以硼酸三丁酯为硼源,用溶液液相移植的方法制备了B2O3/MCM-41材料.用DTA、XRD、FTIR、XPS和氮气吸附-脱附曲线等手段表征了合成的材料.结果表明:硼物种发生析晶,以B2O3的形式存在,硼的配位状态为三配位的BO3结构单元.
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