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The title compound in monohydrate was prepared fromaminoiminomethanesulfinic aicd by H2O2 oxidation in aqueous sulfuric acid solution. The compound is unstable in moisture, especially in acid atmosphere.

参考文献

[1] Miller A E,Bischoff J J. Synthesis,1986,9:777
[2] Kim K,Lin Y T,Mosher H S. Tetrahedron Lett,1988,26:3183
[3] Debowski Z. Przem Chem,1965,44:82
[4] Walter W,Randau G. Justus Liebigs Ann Chem,1969,722:98
[5] ZOU Chun-Sheng(邹春生). Yinran(印染),1984,2:45
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