We have succeeded in studying the structural characteristics of a single thread of Bi-based 2212-phase whisker by X-ray diffraction. It is found that the structural characteristics of a single thread of whisker coincide with those of a 2212-phase single crystal. The single thread of whisker is a 2212 plate-like single crystal and is stacked in a layered structure. There are a number of low-angle boundaries in the BC-plane, but few in the AB-plane of the whisker.
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