化学镀Ni-P镀层的显微组织对其服役性能有重要影响.通过SEM、TEM、XRD和DTA等分析手段,研究了压铸镁合金表面Ni-P镀层的晶化过程.结果表明,初始化学镀层不仅有非晶,还有亚稳态纳米晶;镀层的初始晶化温度大约为300 ℃,450 ℃晶化过程完成;升温过程中的原子扩散和纳米晶的长大导致有新的亚稳态相析出和转变;有序畴和析出物一起长大最终产生晶界.
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