采用一种新的旋转基体稳态流化床沉积装置制备大尺寸的各向同性热解炭材料.利用金相显微镜、扫描电镜、透射电镜和XRD对各向同性热解炭材料的微观结构进行了表征,并对其力学性能进行了测试.结果表明,改进后的旋转基体稳态流化床沉积工艺能够制备出大尺寸的各向同性热解炭材料.材料的结构均匀,气孔较少,主要由球形颗粒状碳结构组成,构成这种球形颗粒状碳结构的是乱层结构的石墨片层堆积体.各向同性热解炭与传统炭材料相比具有较高的杨氏模量、硬度和强度.
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