{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":5,"startPagecode":1},"records":[{"abstractinfo":"对经硫酸法硬质阳极氧化处理的ZL-101铸铝,采用磁控溅射法镀覆石墨镀层,将石墨微粒填充到多孔性氧化膜内以达到减摩作用.用扫描电镜(SEM)、电探波谱(WDS)和X射线光电子能谱(XPS)技术,对膜层形貌和石墨在膜层内的分布状态作了分析;用PMJ-Ⅰ型平面磨耗试验机和MM-200磨损试验机对膜层耐磨性进行了测定.结果表明,石墨离子可渗入到膜的内层,镀层结合牢固,表观光滑,膜的耐磨性得到显著提高.","authors":[{"authorName":"阎永京","id":"809623a3-29d2-48a9-bd52-62e35473f281","originalAuthorName":"阎永京"},{"authorName":"<span style=\"color:red\">祝</span><span style=\"color:red\">天</span><span style=\"color:red\">舒</span>","id":"a34d2b3b-3a1c-4def-a5b2-f0689babb303","originalAuthorName":"祝天舒"},{"authorName":"寿汉章","id":"a9216700-78aa-4ac1-b0b3-7fcb34f57174","originalAuthorName":"寿汉章"}],"doi":"10.3969/j.issn.1005-748X.2000.07.001","fpage":"291","id":"c1bad237-7e38-44ea-808b-98515d41fabe","issue":"7","journal":{"abbrevTitle":"FSYFH","coverImgSrc":"journal/img/cover/FSYFH.jpg","id":"25","issnPpub":"1005-748X","publisherId":"FSYFH","title":"腐蚀与防护"},"keywords":[{"id":"e3c15fad-edd7-4e16-b56b-8f46d7cad35c","keyword":"铝阳极氧化膜","originalKeyword":"铝阳极氧化膜"},{"id":"b842d4cb-1cb4-4ac5-94c5-dab92617aeb3","keyword":"磁控溅射石墨","originalKeyword":"磁控溅射石墨"},{"id":"f8d30479-d214-4f6e-8213-5cfc4790c653","keyword":"耐磨性","originalKeyword":"耐磨性"},{"id":"b8cea1d8-01aa-462a-8e5e-ab04247d0905","keyword":"质量和厚度损失","originalKeyword":"质量和厚度损失"},{"id":"7242d97b-3f4f-4e2a-8c93-82dccd2f7046","keyword":"摩擦系数","originalKeyword":"摩擦系数"}],"language":"zh","publisherId":"fsyfh200007001","title":"磁控溅射石墨镀层的减摩性能","volume":"21","year":"2000"},{"abstractinfo":"应用反相高效液相色谱外标定量法同时测定了<span style=\"color:red\">舒</span>普深中的<span style=\"color:red\">舒</span>巴坦钠和头孢哌酮钠.采用pH4.0的磷酸水溶液-乙腈(体积比为80:20)组成的流动相,在ODS柱上,于12min内同时测定<span style=\"color:red\">舒</span>巴坦钠和头孢哌酮钠.方法简单,重现性好,在线性范围内<span style=\"color:red\">舒</span>巴坦钠的相关系数为0.999(n=5),头孢哌酮钠的相关系数为0.9991(n=5).方法适于对药品<span style=\"color:red\">舒</span>普深的生产过程及临床上该药的血药浓度的监测.","authors":[{"authorName":"李发胜","id":"a3f48b51-f1df-4417-b7d4-8447c9935c2b","originalAuthorName":"李发胜"},{"authorName":"徐智秀","id":"2b033849-c355-46dd-b0ac-61ffb6007499","originalAuthorName":"徐智秀"},{"authorName":"肖红斌","id":"d27aefce-e9ae-41b3-a569-4cbd0ed693d2","originalAuthorName":"肖红斌"},{"authorName":"梁鑫淼","id":"6cdad3e5-17a8-4c8a-bcac-0df3f1738f4a","originalAuthorName":"梁鑫淼"}],"doi":"10.3321/j.issn:1000-8713.2000.06.011","fpage":"525","id":"5ee3304b-2a61-42fe-a871-86a4e6c0a05c","issue":"6","journal":{"abbrevTitle":"SP","coverImgSrc":"journal/img/cover/SP.jpg","id":"58","issnPpub":"1000-8713","publisherId":"SP","title":"色谱 "},"keywords":[{"id":"5b6b3c3e-fdb2-43c2-8232-5f72cd2d1ce0","keyword":"高效液相色谱法","originalKeyword":"高效液相色谱法"},{"id":"67a09548-bc6a-4e95-8258-bbacca468ac3","keyword":"<span style=\"color:red\">舒</span>普深","originalKeyword":"舒普深"},{"id":"9831ef9d-7a2a-46f9-bb52-9914d420e0a8","keyword":"<span style=\"color:red\">舒</span>巴坦钠","originalKeyword":"舒巴坦钠"},{"id":"2867daa3-2305-4af3-9a23-2f0996b682b1","keyword":"头孢哌酮钠","originalKeyword":"头孢哌酮钠"}],"language":"zh","publisherId":"sp200006011","title":"高效液相色谱法测定<span style=\"color:red\">舒</span>普深中的<span style=\"color:red\">舒</span>巴坦钠和头孢哌酮钠","volume":"18","year":"2000"},{"abstractinfo":"应用ELTRAOH900氧氢测定仪,高纯N2作载气,测定钛中氢含量,对是否需要<span style=\"color:red\">舒</span>茨试剂对样品气中CO净化并使用碱石棉去除进行了实验研究.结果表明,样品气中CO净化和不净化两种条件下测定钛参比物质中氢含量的测定值相对误差(准确度)几乎相同.证明样品气中CO不会干扰氢的测定,无需<span style=\"color:red\">舒</span>茨试剂净化样品气.","authors":[{"authorName":"张长均","id":"c318a811-89e9-4929-90ad-6abcd3c60245","originalAuthorName":"张长均"},{"authorName":"王蓬","id":"00cb3324-3bc3-4fa3-9361-7da9dd25d708","originalAuthorName":"王蓬"},{"authorName":"杨植岗","id":"efd17461-60b4-4a69-a78d-7b7e7666c71e","originalAuthorName":"杨植岗"},{"authorName":"张之果","id":"2c2df745-5544-473b-8a4e-e91b7ffee232","originalAuthorName":"张之果"},{"authorName":"杜学强","id":"a9e3f0f6-459f-4ccd-a077-ebf62a9d0291","originalAuthorName":"杜学强"}],"doi":"10.3969/j.issn.1000-7571.2004.z1.114","fpage":"366","id":"87c31895-8c16-4f5b-bc5e-d7849b9e6c17","issue":"z1","journal":{"abbrevTitle":"YJFX","coverImgSrc":"journal/img/cover/YJFX.jpg","id":"71","issnPpub":"1000-7571","publisherId":"YJFX","title":"冶金分析   "},"keywords":[{"id":"4b2a9925-c0fd-44ec-8d23-42049fac8edf","keyword":"钛","originalKeyword":"钛"},{"id":"44ab7581-bb82-49ac-b9cf-f0f40ba1be5e","keyword":"氢","originalKeyword":"氢"},{"id":"342a7b46-2756-4248-93c6-82203befaac6","keyword":"<span style=\"color:red\">舒</span>茨试剂","originalKeyword":"舒茨试剂"}],"language":"zh","publisherId":"yjfx2004z1114","title":"无<span style=\"color:red\">舒</span>茨试剂测定钛中氢","volume":"24","year":"2004"},{"abstractinfo":"在KH2PO4-Na2HPO4(pH 6.24±0.1)支持电解质中,N-(4-硝基-2-苯氧基苯基)(尼美<span style=\"color:red\">舒</span>利,nimesulide)甲基磺酰胺产生1个催化氢波,峰电位Ep=-1.20 V(vs.SCE).加入K2S2O8后,该催化氢波被催化,峰电流增加约20倍,峰电位基本不变,产生1个较灵敏的平行催化氢波.其二阶导数峰峰电流i\"p与尼美<span style=\"color:red\">舒</span>利浓度在4.0×10-7～8.0×10-6 mol/L范围内呈线性关系(r=0.988 6,n=9),检出限为2.0×10-7 mol/L.该方法可用于药物制剂中尼美<span style=\"color:red\">舒</span>利含量的测定.","authors":[{"authorName":"马淮凌","id":"b0afb74a-e052-40c8-a8ce-3c08768f3051","originalAuthorName":"马淮凌"},{"authorName":"凌翠霞","id":"28aa9641-fc22-4bd4-8ed9-ee06f70ab7a7","originalAuthorName":"凌翠霞"},{"authorName":"马啸华","id":"fc9616a2-ddb4-4da9-b36e-f820760a6f27","originalAuthorName":"马啸华"}],"doi":"10.3969/j.issn.1000-0518.2006.12.012","fpage":"1359","id":"6deae94c-734d-4585-a81f-427bbeeec9ef","issue":"12","journal":{"abbrevTitle":"YYHX","coverImgSrc":"journal/img/cover/YYHX.jpg","id":"73","issnPpub":"1000-0518","publisherId":"YYHX","title":"应用化学"},"keywords":[{"id":"4236660c-7b16-4adf-814c-acbe163cfbc1","keyword":"尼美<span style=\"color:red\">舒</span>利","originalKeyword":"尼美舒利"},{"id":"6681b759-7a36-43f0-9233-8120361cdfe4","keyword":"过二硫酸钾","originalKeyword":"过二硫酸钾"},{"id":"c18277a6-bbee-4e3f-a2f1-28d167eef015","keyword":"催化氢波","originalKeyword":"催化氢波"},{"id":"915591ba-e083-4071-bd98-a558d0d02530","keyword":"平行催化氢波","originalKeyword":"平行催化氢波"}],"language":"zh","publisherId":"yyhx200612012","title":"平行催化氢波法测定非甾体抗炎药尼美<span style=\"color:red\">舒</span>利","volume":"23","year":"2006"},{"abstractinfo":"对空间目标的监视可采用地基和<span style=\"color:red\">天</span>基两种方式实现.与地基观测相比,<span style=\"color:red\">天</span>基观测在空域覆盖性和监视时效性等方面具有较大优势,空间目标<span style=\"color:red\">天</span>基观测技术已成为当今空间领域的前沿性技术.目前,许多国家和组织都在大力发展空间目标<span style=\"color:red\">天</span>基观测技术.<span style=\"color:red\">天</span>基光学观测可采用光学栅栏、特定<span style=\"color:red\">天</span>区和地球同步带搜索方式实现空间目标的捕获;可通过恒星跟踪和天文定位方法获取空间目标的位置信息;可采用等待或跟踪方式实现对目标的成像.","authors":[{"authorName":"余建慧","id":"96199efd-c88d-4b6b-8690-120ba34da506","originalAuthorName":"余建慧"},{"authorName":"苏增立","id":"ccac5121-ad38-4bf7-9bf0-dd1498fab18a","originalAuthorName":"苏增立"},{"authorName":"谭谦","id":"adcac790-b419-4c96-83ac-85f78e09fa2b","originalAuthorName":"谭谦"}],"doi":"10.3969/j.issn.1007-5461.2006.06.004","fpage":"772","id":"5b22ea07-9137-433c-bd31-fe360dfbc619","issue":"6","journal":{"abbrevTitle":"LZDZXB","coverImgSrc":"journal/img/cover/LZDZXB.jpg","id":"53","issnPpub":"1007-5461","publisherId":"LZDZXB","title":"量子电子学报   "},"keywords":[{"id":"7966825d-0420-4da9-9c3d-389d69e96339","keyword":"遥感","originalKeyword":"遥感"},{"id":"796b314e-8e99-4f43-99f8-9415d1030654","keyword":"<span style=\"color:red\">天</span>基光学观测","originalKeyword":"天基光学观测"},{"id":"b643794a-cce6-4209-9dc3-4ff2294ccc88","keyword":"光学探测","originalKeyword":"光学探测"},{"id":"89dcd054-7177-418a-84da-31791ef3d535","keyword":"光学成像","originalKeyword":"光学成像"}],"language":"zh","publisherId":"lzdzxb200606004","title":"空间目标<span style=\"color:red\">天</span>基光学观测模式分析","volume":"23","year":"2006"},{"abstractinfo":"安钢炼铁厂7#高炉主卷扬上料系统关键设备--<span style=\"color:red\">天</span>轮,在安装使用不久出现轴承严重损坏,造成高炉不能正常上料.经过对<span style=\"color:red\">天</span>轮内部结构及轴承本身等方面进行改进后,取得了良好的使用效果.","authors":[{"authorName":"李增生","id":"0f379bff-d466-464e-a023-f9e6576365f3","originalAuthorName":"李增生"},{"authorName":"王义","id":"ecb5191f-2f39-43d0-840c-2889bba44dc9","originalAuthorName":"王义"},{"authorName":"陈先利","id":"33e87cb5-6378-49b5-9a09-4aaadb9d3599","originalAuthorName":"陈先利"},{"authorName":"秦国良","id":"4b1d8cc1-945c-4a17-a91c-73aaca2f36a5","originalAuthorName":"秦国良"}],"doi":"10.3969/j.issn.1000-6826.2009.06.018","fpage":"54","id":"4a55bc01-6e55-4a6a-88c0-5699f33b01f2","issue":"6","journal":{"abbrevTitle":"JSSJ","coverImgSrc":"journal/img/cover/3abe017a-2574-4821-8152-4ae974ef0471.jpg","id":"47","issnPpub":"1000-6826","publisherId":"JSSJ","title":"金属世界"},"keywords":[{"id":"a70ed3d8-9383-4e11-9f91-a92e5dac1c47","keyword":"高炉","originalKeyword":"高炉"},{"id":"dcbb1649-aa16-4fd1-abce-26e059778aa9","keyword":"<span style=\"color:red\">天</span>轮","originalKeyword":"天轮"},{"id":"938596bc-273e-451a-ac55-d92df79be10c","keyword":"轴承","originalKeyword":"轴承"},{"id":"ad31f801-1014-4186-bf39-a7b2f8959ab9","keyword":"润滑","originalKeyword":"润滑"}],"language":"zh","publisherId":"jssj200906018","title":"高炉<span style=\"color:red\">天</span>轮轴承损坏原因分析与处理","volume":"","year":"2009"},{"abstractinfo":"建立了柴胡<span style=\"color:red\">舒</span>肝丸(Chaihu Shugan Pill,CHSGP)的毛细管区带电泳指纹图谱(capillary electrophoresis fingerprint,CEFP),并采用内标法测定了黄芩苷的含量.以50 mmol/L 硼砂-150 mmol/L 磷酸二氢钠-50 mmol/L 磷酸氢二钠(1:1:1,v/v/v)(含5 mmol/L庚烷磺酸钠)为背景电解质(BGE)溶液,采用未涂层石英毛细管(总长度75 cm,有效分离长度63 cm,内径75 μm),以色谱指纹图谱分离量指数(RF)为目标函数优化实验条件,在紫外检测波长265 nm、运行电压11 kV条件下,以黄芩苷峰为参照物峰,确定了22个共有指纹峰,建立了CHSGP的CEFP,通过对20批样品聚类分析确定用其中13批生成对照CEFP(RCEFP),以此RCEFP为标准用系统指纹定量法鉴别20批柴胡<span style=\"color:red\">舒</span>肝丸质量.结果其中的4批化学成分数量和分布比例不合格,4批含量明显偏低,其他12批完全合格.采用内标法测定黄芩苷的含量,在5～200 mg/L范围内线性良好(r=0.999.9),平均回收率(n=9)为98.2%.该法具有较好的精密度和重现性,为柴胡<span style=\"color:red\">舒</span>肝丸的质量控制提供了一种新的参考.","authors":[{"authorName":"孙国祥","id":"b7cbe884-4dc4-4384-98a3-0dbeb14c99ef","originalAuthorName":"孙国祥"},{"authorName":"闫娜娜","id":"63d6f50c-85a5-4b97-abc7-a0761fdc8934","originalAuthorName":"闫娜娜"},{"authorName":"丁国瑜","id":"e9e8271a-8e86-48bb-b074-bbbcb5130b4c","originalAuthorName":"丁国瑜"}],"doi":"10.3724/SP.J.1123.2010.01077","fpage":"1077","id":"5c189380-25d4-494b-9438-987f08d6d3be","issue":"11","journal":{"abbrevTitle":"SP","coverImgSrc":"journal/img/cover/SP.jpg","id":"58","issnPpub":"1000-8713","publisherId":"SP","title":"色谱 "},"keywords":[{"id":"cea52fe8-7d62-4b4b-acc0-53a428d8610d","keyword":"毛细管电泳","originalKeyword":"毛细管电泳"},{"id":"1badf2a0-f075-421a-b924-230a13f5c887","keyword":"指纹图谱","originalKeyword":"指纹图谱"},{"id":"3e22215b-abd7-49d2-94d0-a9a68d96945a","keyword":"三角形优化法","originalKeyword":"三角形优化法"},{"id":"2eb89951-a07c-4b82-b587-92596783eb50","keyword":"四面体优化法","originalKeyword":"四面体优化法"},{"id":"ab244bae-2319-4c4e-957e-eec96574fb1c","keyword":"系统指纹定量法","originalKeyword":"系统指纹定量法"},{"id":"57516392-4abf-485a-871d-4432af97c1cf","keyword":"色谱指纹图分离量指数","originalKeyword":"色谱指纹图分离量指数"},{"id":"87ac5326-574a-48c5-9d67-3cdb2f41dca0","keyword":"黄芩苷","originalKeyword":"黄芩苷"},{"id":"a0074350-51c8-4fc0-a461-10de7f30593e","keyword":"柴胡<span style=\"color:red\">舒</span>肝丸","originalKeyword":"柴胡舒肝丸"}],"language":"zh","publisherId":"sp201011014","title":"柴胡<span style=\"color:red\">舒</span>肝丸的毛细管电泳指纹图谱及其黄芩苷含量的测定","volume":"28","year":"2010"},{"abstractinfo":"应用反相高效液相色谱法检测了肾<span style=\"color:red\">舒</span>冲剂水煎液中的小檗碱.样品经超声提取后,以C18化学键合硅胶为固定相,乙腈-0.04 mol/L H3PO4(体积比为42:58)为流动相,用349 nm的波长定量检测.测定结果表明,小檗碱的质量浓度在1.2～19.2 mg/L 范围内线性良好,最低检测限为0.6 mg/L, 测定批内(n=5)及批间(n=5)相对标准偏差分别为0.6%～3.5%和5 .3%～6.5%, 回收率为89.10%～91.35%.","authors":[{"authorName":"王曙东","id":"5e671a7b-97d3-4642-9d1c-0105daf0bb1c","originalAuthorName":"王曙东"},{"authorName":"宋炳生","id":"3cffed2d-4f9f-4274-bf49-4b47a2f55106","originalAuthorName":"宋炳生"},{"authorName":"李克","id":"664645e6-142c-4e6f-ac0a-bb0d1fa01db1","originalAuthorName":"李克"}],"doi":"10.3321/j.issn:1000-8713.2000.03.019","fpage":"261","id":"5ed1ff78-6040-4ed2-bc82-127e2432b93a","issue":"3","journal":{"abbrevTitle":"SP","coverImgSrc":"journal/img/cover/SP.jpg","id":"58","issnPpub":"1000-8713","publisherId":"SP","title":"色谱 "},"keywords":[{"id":"eb9c4435-5f41-4b10-a92a-f5215ba6f14d","keyword":"高效液相色谱法","originalKeyword":"高效液相色谱法"},{"id":"047f5ef6-7605-440a-b641-fa13cfb533de","keyword":"小檗碱","originalKeyword":"小檗碱"},{"id":"4675b2af-6aa6-43a2-ab71-f943346d9463","keyword":"肾<span style=\"color:red\">舒</span>冲剂","originalKeyword":"肾舒冲剂"}],"language":"zh","publisherId":"sp200003019","title":"反相高效液相色谱法测定肾<span style=\"color:red\">舒</span>冲剂水煎液中的小檗碱","volume":"18","year":"2000"},{"abstractinfo":"介绍了印度<span style=\"color:red\">天</span>普乐粉矿的烧结、冶金性能试验研究情况及<span style=\"color:red\">天</span>普乐粉矿在马钢烧结和炼铁生产中的应用实践.","authors":[{"authorName":"蒋定中","id":"95062ffa-e121-4701-bff0-da708c83be65","originalAuthorName":"蒋定中"},{"authorName":"王富生","id":"1d432e15-eb16-438c-a76a-88247c01631f","originalAuthorName":"王富生"}],"doi":"","fpage":"1","id":"9253f165-d4f3-48dc-994c-489fd74291f7","issue":"3","journal":{"abbrevTitle":"GT","coverImgSrc":"journal/img/cover/GT.jpg","id":"27","issnPpub":"0449-749X","publisherId":"GT","title":"钢铁"},"keywords":[{"id":"fe2a4888-8360-4907-b54a-56c79f531e06","keyword":"<span style=\"color:red\">天</span>普乐粉矿","originalKeyword":"天普乐粉矿"},{"id":"d4431887-c833-43c4-ab72-659c1c4605e8","keyword":"烧结试验","originalKeyword":"烧结试验"},{"id":"697c2e0d-6052-461f-a227-d7376e9153b1","keyword":"生产实践","originalKeyword":"生产实践"},{"id":"ca57ca38-f264-4266-9a55-1ee38ba3fb01","keyword":"降低成本","originalKeyword":"降低成本"}],"language":"zh","publisherId":"gt199903001","title":"印度<span style=\"color:red\">天</span>普乐粉矿烧结试验研究与生产实践","volume":"","year":"1999"},{"abstractinfo":"辽宁<span style=\"color:red\">天</span>利金业有限责任公司投资300余万元,对原供热系统进行改造.通过余热回收机组充分利用生产过程中产生的生物质能,满足了公司冬季生产及生活供暖,提高了可再生能源使用效率,降低企业能源成本,改善了周边的环境质量.该回收机组环保、节能、运行可靠,年节约成本约83万元,减少CO2排放量约2300t,经济效益、环保效益和社会效益显著.","authors":[{"authorName":"徐建龙","id":"449d5f33-4ea1-45fb-8291-ff3460993a69","originalAuthorName":"徐建龙"},{"authorName":"刘子龙","id":"51a6d9bf-961a-4b97-a6c5-c8feccf6a3ff","originalAuthorName":"刘子龙"},{"authorName":"徐春华","id":"1ecaef7e-0f0b-44a6-9e13-f0b1e5c00fb6","originalAuthorName":"徐春华"}],"doi":"10.3969/j.issn.1001-1277.2010.08.001","fpage":"1","id":"cf4c6e26-7ce4-49c5-88de-eb2c6784066d","issue":"8","journal":{"abbrevTitle":"HJ","coverImgSrc":"journal/img/cover/HJ.jpg","id":"44","issnPpub":"1001-1277","publisherId":"HJ","title":"黄金"},"keywords":[{"id":"a079652f-f451-416f-8087-a0d049e0c31a","keyword":"余热","originalKeyword":"余热"},{"id":"0a779894-00b6-4282-acfa-958afd77ce47","keyword":"生物质能","originalKeyword":"生物质能"},{"id":"934fb808-d3e4-44ac-8a5d-b7fd43df8628","keyword":"低碳","originalKeyword":"低碳"},{"id":"b15bd9a0-9d48-42b2-89ff-fddaeaa6a30a","keyword":"<span style=\"color:red\">天</span>利公司","originalKeyword":"天利公司"}],"language":"zh","publisherId":"huangj201008001","title":"<span style=\"color:red\">天</span>利公司生物质能的应用实践","volume":"31","year":"2010"}],"totalpage":51,"totalrecord":508}