An intercalative composite of graphite oxide (GO) as host intercalated by an object of TiO_2 nanoparticles was obtained at low temperature by mixing GO with Ti(SO_4)2 solution, and by another object of Ti_2O_3 while mixing with TiCl_4 ethanol solution. Microstructures of the GO and its intercalative composites at different C/Ti ratio were studied by XRD, SEM, AFM and FT-IR, and the evolution of these lamellar structures was studied based on the temperature change. The photocata-lytic activity of the intercalative composites was characterized according to the degradation of methyl orange. The intercalative composite formed by Ti(SO_4)2 solution presents an excellent photocatalytic reactivity, while that formed by TiCl_4 presents no observablly photocatalytic reactivity. The electric conductivity variation of different composites was checked, in order to investigate the role of the possible electron transfer between the graphite layer and TiO_2 nanocrystal during TiO_2 excited by UV light irradiation.
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