利用扫描电镜(SEM)、透射电镜(TEM)、电子探针(EPMA)、能谱(EDS)和X射线衍射(XRD)技术研究了硅对定向凝固Ni3Al基合金IC6A微观组织的影响.结果表明在IC6A合金中添加0.10%~0.20%Si(质量分数,下同)会使合金的枝晶间区析出块状的Mo1.24Ni0.76相和Mo6(Ni0.75Si0.25)7相,当硅的添加量达到0.30%时,合金的枝晶间区除了析出这两种相外,还有针状的δ-NiMo相析出.这二相的析出不利于合金的高温持久性能,它们的硬度较大,只能通过孪晶的方式变形.硅有利于提高IC6A合金的高温抗氧化性能,而对合金的抗腐蚀性能和瞬时拉伸性能无明显影响.
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