研究了用喷雾干燥法处理Yb2O3掺杂的氧化锆超细粉的性能.采用LS800型激光衍射粒度分析仪、JB-1型氮吸附比表面仪、Rigaku-DmaxⅡ型X射线衍射仪(XRD)和JSM-6700F型扫描电镜(SEM)分析了喷雾干燥法制备的Yb2O3(Al2O3)-8YSZ超细粉的粒度分布和比表面积,研究了粉末微观形貌特征.结果表明,制备的是球形颗粒、分散性好,晶粒尺寸均匀的超微细2%Yb2O3(Al2O3)-8YSZ(摩尔分数)粉末.
参考文献
[1] | 锆粉的制备与应用[J].稀有金属快报,2005(10):45-47. |
[2] | 王泽彬,孙越,王岷,李春艳.粉末状氢氧化锆的制备[J].稀有金属快报,2005(01):28-29. |
[3] | Tekeli S;Erdogan M;Aktas B .Influence of α-Al2O3 Addition on Sintering and Grain Grownth Behaviour of 8mol% Y2O3-Stabilised Cubic Zirconia(C-ZrO2)[J].Ceramics International,2004,30:2203-2209. |
[4] | 于鑫萌 .电熔氧化锆的发展及前景[J].稀有金属快报,2005,23(06):6-10. |
[5] | Menzler Norbert H;Lavergnat Dominique .Materials Synthesis and Characterization of 8YSZ Nanomaterials for the Fabri cation of Electrolyte Membranes in Solid Oxide Fuel Cells[J].Ceramics International,2003,29:619-628. |
[6] | Yamamoto O.;Takeda Y.;Imanishi N.;Mizutani Y.;Kawai M. Nakamura Y.;Arati Y. .ELECTRICAL CONDUCTIVITY OF STABILIZED ZIRCONIA WITH YTTERBIA AND SCANDIA[J].Solid state ionics,1995(0):137-142. |
[7] | 豆斌朝,林振汉,吴亮,平信义.氧化锆固体电解质的掺杂性能和应用[J].稀有金属快报,2004(06):18-20. |
[8] | Guo X. .SPACE-CHARGE CONDUCTION IN YTTRIA AND ALUMINA CODOPED-ZIRCONIA[J].Solid state ionics,1997(3/4):247-254. |
[9] | Manuel Gaudon;Elisabeth Djurado;Menzler Norbert H .Morphology and Sintering Behaviour of Yttria Stabilized Zirconia(8-YSZ)Powders Synthesized by Spray Pyrolysis[J].Ceramics International,2004,30:2295-2303. |
[10] | Sirarat Kongwudithiti;Piyasan Praerthdam;Peter Silverston;el al .Influence of Sythesis Conditions on the Preparation of Zirconia Powder by the Glycothermal Method[J].Ceramics International,2003,29:807-814. |
[11] | 林振汉,张玲秀,吴亮.喷雾干燥法处理水合氧化锆[J].中国有色金属学报,2005(07):1118-1123. |
[12] | Xin Guo .Roles of Alumina in Zirconia for Functional Applications[J].Journal of the American Ceramic Society,2003(11):1867-1873. |
[13] | Bastow T J;Mathews Tom;Sellar J R .Al2O3 Solubility in the Fast Ion Conductor 0.88ZrO2-(0.12-x)Sc2O3-xAl2O3 Determined by 27Al NMR[J].Solid State Ionics,2004,175:415-417. |
[14] | Pinggen Rao;Mikio Iwasa;Jianqing Wu .Effect of Al_2O_3 addition on ZrO_2 phase composition in the Al_2O_3-ZrO_2 system[J].Ceramics International,2004(6):923-926. |
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