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以碳化硅微粉作为原料,并选用Al2O3、高岭土和MgO作为烧结助剂,同时选用羧甲基纤维素钠(CMC)、聚丙烯酰胺(PAM)和可溶性淀粉作为添加剂,通过有机泡沫浸渍法制备出莫来石/碳化硅复相泡沫陶瓷材料.研究了不同原料组成、不同烧结温度等工艺参数对所制备的莫来石/碳化硅复相泡沫陶瓷物相组成、微观结构的影响,同时对莫来石/碳化硅复相泡沫陶瓷的孔隙率、力学性能进行了测试.研究结果表明:莫来石/碳化硅复相泡沫陶瓷的微观结构控制主要受碳化硅含量的影响,随着碳化硅含量的增加,莫来石/碳化硅复相泡沫陶瓷的孔隙率有明显的降低,但抗压强度随之提高;随着烧结温度的提高,孔棱的致密度增加,抗压强度亦显著提高;莫来石/碳化硅复相泡沫陶瓷的最佳烧结温度为1600℃,陶瓷粉料中最佳的SiC含量为35%.在1600℃烧结温度下,碳化硅的含量为35%时,获得了孔隙率为76.19%和抗压强度为4.63 MPa的莫来石/碳化硅复相泡沫陶瓷.

参考文献

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