利用自蔓延高温合成技术(self-propagating high temperature syntheris,SHS)合成La0.67Sr0.33MnO3粉体,探讨了自蔓延合成工艺对粉体结构及放电等离子体(spark plasma sintering,SPS)和普通烧结对La0.67Sr0.33MnO3粉体烧结性能和陶瓷显微结构的影响.经XRD,SEM,密度测试等结果表明:在自蔓延法合成出的物相为单一的钙钛矿型结构.SPS烧结与传统的固相烧结法相比:SPS快速烧结大大降低了传统固相法烧结温度,烧结后的晶粒大小基本均匀,烧结体致密度高.经过巨磁电子效应(colossal magnetoresistance,CMR)的测量得出,采用SPS放电等离子烧结的样品相对于普通烧结的样品,低温CMR效应有所增大.
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