采用铜模吸铸法制备出La62.0Al15.7(Cu0.5, Ni0.5)22.3大块非晶合金,并在室温和3.0～5.0 GPa压力条件下对该非晶合金进行了等温高压处理,研究了高压处理对该非晶结构弛豫和力学行为的影响.结果表明,高压处理对非晶合金的玻璃转变温度无明显影响,但使合金发生了明显的结构弛豫,其自由体积和第一晶化温度随压力的增加先增加后减小,最大值出现在4.0 GPa压力之下.纳米压痕和维氏硬度测试表明,其硬度值随压力变化规律与自由体积随压力变化规律一致.
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