{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":5,"startPagecode":1},"records":[{"abstractinfo":"采用电化学法,合成出含双键聚硅烷与不含双键聚硅烷,通过FT-IR,UV,1H NMR表征其结构.分别研究了电化学反应体系和直接化学反应体系中Si-Cl键含量的变化,以及加入引发剂蒽对反应速率的影响.结果表明:含双键聚硅烷的合成反应速率快于不含双键的聚硅烷,相同反应电量下含双键聚硅烷反应体系中的Si-Cl键含量比不含双键聚硅烷少10%～15%;在电化学合成聚硅烷的过程中,单体与镁发生的格氏反应在整个反应中占有相当的比例;引发剂蒽的加入能够有效地提高不含双键聚硅烷的反应速率.本文还对电化学合成聚硅烷的反应机理进行了推测.","authors":[{"authorName":"吴市","id":"1225249b-930b-4870-978f-547771c12ebe","originalAuthorName":"吴市"},{"authorName":"张<span style=\"color:red\">峰</span>君","id":"1468a1f8-3fee-4776-b468-3e964c01d5f2","originalAuthorName":"张峰君"},{"authorName":"钱林","id":"319dae88-df01-4e78-b26a-440b494f7982","originalAuthorName":"钱林"},{"authorName":"陈来","id":"515078b9-4fed-4c96-81a2-ef48b1c426aa","originalAuthorName":"陈来"},{"authorName":"张家宝","id":"9d42fdd3-ea67-4419-8147-0b88c2634fd2","originalAuthorName":"张家宝"},{"authorName":"<span style=\"color:red\">潘</span><span style=\"color:red\">健</span><span style=\"color:red\">峰</span>","id":"faa506e0-164d-4324-b4aa-73ff23158a2c","originalAuthorName":"潘健峰"},{"authorName":"周春节","id":"fe9d1a67-c0da-40dc-8d20-144360cd9625","originalAuthorName":"周春节"},{"authorName":"任慕苏","id":"987b24b9-cf01-4232-bc60-2272d6c2ce8a","originalAuthorName":"任慕苏"},{"authorName":"孙晋良","id":"b4716f12-bd07-4b96-8c4f-fe558c40c245","originalAuthorName":"孙晋良"}],"doi":"","fpage":"273","id":"ff1e167d-a970-402a-a44d-da5ccb81722f","issue":"2","journal":{"abbrevTitle":"CLKXYGCXB","coverImgSrc":"journal/img/cover/CLKXYGCXB.jpg","id":"13","issnPpub":"1673-2812","publisherId":"CLKXYGCXB","title":"材料科学与工程学报"},"keywords":[{"id":"3dbd2da1-a945-438d-8c78-b506582f6e91","keyword":"聚硅烷","originalKeyword":"聚硅烷"},{"id":"29ad9f88-d680-4297-9e2b-a0100c12f05a","keyword":"电化学合成","originalKeyword":"电化学合成"},{"id":"8f442028-b3c3-4875-8547-062e024294bc","keyword":"反应速率","originalKeyword":"反应速率"}],"language":"zh","publisherId":"clkxygc200802029","title":"电化学合成聚硅烷的反应速率","volume":"26","year":"2008"},{"abstractinfo":"基于构造逐级控制理论,以江苏泗洪县褶皱区的区域地质为背景,运用地质构造解析和物化探等手段研究矿区构造.结果表明,区域构造控制矿区构造,矿区构造反映区域构造.宿迁市泗洪县<span style=\"color:red\">潘</span>赵庄铜镍矿区处于构造有利区,岩石化学特征对形成铜镍硫化物矿床较为有利,具备铜镍硫化物矿床的找矿前提,确定有利靶区受构造控制作用明显,存在于岩体中下部熔离型矿体及岩体边贯入式矿体两处.","authors":[{"authorName":"罗跃","id":"744127b8-7fa6-4807-96bc-8226affe3bff","originalAuthorName":"罗跃"},{"authorName":"周贤金","id":"074c8c12-ab87-4459-9d53-f08320a80ca8","originalAuthorName":"周贤金"},{"authorName":"施建斌","id":"e7efc5f3-3467-429c-a26b-986b5b37f807","originalAuthorName":"施建斌"},{"authorName":"冯学知","id":"c4d96ab0-cf41-4f0a-aea3-6042ba5a1bdf","originalAuthorName":"冯学知"},{"authorName":"刘正疆","id":"6b5ad79e-3d4c-4e3f-b65a-78778d2f5430","originalAuthorName":"刘正疆"},{"authorName":"张琪","id":"69cc55d7-64c9-4bcb-8cad-a9d676dd0962","originalAuthorName":"张琪"}],"doi":"10.3969/j.issn.2095-1744.2013.06.010","fpage":"48","id":"139b4e79-0f29-4c56-ac61-41753022d73d","issue":"6","journal":{"abbrevTitle":"YSJSGC","coverImgSrc":"journal/img/cover/YSJSGC.jpg","id":"76","issnPpub":"2095-1744","publisherId":"YSJSGC","title":"有色金属工程"},"keywords":[{"id":"c20e5d56-689a-40aa-9a63-796dac006db7","keyword":"铜-镍硫化矿","originalKeyword":"铜-镍硫化矿"},{"id":"5a907ae9-825e-4737-a764-797201503314","keyword":"构造逐级控制","originalKeyword":"构造逐级控制"},{"id":"c138a0de-cc7e-440c-8177-b76cf229ee27","keyword":"构造指示矿","originalKeyword":"构造指示矿"},{"id":"36755356-60f4-4d84-90e5-ab2910d6c12a","keyword":"靶区","originalKeyword":"靶区"},{"id":"44cad5bd-df83-4450-97f6-9b6e490ab7c9","keyword":"泗洪县","originalKeyword":"泗洪县"}],"language":"zh","publisherId":"ysjs201306015","title":"<span style=\"color:red\">潘</span>赵庄铜镍矿区构造逐级控制及构造指示矿特征探讨","volume":"3","year":"2013"},{"abstractinfo":"试样于<span style=\"color:red\">潘</span>菲氏管中加入还原铁粉,加热使汞与基体及共存元素分离;试验了氢化物-原子荧光光谱法测定汞的最佳条件.汞的检出限为0.05ng/mL,线性范围为0.5～250ng/mL,汞的回收率为94%～101%.方法应用于锌精矿中汞的测定,取得满意结果.","authors":[{"authorName":"钟勇","id":"28126a39-4461-43d5-85c3-fe3a51b87f74","originalAuthorName":"钟勇"}],"doi":"10.3969/j.issn.1000-7571.2002.01.012","fpage":"38","id":"d43ad448-87f6-4c0c-9651-93da5de3aadf","issue":"1","journal":{"abbrevTitle":"YJFX","coverImgSrc":"journal/img/cover/YJFX.jpg","id":"71","issnPpub":"1000-7571","publisherId":"YJFX","title":"冶金分析   "},"keywords":[{"id":"a2e8e9c0-5aab-4736-9937-982056210857","keyword":"<span style=\"color:red\">潘</span>菲氏管","originalKeyword":"潘菲氏管"},{"id":"c3888355-ef2a-44c7-91ef-2b4d70031e81","keyword":"氢化物","originalKeyword":"氢化物"},{"id":"805c6bb7-c5dc-489d-9e0c-37dc385c05f8","keyword":"冷原子荧光光谱法","originalKeyword":"冷原子荧光光谱法"},{"id":"e2805568-4e3c-4b8f-bf78-31f522e2f76d","keyword":"锌精矿","originalKeyword":"锌精矿"},{"id":"536aae8f-f0d4-4aff-a0b7-256b6e58239f","keyword":"汞","originalKeyword":"汞"}],"language":"zh","publisherId":"yjfx200201012","title":"<span style=\"color:red\">潘</span>菲氏管分离氢化物-冷原子荧光光谱法测定锌精矿中微量汞","volume":"22","year":"2002"},{"abstractinfo":"用受迫振动法测量了夹角为60°和129.5°的铝双晶的内耗,都观测到一个温度内耗<span style=\"color:red\">峰</span>,峰巅温度是200℃左右(频率1Hz)激活能为0.88eV对于这个内耗<span style=\"color:red\">峰</span>的机制做了初步解释。","authors":[{"authorName":"关幸生","id":"8e7fa0a7-4b2b-43eb-ab0e-385b95cbfd10","originalAuthorName":"关幸生"},{"authorName":"葛庭燧","id":"67b972cc-f4c0-4797-9aed-85c45cb1ce80","originalAuthorName":"葛庭燧"}],"categoryName":"|","doi":"","fpage":"1","id":"2aff307d-21f5-4a68-a5ac-0b1cd08864dc","issue":"8","journal":{"abbrevTitle":"JSXB","coverImgSrc":"journal/img/cover/JSXB.jpg","id":"48","issnPpub":"0412-1961","publisherId":"JSXB","title":"金属学报"},"keywords":[{"id":"ed61f5ab-f338-42d9-b668-0b6a379c39fe","keyword":"铝双晶","originalKeyword":"铝双晶"},{"id":"36aafee6-63d2-4133-8924-6e4a2ec321a9","keyword":"grain boundary internal friction peak","originalKeyword":"grain boundary internal friction peak"},{"id":"10d06012-bca3-4f68-aa60-0d4f370bb37a","keyword":"activation enegry","originalKeyword":"activation enegry"}],"language":"zh","publisherId":"0412-1961_1993_8_5","title":"铝双晶晶界的内耗<span style=\"color:red\">峰</span>","volume":"29","year":"1993"},{"abstractinfo":"采用不完全相变内耗(IF)测量法, 在Cu-Al-Ni-Mn-Ti合金马氏体相变中获得双内耗<span style=\"color:red\">峰</span>, 即低温内耗<span style=\"color:red\">峰</span>和高温内耗<span style=\"color:red\">峰</span>. 高温内耗<span style=\"color:red\">峰</span>主要出现在频率小于0.050 Hz的范围, 其位置对应于相对动力学模量的拐点位置; 高温内耗峰峰值在测量频率范围内与振动频率成反比关系, 满足经典的Belko和Delorme模型; 高温内耗<span style=\"color:red\">峰</span>具有明显的反常应变振幅效应, 其峰值随变温速率的增大而增大, 这些都说明高温内耗<span style=\"color:red\">峰</span>的形成与相转变量有关.","authors":[{"authorName":"戴鹏","id":"a2f5e766-4187-4d3e-840f-f8a7ab3aabb2","originalAuthorName":"戴鹏"},{"authorName":"吴明在","id":"ce4a423d-0344-437f-b781-e30753e4e0bf","originalAuthorName":"吴明在"},{"authorName":"宫晨利","id":"1a5ce7ae-c4a3-47f5-bc05-322499b45b99","originalAuthorName":"宫晨利"}],"doi":"10.3969/j.issn.0258-7076.2009.06.006","fpage":"795","id":"b04ec2cc-59d3-401d-a6cb-cc56b054c880","issue":"6","journal":{"abbrevTitle":"XYJS","coverImgSrc":"journal/img/cover/XYJS.jpg","id":"67","issnPpub":"0258-7076","publisherId":"XYJS","title":"稀有金属"},"keywords":[{"id":"e18e678d-f0ca-4f50-a148-2b6eb16937d9","keyword":"热弹性马氏体","originalKeyword":"热弹性马氏体"},{"id":"6757b8da-6539-4a04-8b55-003e8e583328","keyword":"内耗","originalKeyword":"内耗"},{"id":"c2ef60e4-a840-4557-a094-76bec2c54d9f","keyword":"高温内耗<span style=\"color:red\">峰</span>","originalKeyword":"高温内耗峰"}],"language":"zh","publisherId":"xyjs200906006","title":"热弹性马氏体相变中的高温内耗<span style=\"color:red\">峰</span>","volume":"33","year":"2009"},{"abstractinfo":"本文对Ag掺杂熔融织构YBCO材料的<span style=\"color:red\">峰</span>效应进行了研究.磁测量结果表明,Ag掺杂不会影响<span style=\"color:red\">峰</span>效应的产生,但能显著改变<span style=\"color:red\">峰</span>效应对温度和磁场的依赖关系;<span style=\"color:red\">峰</span>效应出现的磁场随Ag掺杂量的增加而增高,且适量的Ag掺杂使得高温下仍能出现<span style=\"color:red\">峰</span>效应.该研究表明,Ag掺杂可以作为显著提高熔融织构YBCO材料磁场下临界电流密度的有效手段,从而可使其在高场下的性能得以显著改善.","authors":[{"authorName":"刘果红","id":"9a9e4fa1-0a54-4b10-8099-33ccada5f513","originalAuthorName":"刘果红"},{"authorName":"张莉","id":"65a290ff-7014-48ec-9d8c-e509f7001040","originalAuthorName":"张莉"},{"authorName":"丁世英","id":"9528706b-a748-41ab-8fe3-c08bdb564e3e","originalAuthorName":"丁世英"},{"authorName":"肖玲","id":"3bcd2ad1-b750-4edb-a7dd-5796c7c65038","originalAuthorName":"肖玲"}],"doi":"","fpage":"199","id":"4c9e6752-ea68-4277-9a88-1c453adebe5e","issue":"3","journal":{"abbrevTitle":"DWWLXB","coverImgSrc":"journal/img/cover/DWWLXB.jpg","id":"19","issnPpub":"1000-3258","publisherId":"DWWLXB","title":"低温物理学报   "},"keywords":[{"id":"8c259a45-73a5-4917-8a9d-e8c83fefe7e2","keyword":"YBCO熔融织构","originalKeyword":"YBCO熔融织构"},{"id":"fa6b6936-e9dd-498b-8a59-165540cfc21d","keyword":"Ag掺杂","originalKeyword":"Ag掺杂"},{"id":"abc275b3-7cfe-4c3a-90cb-6938f96d2ca4","keyword":"<span style=\"color:red\">峰</span>效应","originalKeyword":"峰效应"}],"language":"zh","publisherId":"dwwlxb201003010","title":"Ag掺杂熔融织构YBCO<span style=\"color:red\">峰</span>效应研究","volume":"32","year":"2010"},{"abstractinfo":"给出了Voigt函数的一种计算方法,同时给出了一种用Voigt<span style=\"color:red\">峰</span>形函数拟合由Kα1、Kα2引起的晶体X射线双峰衍射谱的一种算法,此算法可同时对多个衍射双峰进行拟合和分<span style=\"color:red\">峰</span>,从而给出较准确的衍射<span style=\"color:red\">峰</span>宽度,用于计算晶体颗粒尺寸和应力等.用此算法计算了纳米GSGG的颗粒度,结果表明:在低角度,双峰叠加对衍射<span style=\"color:red\">峰</span>的半高全宽的影响可忽略,而在高角度双峰的衍射间隔加宽,使计算获得的粒度明显偏小.","authors":[{"authorName":"张庆礼","id":"26dc05bd-4b60-4c24-8770-0cfd3a7fb71a","originalAuthorName":"张庆礼"},{"authorName":"丁丽华","id":"a514450b-3a4a-48b1-83d7-ccdc38437501","originalAuthorName":"丁丽华"},{"authorName":"邵淑芳","id":"f0c78c3a-5f4d-42bb-88f3-9db6e0caeeaf","originalAuthorName":"邵淑芳"},{"authorName":"刘文鹏","id":"0f7439f4-10ff-426a-a746-875dd158cc68","originalAuthorName":"刘文鹏"},{"authorName":"王晓梅","id":"4ac916b3-d9b1-4dbc-a498-ef85dc0f49bf","originalAuthorName":"王晓梅"},{"authorName":"孙敦陆","id":"081ec13e-4bc3-4b81-becd-20920141c2f8","originalAuthorName":"孙敦陆"},{"authorName":"殷绍唐","id":"5afc1187-154c-4c5e-8c47-c62e8b0221f9","originalAuthorName":"殷绍唐"}],"doi":"","fpage":"330","id":"55263ffa-c0f9-49f7-aa52-a891cc7d224d","issue":"2","journal":{"abbrevTitle":"RGJTXB","coverImgSrc":"journal/img/cover/RGJTXB.jpg","id":"57","issnPpub":"1000-985X","publisherId":"RGJTXB","title":"人工晶体学报"},"keywords":[{"id":"bb325c51-72ba-4728-8db0-0dd5f3730664","keyword":"Voigt函数","originalKeyword":"Voigt函数"},{"id":"41a58dd8-2d1a-4b91-9600-f92e60fa5dbd","keyword":"X射线衍射","originalKeyword":"X射线衍射"},{"id":"a88d7670-a37f-496b-aafe-b2bf9d4ca8c8","keyword":"<span style=\"color:red\">峰</span>形函数","originalKeyword":"峰形函数"},{"id":"61ab48c8-7747-432b-b0bd-a276acff77a4","keyword":"GSGG","originalKeyword":"GSGG"}],"language":"zh","publisherId":"rgjtxb98200902010","title":"X射线衍射双峰的Voigt<span style=\"color:red\">峰</span>形函数拟合","volume":"38","year":"2009"},{"abstractinfo":"为了准确描述酚醛树脂热解时相互重叠的反应过程,进行了5种线性升温速率下的酚醛树脂热分析试验,提出一种高斯分<span style=\"color:red\">峰</span>方法.该方法通过分析酚醛树脂的微分热重(DTG)曲线以及不同温度下热分解产物的种类和含量,将酚醛树脂热解划分为四个反应过程.分<span style=\"color:red\">峰</span>结果与试验结果吻合较好,对后续准确求解酚醛树脂各个反应过程热分解动力学参数有重要意义.","authors":[{"authorName":"周启超","id":"1e3eac01-8bea-4d3d-b696-9fd0e0d288dc","originalAuthorName":"周启超"},{"authorName":"杨红亮","id":"9b50ffbe-b7a5-4d9a-b905-ed3a469b4296","originalAuthorName":"杨红亮"},{"authorName":"季妮芝","id":"32ecc8b5-96be-48b0-b09a-0192e7c298bc","originalAuthorName":"季妮芝"},{"authorName":"陈伟华","id":"69af5197-94f3-4822-9659-4feb62677746","originalAuthorName":"陈伟华"}],"doi":"10.3969/j.issn.1007-2330.2015.03.003","fpage":"11","id":"4a254c9c-db2f-4142-832b-19b9e8950f07","issue":"3","journal":{"abbrevTitle":"YHCLGY","coverImgSrc":"journal/img/cover/YHCLGY.jpg","id":"77","issnPpub":"1007-2330","publisherId":"YHCLGY","title":"宇航材料工艺   "},"keywords":[{"id":"f0486c8d-6cfa-4ea5-b65a-f01ba321ac27","keyword":"高斯分<span style=\"color:red\">峰</span>","originalKeyword":"高斯分峰"},{"id":"d345aa44-fc4c-40c8-a457-dff20877501a","keyword":"热解气体","originalKeyword":"热解气体"},{"id":"51cafb5e-a7d3-4ad1-a4f9-f1f007bb70bc","keyword":"反应方程","originalKeyword":"反应方程"},{"id":"2212d30b-d8e9-47ff-8fdf-d1aae5c78dd2","keyword":"酚醛树脂","originalKeyword":"酚醛树脂"},{"id":"020b00bb-720f-47a7-84a2-c3003b24d1c2","keyword":"热分解","originalKeyword":"热分解"}],"language":"zh","publisherId":"yhclgy201503003","title":"酚醛树脂热解高斯分<span style=\"color:red\">峰</span>法","volume":"45","year":"2015"},{"abstractinfo":"用声频内耗方法研究了Fe—0.5C,Fe—0.5Ti 和Fe—0.5C—0.5Ti 合金中的氢致冷加工内耗<span style=\"color:red\">峰</span>(H—CWP)。确定了不同合金中H—CWP 的特征及其激活能以及氢与位错的结合能。对合金元素对H—CWP 以及氢与位错的交互作用的影响进行了讨论。","authors":[{"authorName":"杜家驹","id":"f2a21d8a-9674-4112-8054-829cc72c51a7","originalAuthorName":"杜家驹"},{"authorName":"毛鸥","id":"1305be34-9cd4-4344-a154-5d5581f0b3b8","originalAuthorName":"毛鸥"},{"authorName":"李全新","id":"c5e87d99-766d-4e57-a802-67f5aac00f78","originalAuthorName":"李全新"},{"authorName":"王翔","id":"137070c2-7682-4e93-ad44-1b486b2b9bca","originalAuthorName":"王翔"}],"categoryName":"|","doi":"","fpage":"27","id":"90344183-c110-4337-a8d0-1a0b1305f1b5","issue":"1","journal":{"abbrevTitle":"CLYJXB","coverImgSrc":"journal/img/cover/CLYJXB.jpg","id":"16","issnPpub":"1005-3093","publisherId":"CLYJXB","title":"材料研究学报"},"keywords":[{"id":"b5c2c54f-42ad-40b6-979b-60f7759a7e4e","keyword":"氢脆","originalKeyword":"氢脆"},{"id":"8b8a51a5-b88e-4e84-8bf1-0aa46bd8229a","keyword":"internal friction","originalKeyword":"internal friction"},{"id":"7310b052-4a03-406c-b72d-2de205879c3d","keyword":"dislocation","originalKeyword":"dislocation"}],"language":"zh","publisherId":"1005-3093_1989_1_1","title":"铁基合金中氢致冷加工内耗<span style=\"color:red\">峰</span>","volume":"3","year":"1989"},{"abstractinfo":"报道了在用脉冲355 nm的YAG激光对水/甲醇二元团簇的多光子电离飞行时间质谱研究中,发现在电离激光相对于脉冲分子束的不同延时或是同一延时下不同的激光能量下,测得的离子谱<span style=\"color:red\">峰</span>除强度变化外,峰值发生漂移.离子峰值漂移的大小与信号强度密切相关.信号强度越大,离子的飞行时间越短,峰值漂移越大.分析认为:这种峰值漂移不是因为新质量数谱<span style=\"color:red\">峰</span>的出现,而是离子在穿越质谱仪的离子引出区和加速区极板时发生部分离子吸附,引起极板间电压的起伏造成的.离子信号越强,意味着极板对离子吸附的量越大,导致离子峰值的漂移越大.离子在电场起伏下的数值模拟结果与实验中观测到的离子峰值漂移规律一致.","authors":[{"authorName":"张树东","id":"d69f4f0d-0582-4bf9-8b72-0478d48484c8","originalAuthorName":"张树东"},{"authorName":"张明霞","id":"07d2b4b9-4a03-425b-8be6-13d93e54e190","originalAuthorName":"张明霞"},{"authorName":"王艳","id":"27606d74-6f5d-4849-b049-c27b76ccc121","originalAuthorName":"王艳"},{"authorName":"朱湘君","id":"d079389c-0b03-45b2-860a-8c28a70db859","originalAuthorName":"朱湘君"},{"authorName":"孔祥和","id":"0df165c1-0a44-4035-8376-01ee9e2ee55f","originalAuthorName":"孔祥和"}],"doi":"10.3969/j.issn.1007-5461.2007.04.008","fpage":"438","id":"9a811852-ff62-4732-9321-9aae123a488a","issue":"4","journal":{"abbrevTitle":"LZDZXB","coverImgSrc":"journal/img/cover/LZDZXB.jpg","id":"53","issnPpub":"1007-5461","publisherId":"LZDZXB","title":"量子电子学报   "},"keywords":[{"id":"82da604d-909f-4647-b6d3-35d7c178b654","keyword":"光谱学","originalKeyword":"光谱学"},{"id":"397cc616-5c7e-4f0e-98e4-0137b9340e43","keyword":"质谱漂移","originalKeyword":"质谱漂移"},{"id":"ea5b4957-550f-400c-a013-4f376b8fc366","keyword":"激光电离","originalKeyword":"激光电离"},{"id":"fb6276a8-099f-48c0-86cc-84747e0f2c1b","keyword":"分子团簇","originalKeyword":"分子团簇"},{"id":"542349c2-c83a-459d-97b4-1f2b184bc3f9","keyword":"离子吸附","originalKeyword":"离子吸附"}],"language":"zh","publisherId":"lzdzxb200704008","title":"飞行时间质谱<span style=\"color:red\">峰</span>形分析","volume":"24","year":"2007"}],"totalpage":653,"totalrecord":6521}