通过烧结杯试验制备了不同碱度和不同MgO含量2个系列的低硅烧结矿样品.利用XRD(X射线衍射仪)和TEM(透射电子显微镜)分别对样品的结构和表面形貌进行了表征.随碱度和MgO含量提高,CaFe2O4和Fe3O4含量发生了显著变化;孔隙结构由柱状变为溶蚀网状,更加复杂.利用单重分形软件和表面分形模型分别计算了2个系列样品的表面分形维数(Dss和Dsv).随着碱度和MgO含量提高,表面分形维数增加;利用表面分形模型计算的Dsv和Rsv(线性相关系数)大于单重分形软件计算的Dss和Rss,表面分形模型可以反映更多细节,且相关性更好.因此可以用表面分形模型替代传统的单重分形软件来表征孔隙结构的复杂性,解决了孔隙表面形貌拍摄的困难和选择区域的局限性.
参考文献
[1] | Virendra S Warke;Richard D Sisson Jr;Makhlouf M Makhlouf .The Effect of Porosity on the Austenite to Ferrite Transformation in Powder Metallurgy Steels[J].MATERIALS SCIENCE & ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING,2011,528:3533. |
[2] | 蒋大军,宋剑,何木光,杜斯宏.钒钛磁铁矿烧结降低返矿率技术研究与实践[J].中国冶金,2014(04):39-44. |
[3] | Iasef Md Rian;Jin-Ho Park;Hyung Uk Ahn;Dongkuk Chang .Fractal geometry as the synthesis of Hindu cosmology in Kandariya Mahadev temple, Khajuraho[J].Building and environment,2007(12):4093-4107. |
[4] | Yuting Wang;Sidney Diamond .A fractal study of the fracture surfaces of cement pastes and mortars using a stereoscopic SEM method[J].Cement and Concrete Research,2001(10):1385-1392. |
[5] | WU Ai-xiang,YANG Bao-hua,ZHOU Xu.Fractal analysis of granular ore media based on computed tomography image processing[J].中国有色金属学会会刊(英文版),2008(06):1523-1528. |
[6] | Simon S Cross .The Application of Fractal Geometric Analysis to Microscopic Images[J].MICRON,1994,25(01):101. |
[7] | LU Guo-jun .Fractal Image Compression[J].Signal Processing Image Communication,1993,5(04):327. |
[8] | 李远亮,张庆军,莫文玲,姜丽梅,刘金刚,张玉柱.变碱度条件下低硅烧结矿孔径分布的多重分形[J].钢铁,2013(01):10-14. |
[9] | 李远亮,张庆军,莫文玲,姜丽梅,刘金刚,张玉柱.变碱度条件下低硅烧结矿孔径分布的多重分形[J].钢铁,2013(01):10-14. |
[10] | 张玉柱,鲍继伟,龙跃,邢宏伟.CaO对气淬钢渣中C2S等温析晶动力学影响规律[J].钢铁,2013(11):84-88. |
[11] | Victor M. Bolanos-Garcia;Naomi E. Chayen .New directions in conventional methods of protein crystallization[J].Progress in Biophysics and Molecular Biology: An International Review Journal,2009(1/3):3-12. |
[12] | R.V. Castillo;A.J. Miiller .Crystallization and morphology of biodegradable or biostable single and double crystalline block copolymers[J].Progress in Polymer Science,2009(6):516-560. |
[13] | WANG Yi-ci,ZHANG Jian-liang,ZHANG Fang,LUO Guo-ping.Formation Characteristics of Calcium Ferrite in Low Silicon Sinter[J].钢铁研究学报:英文版,2011(10):1-7. |
[14] | DONG Hui;JIA Feng-rui;ZHAO Yong et al.Experimental Investigation on the Drying Process of the Sinter Mixture[J].Powder Technology,2012,218:1. |
[15] | Marian Raczka;Gabriela Gorny;Ludoslaw Stobierski .Effect of carbon content on the microstructure and properties of silicon carbide-based sinters[J].Materials Characterization,2001(2/3):245-249. |
[16] | Robert Riding .Structure and Composition of Organic Reefs and Carbonate Mud Mounds:Concepts and Categories[J].Earth-Science Reviews,2002,58(01):163. |
[17] | XIE He-ping.Introduction of Fractal-Rock Mechanics[M].北京:科学出版社,2005 |
[18] | Hermanowicz S W;Schindler U;Wilderer P .Fractal Structure of Biofilms:New Tools for Investigation of Morphology[J].Water Science and Technology,1995,32(08):99. |
[19] | Hillar M Rootare;Judson Spencer .A Computer Program for Pore Volume and Pore Area Distribution Calculations From Mercury Porosimeter Data on Particulate or Porous Materials[J].Powder Technology,1972,6(01):17. |
[20] | MacAskill I A;Heard D W;Bishop D P .Effects of Silicon on the Metallurgy and Sintering Response ofAl-Ni-Mg PM Alloys[J].MATERIALS SCIENCE & ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING,2007,452-453:688. |
[21] | Jakubowicz J;Smardz K;Smardz L .Characterization of porous silicon prepared by powder technology[J].Physica, E. Low-dimensional systems & nanostructures,2007(1/2):139-143. |
[22] | 何木光.控制钒钛磁铁烧结矿 FeO 含量的方法[J].中国冶金,2014(7):32-35,41. |
[23] | Florindo, J.B.;Bruno, O.M. .Fractal descriptors based on Fourier spectrum applied to texture analysis[J].Physica, A. Statistical mechanics and its applications,2012(20):4909-4922. |
[24] | Drochss P. Valencia;Felipe J. González.Estimation of diffusion coefficients by using a linear correlation between the diffusion coefficient and molecular weight[J].Journal of Electroanalytical Chemistry: An International Journal Devoted to All Aspects of Electrode Kinetics, Interfacial Structure, Properties of Electrolytes, Colloid and Biological Electrochemistry,2012:121-126. |
[25] | 崔志敏,李秀景,陈颖,张庆军,张玉柱.低硅烧结矿表面的多重分形谱计算和分析[J].钢铁研究学报,2014(04):29-32. |
上一张
下一张
上一张
下一张
计量
- 下载量()
- 访问量()
文章评分
- 您的评分:
-
10%
-
20%
-
30%
-
40%
-
50%