欢迎登录材料期刊网

材料期刊网

高级检索

Silver powder was fabricated by spray pyrolysis,using 2%-20% AgNO_3 solution,336-500 mL/h flux of AgNO_3 solution,0.28-0.32 MPa flux of carrier gas and in the 620-820℃tem-perature range.The effects of furnace set temperature,concentration of AgNO_3 aqueous solution,flux of AgNO_3 aqueous solution as well as carrier gas on the morphology and particle size distribution of silver powder,were investigated.The experimental results showed that with the high concentration of AgNO_3 aqueous solution,the average grain size of silver decreased with the increasing of furnace set temperature.But the gain size distribution was not homogenous,the discontinuous grain growth oc-curred.With the low concentration of AgNO_3 aqueous solution,the higher furnace set temperature made the nano sliver grains sintered together to grow.Nano silver powder about 100 nm was fabricated by spray pyrolysis,using 2wt% AgNO_3 solutions,336 mL/h flux of AgNO_3 aqueous solution,0.32 MPa flux of carrier gas at 720℃ furnace set temperature.

参考文献

[1] H.H.Nersisyan;J.H.Lee;H.T.Son;C.W.Won;D.Y.Maeng .A new and effective chemical reduction method for preparation of nanosized silver powder and colloid dispersion[J].Materials Research Bulletin: An International Journal Reporting Research on Crystal Growth and Materials Preparation and Characterization,2003(6):949-956.
[2] Wang LS;Deng JC;Yang F;Chen T .Preparation and catalytic properties of Ag/CuO nano-composites via a new method[J].Materials Chemistry and Physics,2008(2/3):165-169.
[3] Abu Bakar NHH;Ismail J;Abu Bakar M .Synthesis and characterization of silver nanoparticles in natural rubber[J].Materials Chemistry and Physics,2007(2/3):276-283.
[4] Singh N;Khanna PK .In situ synthesis of silver nano-particles in polymethylmethacrylate[J].Materials Chemistry and Physics,2007(2/3):367-372.
[5] Pickering AL;Cooper GJT;Long DL;Cronin L .Facile synthesis and structures of infinite one-dimensional silver(I) coordination polymers[J].Polyhedron: The International Journal for Inorganic and Organometallic Chemistry,2004(12):2075-2079.
[6] Zhiqiang Niu;Yan Fang .A new surface-enhanced Raman scattering system for C60 fullerene:Silver nano-particles/C60/silver film[J].Vibrational Spectroscopy: An International Journal devoted to Applications of Infrared and Raman Spectroscopy,2007(2):415-419.
[7] V. Shashikala;V. Siva Kumar;A.H. Padmasri;B. David Raju;S. Venkata Mohan;P. Nageswara Sarma;K.S. Rama Rao .Advantages of nano-silver-carbon covered alumina catalyst prepared by electro-chemical method for drinking water purification[J].Journal of molecular catalysis, A. Chemical,2007(1/2):95-100.
[8] Sobana N;Muruganadham M;Swaminathan M .Nano-Ag particles doped TiO2 for efficient photodegradation of Direct azo dyes[J].Journal of molecular catalysis, A. Chemical,2006(1/2):124-132.
[9] Lee SH;Oh SM;Park DW .Preparation of silver nanopowder by thermal plasma[J].Materials science & engineering, C. Biomimetic and supramolecular systems,2007(5/8):1286-1290.
[10] S. Remita;P. Fontaine;E. Lacaze;Y. Borensztein;H. Sellame;R. Farha;C. Rochas;M. Goldmann .X-ray radiolysis induced formation of silver nano-particles: A SAXS and UV–visible absorption spectroscopy study[J].Nuclear Instruments & Methods in Physics Research. B, Beam Interactions with Materials and Atoms,2007(2):436-440.
[11] Raffi M;Akhter JI;Hasan MM .Effect of annealing temperature on Ag nano-composite synthesized by sol-gel[J].Materials Chemistry and Physics,2006(2/3):405-409.
[12] P.K. Khanna;V.V.V.S. Subbarao .Nanosized silver powder via reduction of silver nitrate by sodium formaldehydesulfoxylate in acidic pH medium[J].Materials Letters,2003(15):2242-2245.
[13] Wu SP;Meng SY .Preparation of ultrafine silver powder using ascorbic acid as reducing agent and its application in MLCI[J].Materials Chemistry and Physics,2005(2/3):423-427.
[14] J.L.H. Chau;M.-K. Hsu;C.-C. Hsieh .Microwave plasma synthesis of silver nanopowders[J].Materials Letters,2005(8/9):905-908.
[15] R. Li;D.J. Kim;K. Yu .Study of fine silver powder from AgOH slurry by hydrothermal techniques[J].Journal of Materials Processing Technology,2003(1/3):55-59.
[16] Majumdar D. .Generation and sintering characteristics of silver-copper (II)oxide composite powders made by spray pyrolysis[J].Powder Technology,2000(1/2):76-81.
[17] 刘志宏,刘智勇,李启厚,吴厚平,张多默.喷雾热分解法制备超细银粉及其形貌控制[J].中国有色金属学报,2007(01):149-155.
上一张 下一张
上一张 下一张
计量
  • 下载量()
  • 访问量()
文章评分
  • 您的评分:
  • 1
    0%
  • 2
    0%
  • 3
    0%
  • 4
    0%
  • 5
    0%