以络合剂为辅助剂,用水热方法合成了多臂CdS纳米晶体,用TEM、ED、SEM、RAMAN、PL等技术对产物进行了表征.研究了不同络合剂对水热合成多臂CdS纳米晶体的影响,以乙二胺、甲胺、乙胺为辅助剂水热合成所得三臂CdS的产率分别为2%、35%、85%,而以氨为辅助剂时,仅能得到颗粒状CdS纳米晶体.此外,对水热合成多臂CdS纳米晶体的形成机制作了初步探讨.
参考文献
| [1] | Louis R.J.Phys.Chem.,1986,90:2555-2560. |
| [2] | Vossmeyer T,Delonno E,Heath J R.Angew.Chem.Int.Ed.Engl.,1997,36:1080-1083. |
| [3] | Ohara P C,Heath J R,Gelbart W M.Angew.Chem.Int.Ed.Engl.,1997,36:1078-1080. |
| [4] | Merirav U,Foxman E B.Semilonductor Sci.Technol.,1998,11:255-262. |
| [5] | Andres R P,Bielefeld J D,Henderson J I,et al.Science,1996,273:1690-1693. |
| [6] | Willner I,Patolsky F,Wasserman J.Angew.Chem.Int.Ed.Engl.,2001,40:1861-1864. |
| [7] | Hu J,Li L-S,Yang W,et al.Science,2001,292:2060-2063. |
| [8] | Peng Z A,Peng X.J.Am.Chem.Soc.,2001,123:13891395. |
| [9] | Kuan X,Huang Y,Cui Y,et al.Nature,2001,409:66-68. |
| [10] | Manna L,Scher E C,Alivisatos A P.J.Am.Chem.Soc.,2000,122:12700-12706. |
| [11] | Jun Y W,Lee S M,KangN J,et al.J.Am.Chem.Soc.,2001,123:5150-5151. |
| [12] | Jun Y,Jung Y,Cheon J.J.Am.Chem.Soc.,2002,124:615-619. |
| [13] | Gao F,Lu Q,Xie S,Zhao D.Adv.Mater.,2002,14:1537-1540. |
| [14] | Arguello C A,Rousseau D L,Porto S P S.Phys.Rev.,1969,181:1351-1355. |
| [15] | Nada K K,Sahu S N.Solid State Comm.,1999,111:671-675. |
| [16] | Nie Q L,Yuan Q L,Chen W X,et al.Journal of Crystal Growth,2004,265:420-424. |
| [17] | 聂秋林,袁求理,徐铸德(NIE Qiu-Lin,et al).无机材料学报(Journal of Inorganic Materials),2004,19 (6):1411-1414. |
| [18] | Ma X C,Xu F,Qian Y T.Materials Research Bulletin,2005,40:2180-2184. |
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