A Pd‐isatin Schiff base complex immobilized onγ‐Fe2O3 (Pd‐isatin Schiff base‐γ‐Fe2O3) was synthe‐sized and characterized by Fourier transform infrared, scanning electron microscopy, high resolu‐tion transmission electron microscopy, X‐ray diffraction, thermogravimetric gravimetric analysis, inductively‐coupled plasma, X‐ray photoelectron spectroscopy, and elemental analysis. It was used as a magnetically reusable Pd catalyst for the Heck and Suzuki cross‐coupling reactions.
参考文献
[1] | Lu A H;Salabas E L;Schuth F .[J].ANGEWANDTE CHEMIE-INTERNATIONAL EDITION,2007,46:1222. |
[2] | Bao J;Chen W;Liu T T;Zhu Y L Jin P Y Wang L Y Liu J F Wei Y G Li Y D .[J].ACS Nano,2007,1:293. |
[3] | Wang L;Neoh KG;Kang ET;Shuter B;Wang SC .Biodegradable magnetic-fluorescent magnetite/poly(dl-lactic acid-co-alpha,beta-malic acid) composite nanoparticles for stem cell labeling.[J].Biomaterials,2010(13):3502-3511. |
[4] | Hu F Q;Wei L;Zhou Z;Ran Y L Li Z Gao M Y .[J].Advanced Materials,2006,18:2553. |
[5] | Nasongkla N;Bey E;Ren JM;Ai H;Khemtong C;Guthi JS;Chin SF;Sherry AD;Boothman DA;Gao JM .Multifunctional polymeric micelles as cancer-targeted, MRI-ultrasensitive drug delivery systems[J].Nano letters,2006(11):2427-2430. |
[6] | Sun C;Lee JS;Zhang M .Magnetic nanoparticles in MR imaging and drug delivery.[J].Advanced drug delivery reviews,2008(11):1252-1265. |
[7] | Grancharov S G;Zeng H;Sun S H;Wang S X O'Brien S Murray C B Kirtley J R Held G A .[J].Journal of Physical Chemistry B,2005,109:13030. |
[8] | Tegus O;Bruck E;Buschow K H J;de Boer F R .[J].NATURE,2002,415:150. |
[9] | Zeng T Q;Yang L;Hudson R;Song G H Moores A R Li C J .[J].Organic Letters,2011,13:442. |
[10] | Polshettiwar, V.;Luque, R.;Fihri, A.;Zhu, H.;Bouhrara, M.;Basset, J.-M. .Magnetically recoverable nanocatalysts[J].Chemical Reviews,2011(5):3036-3075. |
[11] | Huang, JL;Zhu, FX;He, WH;Zhang, F;Wang, W;Li, HX .Periodic Mesoporous Organometallic Silicas with Unary or Binary Organometals insDEe the Channel Walls as Active and Reusable Catalysts in Aqueous Organic Reactions[J].Journal of the American Chemical Society,2010(5):1492-1493. |
[12] | Koukabi N;Kolvari E;Zolfigol M A;Khazaei A Shaghasemi B S Fasahati B .[J].Advanced Synthesis and Catalysis,2012,354:2001. |
[13] | Beller M;Bolm C.Transition Metals for Organic Synthesis:Build-ing Blocks and Fine Chemicals. 2nd Ed[M].Weinheim:Wiley VCH,2004 |
[14] | Brennfhrer A;Neumann H;Beller M .[J].Angew Chem Int Edt,2009,48:4114. |
[15] | de Vries A H M;Mulders J M C A;Mommers J H M;Henderickx H J W de Vries J G .[J].Organic Letters,2003,5:3285. |
[16] | Gholinejad M;Karimkhani V;Kim I .[J].Applied Organometallic Chemistry,2014,28:221. |
[17] | Blaser H U;Indolese A;Naud F;Nettekoven U Schnyder A .[J].Advanced Synthesis and Catalysis,2004,346:1583. |
[18] | Torborg C;Beller M .[J].Advanced Synthesis and Catalysis,2009,351:3027. |
[19] | Sabounchei S J;Ahmadi M;Panahimehr M;Akhlaghi Bagherjeri F Nasri Z .[J].Journal of Molecular Catalysis A:Chemical,2014,383-384:249. |
[20] | Zamboulis A;Moitra N;Moreau J J E;Catto?n X Wong Chi Man M .[J].Journal of Materials Chemistry,2010,20:9322. |
[21] | Shakil Hussain S M;Ibrahim M B;Fazal A;Suleiman R Fettouhi M El Ali B .[J].POLYHEDRON,2014,70:39. |
[22] | Garcia-Melchor M;Ujaque G;Maseras F;Lledos A .[J].Catal Met Com-plex,2011,37:57. |
[23] | Borah B J;Saikia K;Saikia P P;Barua N C Dutta D K .[J].Catalysis Today,2012,198:174. |
[24] | Slagt V F;de Vries A H M;de Vries J G;Kellogg R M .[J].Org Pro Res Dev,2010,14:30. |
[25] | Morgan B P;Galdamez G A;Gilliard R J Jr;Smith R C.[J].DALTON TRANSACTIONS,2009:2020. |
[26] | Zhou YB;Xi ZX;Chen WZ;Wang DQ .Dinickel(II) Complexes of Bis(N-heterocyclic carbene) Ligands Containing [Ni-2(mu-OH)] Cores as Highly Efficient Catalysts for the Coupling of Aryl Chlorides[J].Organometallics,2008(22):5911-5920. |
[27] | Bakherad M;Jajarmi S .[J].Journal of Molecular Catalysis A:Chemical,2013,370:152. |
[28] | Wang D;Denux D;Ruiz J;Astruc D .[J].Advanced Synthesis and Catalysis,2013,355:129. |
[29] | Bakherad, M.;Keivanloo, A.;Bahramian, B.;Jajarmi, S..Suzuki, Heck, and copper-free Sonogashira reactions catalyzed by 4-amino-5-methyl-3-thio-1,2,4-triazole-functionalized polystyrene resin-supported Pd(II) under aerobic conditions in water[J].Journal of Organometallic Chemistry,2013:206-212. |
[30] | Choudary BM.;Madhi S.;Chowdari NS.;Kantam ML.;Sreedhar B. .Layered double hydroxide supported nanopalladium catalyst for Heck-, Suzuki-, Sonogashira-, and Stille-type coupling reactions of chloroarenes [Review][J].Journal of the American Chemical Society,2002(47):14127-14136. |
[31] | da Silva J F M;Garden S J;Pinto A C .[J].Journal of the Brazilian Chemical Society,2001,12:273. |
[32] | Singh, G.S.;Desta, Z.Y. .Isatins as privileged molecules in design and synthesis of spiro-fused cyclic frameworks (Review)[J].Chemical Reviews,2012(11):6104-6155. |
[33] | Chiyanzu I;Hansell E;Gut J;Rosenthal PJ;McKerrow JH;Chibale K .Synthesis and evaluation of isatins and thiosemicarbazone derivatives against cruzain, falcipain-2 and rhodesain.[J].Bioorganic and Medicinal Chemistry Letters,2003(20):3527-3530. |
[34] | Almeida M R;Leita?o G G;Silva B V;Barbosa J P Pinto A C .[J].Journal of the Brazilian Chemical Society,2010,21:764. |
[35] | Alagarsamy V;Revathi R;Meena S;Ramaseshu K V Rajasekaran S De Clercq E .[J].Indian Journal Of Pharmaceutical Sciences,2004,66:459. |
[36] | Verma M;Pandeya SN;Singh KN;Stables JP .Anticonvulsant activity of Schiff bases of isatin derivatives.[J].Acta pharmaceutica: a quarterly journal of Croatian Pharmaceutical Society and Slovenian Pharmaceutical Society, dealing with all branches of pharmacy and allied sciences,2004(1):49-56. |
[37] | Bal T B;Anand B;Yogeeswari P;Sriram D .[J].Bioorganic and Medicinal Chemistry Letters,2005,15:4451. |
[38] | Singh, G.S.;Desta, Z.Y. .Isatins as privileged molecules in design and synthesis of spiro-fused cyclic frameworks (Review)[J].Chemical Reviews,2012(11):6104-6155. |
[39] | Jiang T;Kuhen KL;Wolff K;Yin H;Bieza K;Caldwell J;Bursulaya B;Tuntland T;Zhang K;Karanewsky D;He Y .Design, synthesis, and biological evaluations of novel oxindoles as HIV-1 non-nucleoside reverse transcriptase inhibitors. Part 2.[J].Bioorganic and Medicinal Chemistry Letters,2006(8):2109-2112. |
[40] | Kulkarni A D;Patil S A;Badami P S .[J].Journal of Sulfur Chemistry,2009,30:145. |
[41] | Sobhani S;Pakdin-Parizi Z;Nasseri N .[J].JOURNAL OF CHEMICAL SCIENCES,2013,125:975. |
[42] | Sobhani S;Honarmand M .[J].Applied Catalysis A:General,2013,467:456. |
[43] | Sobhani S;Pakdin-Parizi Z .[J].RSC Adv,2014,4:13071. |
[44] | Sobhani S;Mesbah Falatooni Z;Honarmand M .[J].RSC Adv,2014,4:15797. |
[45] | Sobhani S;Pakdin-Parizi Z .[J].Applied Catalysis A:General,2014,479:112. |
[46] | Sobhani S;Ghasemzadeh M S;Honarmand M .[J].Catalysis Letters,2014,144:1515. |
[47] | Sobhani S;Ghasemzadeh M S;Honarmand M;Zarifi F .[J].RSC Adv,2014,4:44166. |
[48] | Sobhani S;Bazrafshan M;Arabshahi Delluei A;Pakdin-Parizi Z .[J].Applied Catalysis A:General,2013,454:145. |
[49] | Sobhani S;Jahanshahi R .[J].New Journal of Chemistry,2013,37:1009. |
[50] | Sobhani S;Pakdin-Parizi Z;Razavi N .[J].Applied Catalysis A:General,2011,409-410:162. |
[51] | Esmaeilpour M;Javidi J;Dodeji F N;Abarghoui M M .[J].Transition Metal Chemistry,2014,39:797. |
[52] | Sobhani S;Ghasemzadeh M S;Honarmand M;Zarifi F .[J].RSC Adv,2014,4:44166. |
[53] | Ho KM;Li P .Design and synthesis of novel magnetic core-shell polymeric particles[J].Langmuir: The ACS Journal of Surfaces and Colloids,2008(5):1801-1807. |
[54] | Bernini R;Cacchi S;Fabrizi G;Forte G Petrucci F Prastaro A Niembro S Shafir A Vallribera A .[J].Green Chemistry,2010,12:150. |
[55] | Li P H;Wang L;Zhang L;Wang G W .[J].Advanced Synthesis and Catalysis,2012,354:1307. |
[56] | Modak A;Mondal J;Sasidharan M;Bhaumik A .[J].Green Chemistry,2011,13:1317. |
[57] | Paraskar AS;Sudalai A .Co-catalyzed reductive cyclization of azido and cyano substituted alpha,beta-unsaturated esters with NaBH4: enantioselective synthesis of (R)-baclofen and (R)-rolipram[J].Tetrahedron,2006(20):4907-4916. |
[58] | Rodrigues T;Lopes F;Moreira R .[J].Synthetic Communications,2012,42:747. |
[59] | Iranpoor, N.;Firouzabadi, H.;Motevalli, S.;Talebi, M..Palladium nanoparticles supported on silicadiphenyl phosphinite (SDPP) as efficient catalyst for Mizoroki-Heck and Suzuki-Miyaura coupling reactions[J].Journal of Organometallic Chemistry,2012:118-124. |
[60] | Modak A;Mondal J;Bhaumik A .[J].Green Chemistry,2012,14:2840. |
[61] | Tamami, B.;Nezhad, M.M.;Ghasemi, S.;Farjadian, F..PCP-pincer palladium nanoparticles supported on modified Merrifield resin: A novel and efficient heterogeneous catalyst for carbonecarbon cross-coupling reactions[J].Journal of Organometallic Chemistry,2013:10-16. |
[62] | Monguchi Y;Sakai K;Endo K;Fujita Y Niimura M Yoshimura M Mizusaki T Sawama Y Sajiki H .[J].ChemCatChem,2012,4:546. |
[63] | Saleem F;Rao G K;Kumar A;Kumar S Singha M P Singh A K .[J].RSC Adv,2014,4:56102. |
[64] | Fortea-Pérez, F.R.;Schlegel, I.;Julve, M.;Armentano, D.;De Munno, G.;Stiriba, S.-E..Sustainable carbonecarbon bond formation catalyzed by new oxamate-containing palladium(II) complexes in ionic liquids[J].Journal of Organometallic Chemistry,2013:102-108. |
[65] | Zolfigol M A;Azadbakht T;Khakyzadeh V;Nejatyami R Perrin D M .[J].RSC Adv,2014,4:40036. |
[66] | Shakil Hussain S M;Ibrahim M B;Fazal A;Suleiman R Fettouhi M El Ali B .[J].POLYHEDRON,2014,70:39. |
[67] | Ghiaci M;Zargani M;Moeinpour F;khojastehnezhad A .[J].Appl Or-ganometal Chem,2014,28:589. |
[68] | Liu, Q.-X.;Zhang, W.;Zhao, X.-J.;Zhao, Z.-X.;Shi, M.-C.;Wang, X.-G. .NHC Pd~(II) complex bearing 1,6-hexylene linker: Synthesis and catalytic activity in the Suzuki-Miyaura and Heck-Mizoroki reactions[J].European journal of organic chemistry,2013(7):1253-1261. |
[69] | De Paula, V.I.;Sato, C.A.;Buffon, R. .Pd complexes based on phosphine-linked cyclophosphazenes: Synthesis, characterization and application in suzuki coupling reactions[J].Journal of the Brazilian Chemical Society,2012(2):258-266. |
上一张
下一张
上一张
下一张
计量
- 下载量()
- 访问量()
文章评分
- 您的评分:
-
10%
-
20%
-
30%
-
40%
-
50%