以Bi(NO3)3·5H2O和KCl为原料,乙二醇为溶剂,通过溶剂热法合成了BiOCl系列材料,同时对BiOCl进行了XRD和SEM表征,表征结果表明经溶剂热法合成的BiOCl产品纯净,形貌为1.5～4.0μm的球状结构.实验表明,BiOCl的最佳合成条件为:合成时间10 h,合成温度160℃,该条件下得到的BiOCl对罗丹明B的降解率在15 min时达到97.38％.
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