Magnetite nanoparticles coated with sulfuric acid-functionalized mesoporous MCM-48 were syn-thesized and used as a catalyst in three-component domino reactions of indoles, arylglyoxal mono-hydrates andN-arylenaminones to furnish the desired 3,3′-bisindoles by formation of two C–C and one C–N bonds in a smooth cascade with good yields under mild reaction conditions. The catalyst was recovered easily and maintained activity in successive runs.
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