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为了降低氮化硅材料的成本,运用便宜的低纯度从β-Si3N4粉末,通过无压烧结制备了氮化硅材料.发现β-Si3N4粉末具有很好的烧结性能,得到的结构是由柱状颗粒和小球状颗粒形成的嵌套结构,结构组成均匀,没有晶粒的异常生长.所得材料的抗弯强度为587MPa,韧性达到5.3MPa.m1/2,说明可在一般条件下使用。

Refractory grade β-St3N4 powder was pressureless sintered with the aim of lowering cost. It is showed that β-St3N4 has good sinterability. A microstructure with small rod-like grains was obtained, which dispersed uniformly in the matrix, no abnormal rod-like grains was observed. The material displayed a strength of 587MPa and fracture toughness of 5.3MPa.m1/2, which allow the material used in normal circumstance.

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