吸附平衡理论求得逐级稳定常数βi.","authors":[{"authorName":"陈朝军","id":"b3ac9ac2-9396-4547-b6a6-4f8b7d7f68bf","originalAuthorName":"陈朝军"},{"authorName":"李俊恒","id":"c00b6c24-5445-40fd-b261-aeb6bc7473d9","originalAuthorName":"李俊恒"},{"authorName":"杨秉呼","id":"ff593a6c-fa76-4703-96c4-f33e279c1666","originalAuthorName":"杨秉呼"},{"authorName":"蒋绥萍","id":"9bec6ecd-133c-4762-8fb0-157f4dd54455","originalAuthorName":"蒋绥萍"},{"authorName":"赵国丁","id":"13c4a8e0-4c6c-4423-8c1d-dd0adc0fa74c","originalAuthorName":"赵国丁"}],"doi":"10.3969/j.issn.1004-0277.2001.05.020","fpage":"70","id":"26e0f20c-2232-4bd1-8cf3-c27ae8fe3c98","issue":"5","journal":{"abbrevTitle":"XT","coverImgSrc":"journal/img/cover/XT.jpg","id":"65","issnPpub":"1004-0277","publisherId":"XT","title":"稀土"},"keywords":[{"id":"3f1b54fa-625e-4a86-9ca5-d0c703becffd","keyword":"萘普生","originalKeyword":"萘普生"},{"id":"44589709-2a44-4f61-b7e9-5a38dd9e7df1","keyword":"铈","originalKeyword":"铈"},{"id":"ba0e6b04-7fb3-4ab2-b6e0-71f7bcc4b9aa","keyword":"钆","originalKeyword":"钆"},{"id":"8487ee14-320a-4afd-9ebf-0678599f1d16","keyword":"稳定性","originalKeyword":"稳定性"}],"language":"zh","publisherId":"xitu200105020","title":"萘普生稀土(Ce、Gd)配合物的合成及稳定性研究","volume":"22","year":"2001"},{"abstractinfo":"<正> 一般认为亚共析钢中魏氏组织降低机械性能,尤其是不利于冲击韧性。近年来研究结果则认为魏氏组织可以提高机械性能,也有人认为具有魏氏组织的亚共析钢,由于冷却速度快,增加了珠光体量,细化了铁素体晶粒,从而抵销了针状铁素体的不良影响。另一些人指出切变机制使针状铁素体中有较高密度的位错和较细的亚结构,提高了钢的机械性能。本文根据对裂纹扩展行为的观察,探讨铁素体影响钢的机械性能的原因。 本实验采用25铸钢作试样,其化学成分(wt-％)为:C 0.28,Si 0.37,Mn 0.61,S","authors":[{"authorName":"刘继恒","id":"c3179369-e2c8-4945-954a-577a2237d0b3","originalAuthorName":"刘继恒"},{"authorName":"赵明","id":"de9e536d-6d85-4db6-b708-3f9966be2b8b","originalAuthorName":"赵明"},{"authorName":"钱得荣","id":"e4a6f421-07f1-4fc6-8a38-4e7a34adc788","originalAuthorName":"钱得荣"},{"authorName":"阎胡成","id":"0e99f566-f6e0-4749-bcdf-6af4454a71e9","originalAuthorName":"阎胡成"}],"categoryName":"|","doi":"","fpage":"92","id":"0222ca2e-fa27-4ae4-8bda-fea34ba27e9c","issue":"5","journal":{"abbrevTitle":"JSXB","coverImgSrc":"journal/img/cover/JSXB.jpg","id":"48","issnPpub":"0412-1961","publisherId":"JSXB","title":"金属学报"},"keywords":[],"language":"zh","publisherId":"0412-1961_1986_5_5","title":"魏氏组织铁素体的亚结构及其对裂纹扩展的影响","volume":"22","year":"1986"},{"abstractinfo":"以提高魏氏体组织Ti60合金的拉伸强度与塑性为目标,研究固溶与时效处理对Ti60合金组织与性能演变的影响规律,并优化热处理参数.结果表明,初始魏氏组织晶粒较为粗大,经过固溶与时效处理后,晶粒明显减小,层片状α相明显减少.初始魏氏组织Ti60合金抗拉强度为850 MPa,伸长率为0.9％,1000℃固溶处理后,Ti60合金的抗拉强度达到1100 MPa,伸长率为3.7％.1000℃固溶+600℃8h时效处理后,抗拉强度达到1200 MPa,伸长率为3.3％.随固溶温度提高,其硬度与抗拉强度增加,伸长率降低.随时效时间延长,硬度先增大后减小.经1050℃固溶+600℃8 h时效处理后Ti60合金具有最大硬度值509 HV.","authors":[{"authorName":"戎旭东","id":"00e2c6cf-8ebd-4236-bb60-c083bcd4eb99","originalAuthorName":"戎旭东"},{"authorName":"黄陆军","id":"794ed4ef-eed8-4475-b58e-a300cf622c81","originalAuthorName":"黄陆军"},{"authorName":"王博","id":"7040e675-9c80-483b-af2f-2cb4474fc96e","originalAuthorName":"王博"},{"authorName":"唐骜","id":"6d8ec4ba-b4c6-41d1-b85b-b76b9864123e","originalAuthorName":"唐骜"},{"authorName":"耿林","id":"b9f5abbc-1007-4ee0-9971-8866850ef17c","originalAuthorName":"耿林"}],"doi":"","fpage":"39","id":"b48c7721-ea64-499f-a5fe-b3aac071a8f2","issue":"10","journal":{"abbrevTitle":"CLRCLXB","coverImgSrc":"journal/img/cover/CLRCLXB.jpg","id":"15","issnPpub":"1009-6264","publisherId":"CLRCLXB","title":"材料热处理学报"},"keywords":[{"id":"64128791-9e51-4d68-abb3-3c2c66d73ea4","keyword":"Ti60合金","originalKeyword":"Ti60合金"},{"id":"772dbb5f-8b5d-4de4-be64-5bc34e5d0365","keyword":"热处理","originalKeyword":"热处理"},{"id":"32e68aef-3437-4179-b2cc-2cf021e87867","keyword":"魏氏体组织","originalKeyword":"魏氏体组织"},{"id":"d0ce6237-e6e6-485d-bee5-9d03e6161a24","keyword":"拉伸性能","originalKeyword":"拉伸性能"}],"language":"zh","publisherId":"jsrclxb201510007","title":"热处理对魏氏组织Ti60合金组织与性能的影响","volume":"36","year":"2015"},{"abstractinfo":"以三种低碳合金钢的粗大魏氏组织为原始组织,分别以慢速、中速进行奥氏体化加热.晶粒度测试表明:慢速加热条件下出现组织遗传现象,中速加热时可细化晶粒.慢速加热奥氏体化过程中,观察到球状奥氏体和针状奥氏体.","authors":[{"authorName":"李智超","id":"e73b2b47-9e17-4dfd-814f-921ac81a4441","originalAuthorName":"李智超"},{"authorName":"马栓柱","id":"8fbbbb83-2208-4b2b-98ca-78e6a7444927","originalAuthorName":"马栓柱"},{"authorName":"杜素梅","id":"8716631a-5b5e-4bc5-9268-4301ce0b1092","originalAuthorName":"杜素梅"}],"doi":"10.3969/j.issn.1004-244X.2004.02.004","fpage":"12","id":"44de1e41-6719-4ef5-9b29-2e4baa38f234","issue":"2","journal":{"abbrevTitle":"BQCLKXYGC","coverImgSrc":"journal/img/cover/BQCLKXYGC.jpg","id":"4","issnPpub":"1004-244X","publisherId":"BQCLKXYGC","title":"兵器材料科学与工程 "},"keywords":[{"id":"caeb73e3-44fc-4e74-9e2e-eb59a9634085","keyword":"魏氏组织","originalKeyword":"魏氏组织"},{"id":"194384c6-f80f-4ba3-8dc6-c16746fda416","keyword":"组织遗传现象","originalKeyword":"组织遗传现象"},{"id":"68430359-742b-4a37-8a9c-2f98068df413","keyword":"针状奥氏体","originalKeyword":"针状奥氏体"}],"language":"zh","publisherId":"bqclkxygc200402004","title":"亚共析钢魏氏组织的组织遗传现象研究","volume":"27","year":"2004"}],"totalpage":731,"totalrecord":7303}