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The measured hardness of nanocrystalline Cu with grain sizes (( as small as 10 nm still follows the Hall-Petch relation. A rate sensitivity of 0.06 +/- 0.01 and a flow stress activation volume of 8b(3) were determined at d = 10 nm, suggesting grain boundary activities are enhanced but not yet dominant in the plastic deformation. (c) 2006 Published by Elsevier Ltd. on behalf of Acta Materialia Inc.

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