SmAlO3 powders were successfully synthesized through the citrate sol-gel combustion method. The phase evolution of the prepared powders were characterized using thermal gravimetric (TG) analysis, differential scanning calorimetry (DSC) analysis and Fourier transform infrared spectroscopy (FTIR). X-ray diffraction (XRD) was applied to examine the purity of the powders. The re-flective properties of SmAlO3 with changing temperatures were investigated by ultraviolet-visible near-infrared spectrophotometer (UVPC) specular reflection spectrum. The results displayed that pure SmAlO3 phase with preferable reflectivity at 1.06μm could be obtained at 900 oC for 2 h. Furthermore, the reflectivity of SmAlO3 at various temperatures from-40 to 500 oC transformed within ±0.1%, and all maintained below 1%at 1.06μm. The absorbance of SmAlO3 in the resin solution was 2.134 and the moral absorption coefficient was about 384.8 in the work. The study indicated that SmAlO3 powders may be a promising kind of heat resistant absorb-ing material for 1.06μm laser defense, which could be further applied to laser absorbing coatings with a wide range of temperatures.
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