采用包裹工艺和热压工艺制备了Al2O3/Ni金属陶瓷.在1450°C热压Ni包裹Al2O3复合粉体得到相对密度>98%的金属陶瓷,当温度>1400°C时,随着Ni含量的增加致密度下降.Ni颗粒位于三角晶界,随着含量的增加,断裂方式由沿晶转为穿晶断裂;在A12O3基体中引入Ni颗粒能够降低晶粒尺寸,提高强度和韧性.与单相Al2O3的力学性能相比,综合力学性能较好的NA4金属陶瓷的抗弯强度和断裂韧性分别提高了19%和35%,分析了金属陶瓷的增强增韧机制.
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