Single crystal of Li2Zn2(MoO4)(3) has been grown from a flux of Li2MoO4 by the top-seeded solution-growth method, and its structure was refined by the Rietveld method. It belongs to the orthorhombic system, space group Pnma with alpha = 5.1114, b =10.4906 and c = 17.6172 angstrom. Good agreement between the experimental and calculated profile (RP = 6.69%, R-wp = 9.73% and R-exp = 6.58%) was reached.
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