由二甲亚砜和高岭石实现插层反应,继先后以甲醇和苄基三甲基氯化铵置换之,得到片状的高岭石/苄基铵盐插层复合物。以X射线衍射、红外光谱仪、热重测试和扫描电镜分别表征其结构和形貌,探讨其形成机理和理论模型。
Lamellate kaolinite-benzyltrimethylammonium intercalation compound was synthesized first by DM-SO and kaolinite intercalated reaction,then replaced by methanol and benzyltrimethylammonium chloride(TM-BAC)successively.The new intercalated compounds were characterized by X-ray diffraction (XRD),Fourier transform infrared spectroscopy (FT-IR),thermal gravity analysis (TG)and scanning electron microscope (SEM).The possible intercalation mechanism and theoretical model of intercalation compounds were discussed.
参考文献
[1] | Petr Ptacek;Karel Lang;Frantisek Soukal.Preparation and properties of nanostructured ceramic foam from kaolinite[J].Powder Technology: An International Journal on the Science and Technology of Wet and Dry Particulate Systems,2014:29-34. |
[2] | 邓友军;马毅杰;温淑瑶.有机粘土化学研究进展与展望[J].地球科学进展,2000(2):197-203. |
[3] | Jakub Matusik;Lucyna Matykowska.Behaviour of kaolinite intercalation compounds with selected ammonium salts in aqueous chromate and arsenate solutions[J].Journal of Molecular Structure,2014:52-59. |
[4] | 胡乃非;李溱;马红艳.肌红蛋白在双十二烷基二甲基溴化铵-粘土多双层复合薄膜电极上的电化学与电催化[J].高等学校化学学报,2001(3):450-454. |
[5] | 任子平;杨赞中.有机粘土矿物在环境保护中的应用研究进展[J].中国非金属矿工业导刊,2001(3):24-26. |
[6] | 郭鹏;纪阳;王定;刘钦甫.高岭石-季铵盐插层复合物脱嵌反应热动力学[J].硅酸盐通报,2015(2):466-469. |
[7] | Frost RL.;Paroz GN.;Tran TH.;Kloprogge JT.;Kristof J..The role of water in the intercalation of kaolinite with potassium acetate[J].Journal of Colloid and Interface Science,19982(2):227-236. |
[8] | 陈祖熊;颜卫;王坚;季春勇;成玉梅.肼对高岭土插层的研究(Ⅰ)--肼溶液浓度对插层的影响[J].建筑材料学报,2000(2):151-155. |
[9] | Yoshihiko Komori;yoshiyuki Sugahara;Kazuyuki Kuroda.Intercalation of alkylamines and water into kaolinite with methanol kaolinite as an intermediate[J].Applied clay science,19991/2(1/2):241-252. |
[10] | 刘钦甫;王定;郭鹏;张帅;程宏飞;李晓光;张士龙.季铵盐-高岭石系列插层复合物的制备及结构表征[J].硅酸盐学报,2015(2):222-230. |
[11] | 陆银平;李靖如;李晓光;刘钦甫.大同粗晶高岭石-二甲基亚砜插层复合物的制备及表征[J].矿物岩石,2014(2):13-17. |
[12] | 李靖如;牛胜元;陆银平.淮北焦宝石型高岭石/二甲基亚砜插层复合物的制备与表征[J].硅酸盐通报,2014(11):2785-2789. |
[13] | Fang QH;Huang SP;Wang WC.Intercalation of dimethyl sulphoxide in kaolinite: Molecular dynamics simulation study[J].Chemical Physics Letters,20051/3(1/3):233-237. |
[14] | Komori Y.;Kuroda K.;Sugahara Y..A kaolinite-NMF-methanol intercalation compound as a versatile intermediate for further intercalation reaction of kaolinite[J].Journal of Materials Research,19984(4):930-934. |
[15] | 杜小龙;严志飞;侯壮豪;武树茂;王君霞;吴秀玲.烷基咪唑离子液体插层高岭石复合物的制备与表征?[J].功能材料,2015(7):7122-7126. |
[16] | 吴德意;孔海南;褚春凤.高岭石-甲醇夹层复合体的合成及其特性[J].土壤,2004(1):51-55. |
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