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对Zn-PTFE(聚四氟乙烯)复合电极的复合电沉积过程进行研究,并考察了它在电合成频那醇上的应用.实验结果表明:控制镀液中PTFE悬浮量为30mL/L,镀液温度25℃,以5.0A/dm2电流密度电沉积22.5C,可制备出PTFE微粒分散均匀的复合电极;以此复合电极为阴极电合成频那醇,产率可达53.6%,明显高于Zn电极的25.1%.

A Zn-PTFE(Zinc-polytetrafluoroethylene) composite electrode withwell-dispersed PTFE fine particle has been prepared in conditions of 5.0 A/dm2, 22.5C, and PTFE 30 mL/L at 25 ℃. The composite electrode was used as cathode in electrosynthesis of pinacol from acetone in yield of 53.6%, much higher than that by using Zn electrode as cathode(25.1%).

参考文献

[1] Guglielmi N. J Electrochem Soc,1972,119:1009
[2] Kunugi Y,Fuchigami T,Nonaka T. J Electroanal Chem,1990,287:385
[3] Kunugi Y,Nonaka T. J Electroanal Chem,1993,356:163
[4] HUANG Ling(黄令),XU Shu-Kai(许书楷),ZHOU Shao-Min(周绍民), et al. Yingyong Huaxue(应用化学),1997,14(4):21
[5] XU Hong-Ding(许宏鼎),ZOU Ming-Zhu(邹明珠),CAO Zhan-Shuang(曹占双), et al. Gaodeng Xuexiao Huaxue Xuebao(高等学校化学学报),1995,16(1):50
[6] XIAO Xiu-Feng(肖秀峰),LIU Rong-Fang(刘榕芳),ZHU Ze-Shan(朱则善). Yingyong Huaxue(应用化学),1999,4:108
[7] GUO He-Tong(郭鹤桐),ZHANG San-Yuan(张三元). Composite Coatings(复合镀层). Tianjin(天津):Tianjin University Press(天津大学出版社),1991:53
[8] Цзгаришев Н А,Арямова И И. ДАН,1952,84:313
[9] DING Shao-Min(丁绍民). Jingxi Huagong(精细化工),1996,13(1):42
[10] Totir N D,Lete C,Nenu C. Rev Chim(Buchare-st),1998,49(4):279
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