本文采用分析纯TiO2粉体、粘结剂及造孔剂制备了TiO2电极.通过水煮法测定所制备电极的孔隙率,同时还分析了其物相组成.在此基础上,采用不同电极组装方式进行了电解实验,对电解后的产物进行了X射线衍射仪分析.研究结果表明,所研制的TiO2电极孔隙率达到50%以上;烧结后的电极成份几乎都是金红石型TiO2;在确定的电极组装方式下进行电解实验,能够获得较大的电解电流,而且电解产物含钛量达到98%(w)以上.
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