Our efforts to introduce defects in rutile by conventional mechanical grinding as used for TEM study did not produce any defects or twinning. Experimental SAED patterns of rutile with intercalated alpha-PbO2-type TiO2 lamellae are consistent with those expected from calculated patterns. The values and precision of lattice parameters of alpha-PbO2-type TiO2 derived from such SAED patterns are also consistent with crystal data from X-ray diffraction studies.
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