采用真空快淬技术制备低Nd含量的NdFeB纳米复合磁性材料,通过差示扫描量热法(DSC)、X射线衍射(XRD)、振动样品磁强计(VSM)和微波矢量网络分析仪等手段研究了真空热处理前后样品微观结构和电磁特性的变化.DSC结果显示在510℃和630℃处出现两个放热峰,在稍微高于这两个温度分别热处理后,相对于快淬态样品,材料的磁导率(μ′)和磁损耗(μ″)降低,并且磁损耗出现多重频散特性,同时复介电常数减小,特别在2 GHz处ε″分别为-103.7(540℃)和ε″为-245.3(650℃).根据传输线理论模拟计算涂层的反射损耗,发现快淬态样品在3.7 GHz下厚度为1.5 mm时最小反射损耗为-5.3dB;而热处理后的样品在12 GHz处获得最小反射损耗,分别为-3.3dB(540℃)和-2.1dB(650℃).
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