尝试以含Al、B、C的化合物为烧结助剂进行了α-SiC粉末的无压烧结,研究了烧结助剂中Al和B的配比、烧结温度、保温时间等因素对烧结体密度和力学性能的影响.结果表明,最佳保温时间为1h;当烧结温度为1850℃以上时,烧结体的相对密度达到了90%;当Al/B=3和4时,烧结体的性能相对较好.XRD显示了Al8B4C7相的存在,表明在烧结过程中反应生成了Al8B4C7,烧结机制是液相烧结.扫描电镜照片显示了断面结构和晶粒形貌.
参考文献
[1] | Prochazka S. In: Popper P, ed. Special Ceramics 6. Stoke on Trent. U.K.: British Ceramic Research Association, 1975. 171-181. |
[2] | Tanaka H. In: Somiya S and Inomata Y, eds. Silicon Carbide Ceramics-1, New York: Elsevier, 1991.213-238. |
[3] | Shinozaki S, Hangas J, Carduner K R, et al. J. Mater. Res., 1993, 8(7): 1635-1643. |
[4] | Mulla M A, Krstic V D. J. Mater. Res., 1994, 29(1): 34-38. |
[5] | Mulla M A, Krstic V D. Am. Ceram. Soc. Bull., 1991, 70(3): 439-443. |
[6] | Padture N P. J. Am. Ceram. Soc., 1994, 77(2): 519-523. |
[7] | 谭寿洪,陈忠明,江东亮(Tan Shou-Hong,et al).硅酸盐学报(Joural of Chinese Ceramic Society),1998,26(2):191-197. |
[8] | Mitomo M, Kim Y W, Hirotsuru H. J. Mater. Res., 1996, 11(7): 1601-1604. |
[9] | Shinozaki S, Williams R M, Juterbodk B N, et al. Am. Ceram. Soc. Bull., 1985, 64(10): 1389-1393. |
[10] | Cao J J, MoberlyChan W J, Ritdhie T O, et al. J. Am. Ceram. Soc., 1996, 79(2): 461-469. |
[11] | Inomata Y, Tanaka H, Inoue Z, et al. J. Ceram. Soc. Jpn., 1980, 10(11): 1313-1314. |
[12] | Zhou Y, Tanaka H, Otani S, et al. J. Am. Ceram. Soc., 1999, 82(8): 1959-1964. |
[13] | Tanaka H, Zhou You. J. Mater. Res., 1999, 14(2): 518-522. |
[14] | Iseki T, Kameda T, Maruyama T. J. Mater. Sci., 1984, 19: 1692-1698. |
[15] | Laurent V, Chatain D, Eustathopoulos N. J. Mater. Sci., 1987, 22(1): 244-250. |
[16] | Yamaguchi A, Zhang S. J. Ceram. Soc. Jp., 1995, 103(1): 20-24. |
上一张
下一张
上一张
下一张
计量
- 下载量()
- 访问量()
文章评分
- 您的评分:
-
10%
-
20%
-
30%
-
40%
-
50%