通过调节微弧氧化电解液中Na2SiO3和KOH浓度的配比,制备出厚达200μm以上的陶瓷氧化层,并对膜层进行厚度测量、SEM分析和硬度测试。结果表明:当Na2SiO3的质量浓度为5.5~6.0 g/L、KOH的质量浓度为1 g/L时,膜层厚可达260μm;陶瓷膜层颗粒和放电气孔尺寸均较小,膜层致密性良好;同时硬度可达1500HV以上。
The aluminum ceramic coating with 200μm thickness was prepared by adjusting the concentration ratio of Na2SiO3 and KOH in the micro?arc oxidation electrolyte,and the thickness of ceramic coating,the microstructure and hardness of the ceramic coating were tested. The results show that when the concentration of Na2SiO3 is from 5.5 to 6.0 g/L and KOH concentration is 1 g/L,the thickness of the prepared ceramic coating is 260μm. And the results of scanning electron microscopy (SEM)show that the particles size of ceramic coating and the pore size of discharge are both small,and the compactness of ceramic coating is good,at the same time,its hardness can reach more than 1 500HV.
参考文献
[1] | 陈妍君,冯长杰,邵志松,王春霞,周雅.铝合金微弧氧化技术的研究进展[J].材料导报,2010(09):132-136. |
[2] | 李占明,邱骥,孙晓峰,黄元林.铝合金表面微弧氧化技术研究与应用进展[J].装甲兵工程学院学报,2013(03):82-87. |
[3] | 蒋百灵,张先锋,朱静.铝、镁合金微弧氧化技术研究现状和产业化前景[J].金属热处理,2004(01):23-29. |
[4] | 严志军,朱新河,程东,刘杰.影响铝合金微弧氧化成膜效率的因素分析[J].大连海事大学学报,2007(04):113-117. |
[5] | 杨靖,周慧玲,王军华,杜茂华,韩福柱.电参数对LY12铝合金微弧氧化成膜影响规律的研究[J].电加工与模具,2013(03):26-31. |
[6] | 葛延峰,蒋百灵,时惠英.硅酸钠浓度对铝合金微弧氧化起弧过程能量消耗的影响[J].中国有色金属学报,2013(04):950-956. |
[7] | 段关文,高晓菊,满红,张武,姜光华,李金富.微弧氧化研究进展[J].兵器材料科学与工程,2010(05):102-106. |
[8] | 慕伟意,李争显,杜继红,李少龙.铝合金微弧氧化陶瓷涂层研究进展[J].表面技术,2013(04):94-99. |
[9] | 张津,吴护林.发动机喷管隔热涂层的设计和模拟计算[J].兵工学报,2002(02):209-211. |
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