{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":5,"startPagecode":1},"records":[{"abstractinfo":"采用自由共聚的方法合成了一种温敏性水凝胶,分析了不同质量分数凝胶的低临界溶解温度(LCST)和粘度变化,分别采用水、浙江大学胶体<span style=\"color:red\">灭火</span>剂B和温敏性水凝胶对1A堆垛进行<span style=\"color:red\">灭火</span>实验,通过辐射热探头和热电偶分别对<span style=\"color:red\">灭火</span>过程中的辐射热和温度变化进行采集,结果表明在相同的供给强度下,温敏性水凝胶<span style=\"color:red\">灭火</span>剂的<span style=\"color:red\">灭火</span>时间最短,消耗的<span style=\"color:red\">灭火</span>剂用量最少,<span style=\"color:red\">灭火</span>后所产生的水渍损失最小,而且<span style=\"color:red\">灭火</span>后火场残留物易于清理,通过对<span style=\"color:red\">灭火</span>过程中的危险气体进行检测,结果表明没有额外毒害气体产生.","authors":[{"authorName":"贾春雷","id":"bebd5034-f1b8-4e6c-b438-13f305a831b1","originalAuthorName":"贾春雷"},{"authorName":"蒋仲安","id":"610f2526-4b14-42b7-b3a5-e99907540a69","originalAuthorName":"蒋仲安"},{"authorName":"杨漪","id":"8d5e2b8c-c6d5-4c71-88b3-587b5d28ac1d","originalAuthorName":"杨漪"},{"authorName":"唐凯","id":"005f4371-80fe-4365-9671-ecd911e020c5","originalAuthorName":"唐凯"}],"doi":"10.3969/j.issn.1001-9731.2013.11.017","fpage":"1593","id":"4a7566ad-99fa-45e7-8e60-80f63e039dc4","issue":"11","journal":{"abbrevTitle":"GNCL","coverImgSrc":"journal/img/cover/GNCL.jpg","id":"33","issnPpub":"1001-9731","publisherId":"GNCL","title":"功能材料"},"keywords":[{"id":"7fa38ddf-fcdb-400c-aefe-023359f3ef7a","keyword":"温敏性","originalKeyword":"温敏性"},{"id":"0406e438-7921-4d16-94aa-75740a20f113","keyword":"水凝胶","originalKeyword":"水凝胶"},{"id":"3f00f9fa-df62-4269-b373-0e70e6df9f45","keyword":"低临界溶解温度","originalKeyword":"低临界溶解温度"},{"id":"a7db70a2-5cda-40f6-a219-e8fc717c7f56","keyword":"<span style=\"color:red\">灭火</span>剂","originalKeyword":"灭火剂"},{"id":"e5117865-4c99-4e37-8055-7881b2d026f7","keyword":"<span style=\"color:red\">灭火</span><span style=\"color:red\">效率</span>","originalKeyword":"灭火效率"}],"language":"zh","publisherId":"gncl201311017","title":"温敏性高分子水凝胶制备及<span style=\"color:red\">灭火</span>性能研究","volume":"44","year":"2013"},{"abstractinfo":"采用实验模拟的方法,研究了添加氯化亚铁的细水雾在不同添加剂浓度、不同喷头压力下,熄灭不同性质的液体池火的性能.实验结果表明:添加有氯化亚铁的细水雾,其<span style=\"color:red\">灭火</span>性能发生了显著变化.存在一个最佳的<span style=\"color:red\">灭火</span>浓度,其对应的<span style=\"color:red\">灭火</span>时间最短,耗水量最少,<span style=\"color:red\">灭火</span><span style=\"color:red\">效率</span>最高.细水雾喷头的工作压力和燃料的性质也对细水雾的<span style=\"color:red\">灭火</span>性能有影响:工作压力越大,细水雾的平均<span style=\"color:red\">灭火</span>时间越短.在相同的实验条件下,细水雾扑灭煤油池火的时间要短于扑灭酒精池火的时间.","authors":[{"authorName":"廖光煊","id":"f9247a5a-f734-46c7-96fc-4bf7ec3a166b","originalAuthorName":"廖光煊"},{"authorName":"丛北华","id":"159dfea2-65be-465a-be29-91d30ce55bb7","originalAuthorName":"丛北华"},{"authorName":"况凯骞","id":"2c303c46-24e6-4ecb-8c48-6f1787a80250","originalAuthorName":"况凯骞"}],"doi":"","fpage":"273","id":"7a81a116-d076-4ab8-810f-5b68b5cc69ab","issue":"z1","journal":{"abbrevTitle":"GCRWLXB","coverImgSrc":"journal/img/cover/GCRWLXB.jpg","id":"32","issnPpub":"0253-231X","publisherId":"GCRWLXB","title":"工程热物理学报   "},"keywords":[{"id":"68738121-dfb8-41f8-9466-634d4b8e7000","keyword":"细水雾","originalKeyword":"细水雾"},{"id":"50087d80-433a-4b1d-ac55-46337fe9bd56","keyword":"氯化亚铁添加剂","originalKeyword":"氯化亚铁添加剂"},{"id":"f341030e-ae11-4b84-87de-ad69137e8156","keyword":"油池火","originalKeyword":"油池火"},{"id":"af7e15af-c409-4cff-b498-dcc3ec550e71","keyword":"<span style=\"color:red\">灭火</span>性能","originalKeyword":"灭火性能"}],"language":"zh","publisherId":"gcrwlxb2005z1071","title":"铁基添加剂增强细水雾<span style=\"color:red\">灭火</span>性能的实验研究","volume":"26","year":"2005"},{"abstractinfo":"某型号干粉<span style=\"color:red\">灭火</span>器在充填作业中发生爆炸事故。综合分析事故现场，并利用裂纹分析、断口分析、材料分析及力学分析表明：该<span style=\"color:red\">灭火</span>器材料合格，充填作业正常，爆炸的原因在于<span style=\"color:red\">灭火</span>器存在较严重的加工工艺缺陷，在简体底部的不正常环向旋压损伤致使该部位局部厚度仅为其他部位的50％，并形成环状尖缺口缺陷，造成应力集中，局部高应力导致了低应力爆炸事故的发生。","authors":[{"authorName":"王长利","id":"16214253-c58a-440d-85c2-360c57be32f4","originalAuthorName":"王长利"},{"authorName":"赵承杰","id":"1fa80b82-9da2-4a1d-808b-688782fb2dc4","originalAuthorName":"赵承杰"}],"doi":"10.3969/j.issn.1001-0777.2003.02.012","fpage":"30","id":"e7b1eae6-2d80-454e-8d85-6acc1a0d3cab","issue":"2","journal":{"abbrevTitle":"WLCS","coverImgSrc":"journal/img/cover/WLCS.jpg","id":"64","issnPpub":"1001-0777","publisherId":"WLCS","title":"物理测试"},"keywords":[{"id":"fc371fb7-eff3-4abc-a29e-c868acffc968","keyword":"脆性裂纹","originalKeyword":"脆性裂纹"},{"id":"dcc20da4-9013-4dab-9be2-e840e652beb8","keyword":"爆炸","originalKeyword":"爆炸"},{"id":"a53cb1ca-6ccb-41db-8753-3a7d584b3c45","keyword":"硬化","originalKeyword":"硬化"},{"id":"f9be820b-a2ed-4fc2-b3dd-5012f6f9d679","keyword":"缺口敏感性","originalKeyword":"缺口敏感性"}],"language":"zh","publisherId":"wlcs200302012","title":"<span style=\"color:red\">灭火</span>器爆炸事故分析","volume":"","year":"2003"},{"abstractinfo":"作为一种环保型高效的<span style=\"color:red\">灭火</span>剂,气溶胶<span style=\"color:red\">灭火</span>剂越来越受到世界各国科研人员的重视,特别是近30年来人们对其进行了较为深入的研究和应用开发.综述了气溶胶<span style=\"color:red\">灭火</span>剂的类型、<span style=\"color:red\">灭火</span>机理、使用效果以及当今气溶胶<span style=\"color:red\">灭火</span>剂的主要研究方向,分析了最新气溶胶<span style=\"color:red\">灭火</span>产品的性能和原理,并展望了气溶胶<span style=\"color:red\">灭火</span>剂的发展前景.","authors":[{"authorName":"邢军","id":"3ac379b4-099d-4afd-83c7-33a41ab0d076","originalAuthorName":"邢军"},{"authorName":"杜志明","id":"3aed5071-b90e-4101-b703-3e1f5a84324c","originalAuthorName":"杜志明"},{"authorName":"阿苏娜","id":"2bb3ccd6-a76e-48a6-8e6b-87277b1a3947","originalAuthorName":"阿苏娜"}],"doi":"","fpage":"69","id":"c568060c-8e21-4ce9-910f-efb9a26a62f0","issue":"9","journal":{"abbrevTitle":"CLDB","coverImgSrc":"journal/img/cover/CLDB.jpg","id":"8","issnPpub":"1005-023X","publisherId":"CLDB","title":"材料导报"},"keywords":[{"id":"e3991abc-af22-4704-92b1-ca3a224deb7c","keyword":"气溶胶<span style=\"color:red\">灭火</span>剂","originalKeyword":"气溶胶灭火剂"},{"id":"5f748804-ecb5-4527-94e0-7f87328054dd","keyword":"消防","originalKeyword":"消防"},{"id":"01b114d4-80c6-4ab5-86a0-e1a6ac5673c1","keyword":"综述","originalKeyword":"综述"}],"language":"zh","publisherId":"cldb200809019","title":"气溶胶<span style=\"color:red\">灭火</span>剂的研究进展","volume":"22","year":"2008"},{"abstractinfo":"通过扫描电镜、能谱仪等手段对失效的运五飞机<span style=\"color:red\">灭火</span>瓶管嘴断裂进行断口形貌、化学成分和金相组织分析.结果表明,该<span style=\"color:red\">灭火</span>瓶管嘴断裂是由于应力腐蚀开裂引起的;根据分析结果,提出了预防措施.","authors":[{"authorName":"王在俊","id":"920b09d5-04e7-49b9-8038-ffcea52e274c","originalAuthorName":"王在俊"},{"authorName":"刘显超","id":"a29b1b8a-f3f6-4777-8583-06c65650d5d0","originalAuthorName":"刘显超"}],"doi":"10.3969/j.issn.1002-6495.2007.05.019","fpage":"377","id":"132c8a6b-4f99-4f15-b6f2-d3782b754b90","issue":"5","journal":{"abbrevTitle":"FSXB","coverImgSrc":"journal/img/cover/腐蚀学报封面.jpg","id":"24","issnPpub":"2667-2669","publisherId":"FSXB","title":"腐蚀学报（英文）"},"keywords":[{"id":"3b153524-741f-4c9c-82a4-4d6274bd6249","keyword":"<span style=\"color:red\">灭火</span>瓶管嘴","originalKeyword":"灭火瓶管嘴"},{"id":"acd129a9-eda5-4b91-939a-a1201956db2d","keyword":"断裂","originalKeyword":"断裂"},{"id":"546a1e7e-0153-4833-8916-90311c1809db","keyword":"失效分析","originalKeyword":"失效分析"},{"id":"43d93b74-f472-4e8b-a6ee-8abffc8f139d","keyword":"应力腐蚀","originalKeyword":"应力腐蚀"}],"language":"zh","publisherId":"fskxyfhjs200705019","title":"运五飞机<span style=\"color:red\">灭火</span>瓶管嘴断裂的失效分析","volume":"19","year":"2007"},{"abstractinfo":"采用喷雾干燥和原位改性的方法制得超细球形空心疏水的磷酸二氢铵(NH4H2PO4)<span style=\"color:red\">灭火</span>粉.结果表明:在干燥气体进12温度为180,200℃和220℃的情况下所制得的粉体均为NH4H2PO4.在没有添加羧甲基纤维素钠(CMC)的情况下,非球形颗粒较多.当CMC的添加量分别为0.5%和1.0%质量分数时,制得的颗粒球形度高,空心颗粒增多.随着CMC添加量的增加,粉体的堆积密度减少.提高粉体疏水性理想的硅油乳液添加量为9%质量分数.颗粒的疏水性增加是由于干燥过程中硅油乳液迁移到颗粒表面的缘故.<span style=\"color:red\">灭火</span>实验结果表明:喷雾干燥制得的超细球形空心NH4H2PO4<span style=\"color:red\">灭火</span>粉的<span style=\"color:red\">灭火</span>效能得到提高.","authors":[{"authorName":"傅宪辉","id":"32f9837a-1c04-4e28-b23a-42f0de71aae1","originalAuthorName":"傅宪辉"},{"authorName":"沈志刚","id":"ccfb0999-46c1-4013-9c29-1504c7620369","originalAuthorName":"沈志刚"},{"authorName":"蔡楚江","id":"d3312ba5-8f9f-428f-a988-f62327e36fe1","originalAuthorName":"蔡楚江"},{"authorName":"麻树林","id":"eb2403a6-4ae0-48ee-beac-0d4494c6a656","originalAuthorName":"麻树林"},{"authorName":"邢玉山","id":"410be523-6764-45e6-b7d2-ad514387bb77","originalAuthorName":"邢玉山"}],"doi":"10.3969/j.issn.1001-4381.2008.12.016","fpage":"65","id":"3a10e656-1b2c-4b3b-8de9-acc1233900a9","issue":"12","journal":{"abbrevTitle":"CLGC","coverImgSrc":"journal/img/cover/CLGC.jpg","id":"9","issnPpub":"1001-4381","publisherId":"CLGC","title":"材料工程"},"keywords":[{"id":"ed2d16e9-d961-4d21-beee-4726fffa9c4b","keyword":"喷雾干燥","originalKeyword":"喷雾干燥"},{"id":"a968cd67-b0dc-453e-94f7-d46a4df8ffa0","keyword":"空心","originalKeyword":"空心"},{"id":"a091fa1c-bb99-4274-9bf0-3a9eb1b81728","keyword":"羧甲基纤维素钠","originalKeyword":"羧甲基纤维素钠"},{"id":"de63d95e-a9a7-4707-af5d-3dabc00408f1","keyword":"原位改性","originalKeyword":"原位改性"},{"id":"a460934f-89ab-447a-9dde-e405cfae573d","keyword":"<span style=\"color:red\">灭火</span>","originalKeyword":"灭火"}],"language":"zh","publisherId":"clgc200812016","title":"制备参数对喷雾干燥的磷铵<span style=\"color:red\">灭火</span>粉性能的影响","volume":"","year":"2008"},{"abstractinfo":"用快硬硫铝酸盐水泥、大掺量粉煤灰、水玻璃,外加悬浮剂,一步混合法制备了三元复合胶体防<span style=\"color:red\">灭火</span>材料,研究了该材料的凝结时间、抗压强度和阻化性能,观察了微观形貌,探讨了胶凝机理。结果表明,材料胶结体的初凝时间在1~30 min 范围内可控,并具有良好的早期抗压强度；60℃阻化率达90％,70℃达80％,80℃不低于75％；胶结体内部存在大量絮凝状的C-S-H 凝胶,且与粉煤灰胶连,结构密实。工业实验表明该防<span style=\"color:red\">灭火</span>材料具有良好的防<span style=\"color:red\">灭火</span>效果。","authors":[{"authorName":"赵建国","id":"d403636f-90f9-43f1-8608-1480a5282958","originalAuthorName":"赵建国"},{"authorName":"朱化雨","id":"1a4c79a9-2462-4311-8e19-987dc424948c","originalAuthorName":"朱化雨"},{"authorName":"刘晓泓","id":"27322d37-e45b-40e7-8da2-e09f435160e3","originalAuthorName":"刘晓泓"},{"authorName":"朱孔赞","id":"c9314a64-32c4-4746-9353-38da7c42a74c","originalAuthorName":"朱孔赞"},{"authorName":"冯恩娟","id":"1c9ad73c-c2d5-486e-aa7b-4bf5f4327635","originalAuthorName":"冯恩娟"},{"authorName":"陈怀成","id":"fb685a84-56aa-40a6-b13f-1989a427501e","originalAuthorName":"陈怀成"}],"doi":"10.3969/j.issn.1001-9731.2015.13.029","fpage":"13139","id":"3d0eed35-b7e9-4aff-92c5-935f2ff6622a","issue":"13","journal":{"abbrevTitle":"GNCL","coverImgSrc":"journal/img/cover/GNCL.jpg","id":"33","issnPpub":"1001-9731","publisherId":"GNCL","title":"功能材料"},"keywords":[{"id":"32e74c81-fbb9-4108-8c7b-b3e3c0d20a26","keyword":"煤自燃火灾","originalKeyword":"煤自燃火灾"},{"id":"42fb34e0-1b77-4f4a-bb6a-fc2d04686cd9","keyword":"胶体材料","originalKeyword":"胶体材料"},{"id":"8a789da3-1524-47e9-aa28-1bbfe56a3322","keyword":"防<span style=\"color:red\">灭火</span>材料","originalKeyword":"防灭火材料"},{"id":"4f427df5-e6c4-419b-82a9-2bb3c43730a9","keyword":"煤矿","originalKeyword":"煤矿"}],"language":"zh","publisherId":"gncl201513029","title":"煤矿三元复合胶体防<span style=\"color:red\">灭火</span>材料的制备与性能研究?","volume":"","year":"2015"},{"abstractinfo":"研究了超细NaHCO3与白炭黑复合粒子的制备,并对NaHCO3/SiO2复合粒子粒径、形态、结构及应用性能进行了测定与表征.结果表明,NaHCO3与白炭黑的复合,是NaHCO3被分散后复合于白炭黑的表面及其孔隙、凹陷处,并使之球形化形成结合紧密的复合粒子;复合过程中不产生新物质,强烈机械作用力,可使NaHCO3表面晶体结构发生畸变,随着复合时间增加,畸变不断向颗粒内部扩展,颗粒表面无定形化程度增加;通过复合,提高了NaHCO3粉体的分散性及其在空气中悬浮稳定性,复合粒子冷气溶胶<span style=\"color:red\">灭火</span>剂显示了很好的<span style=\"color:red\">灭火</span>效能.","authors":[{"authorName":"叶明泉","id":"5d83184f-dbcf-4fa9-acbf-5a642ca3bad9","originalAuthorName":"叶明泉"},{"authorName":"韩爱军","id":"db415243-6a6d-49e2-a1cc-8e9c68f2db69","originalAuthorName":"韩爱军"},{"authorName":"李凤生","id":"9286e8a2-bf0e-497a-a3c6-4bf6f406744f","originalAuthorName":"李凤生"}],"doi":"10.3969/j.issn.1000-0518.2004.08.013","fpage":"810","id":"4fef44b6-3e03-433c-b152-d42e5b9337e8","issue":"8","journal":{"abbrevTitle":"YYHX","coverImgSrc":"journal/img/cover/YYHX.jpg","id":"73","issnPpub":"1000-0518","publisherId":"YYHX","title":"应用化学"},"keywords":[{"id":"be879f28-f506-4bde-9be9-7b79cdc2541a","keyword":"气溶胶","originalKeyword":"气溶胶"},{"id":"adf04d65-0863-42a9-88f9-25a8e3a61d9f","keyword":"碳酸氢钠","originalKeyword":"碳酸氢钠"},{"id":"ed75dfb7-682f-4c20-963e-5ae781b86eca","keyword":"白炭黑","originalKeyword":"白炭黑"},{"id":"f66344d5-42c6-4b88-bfca-686bdfc352e9","keyword":"复合粒子","originalKeyword":"复合粒子"},{"id":"2627e492-48de-4f19-9044-7644063e467a","keyword":"干粉<span style=\"color:red\">灭火</span>剂","originalKeyword":"干粉灭火剂"}],"language":"zh","publisherId":"yyhx200408013","title":"冷气溶胶<span style=\"color:red\">灭火</span>剂用NaHCO3/白炭黑复合粒子的制备","volume":"21","year":"2004"},{"abstractinfo":"利用实验测量和Monte Carlo模拟的方法,研究了RIBLL的传输<span style=\"color:red\">效率</span>.分析了影响传输<span style=\"color:red\">效率</span>的主要因素,发现碎片的动量分布形式对传输<span style=\"color:red\">效率</span>的模拟结果有重要的影响.另外通过比较,发现大部分碎片传输<span style=\"color:red\">效率</span>的模拟结果稍大于实验测量结果,两者最大相差约几十倍,这可以帮助估算次级束流强度,指导实验设计.","authors":[{"authorName":"章学恒","id":"c82c2d21-e592-40fe-bf37-e9fc3b618223","originalAuthorName":"章学恒"},{"authorName":"孙志宇","id":"f7a7581a-a033-44f2-bf3a-7787831a2e38","originalAuthorName":"孙志宇"},{"authorName":"王猛","id":"f5f5ccd9-9756-4ff1-b6d4-f3264b572c33","originalAuthorName":"王猛"},{"authorName":"陈志强","id":"8611d5a0-e2c2-4209-a9b3-344d1bbd32c8","originalAuthorName":"陈志强"},{"authorName":"胡正国","id":"9e16ff70-3b15-4782-a942-15d2caf8a30b","originalAuthorName":"胡正国"},{"authorName":"王建松","id":"2d1a2dc9-b844-435e-80f4-d4e1dd29e982","originalAuthorName":"王建松"},{"authorName":"毛瑞士","id":"2c6981aa-3a3e-4254-96f2-129eb484dea6","originalAuthorName":"毛瑞士"},{"authorName":"张雪荧","id":"7d1ef53e-b380-4673-a8e7-78c55e72040a","originalAuthorName":"张雪荧"},{"authorName":"赵铁成","id":"9c87bceb-ab0c-436a-a200-d31cd41f61b6","originalAuthorName":"赵铁成"},{"authorName":"李琛","id":"5a8a64be-a983-4694-9310-a3d1b5c37f42","originalAuthorName":"李琛"},{"authorName":"徐瑚珊","id":"e91d2024-c096-4306-be44-69faa6400353","originalAuthorName":"徐瑚珊"},{"authorName":"肖国青","id":"9a423fba-e3f1-4f2b-99b1-1cd225d92a57","originalAuthorName":"肖国青"},{"authorName":"袁小华","id":"698fa213-7d1b-46d1-aa52-c7c0da3ac5e6","originalAuthorName":"袁小华"},{"authorName":"徐志国","id":"e3e64c31-45f6-4150-836e-96772a2c8ff6","originalAuthorName":"徐志国"},{"authorName":"陈若富","id":"e99071a2-b9f3-4bee-9732-c6adafe3f22b","originalAuthorName":"陈若富"},{"authorName":"郭忠言","id":"be3d5f13-20f7-4664-95aa-b318eb6ca29f","originalAuthorName":"郭忠言"},{"authorName":"王玥","id":"8ce2f105-165e-406d-a84c-ea0fa8736262","originalAuthorName":"王玥"},{"authorName":"黄天衡","id":"e4ddf9e4-8a50-4dd8-aff2-6fd1b18e2a62","originalAuthorName":"黄天衡"},{"authorName":"张宏斌","id":"ab590c52-4810-43ce-b0ab-176c046ce053","originalAuthorName":"张宏斌"}],"doi":"","fpage":"203","id":"a16158e4-4023-4d5a-9436-abd42c3ad748","issue":"3","journal":{"abbrevTitle":"YZHWLPL","coverImgSrc":"journal/img/cover/YZHWLPL.jpg","id":"78","issnPpub":"1007-4627","publisherId":"YZHWLPL","title":"原子核物理评论   "},"keywords":[{"id":"cbde528c-a5e2-48c5-8ce1-afa3cdf6ec2e","keyword":"RIBLL","originalKeyword":"RIBLL"},{"id":"2b516902-7e10-499e-82ba-89030751b69e","keyword":"传输<span style=\"color:red\">效率</span>","originalKeyword":"传输效率"},{"id":"6fc51a2c-9f6d-48a1-a186-41e6111350ca","keyword":"MoCADl","originalKeyword":"MoCADl"},{"id":"03b09bf9-ae9c-4f59-ac40-ff79253b8ba0","keyword":"LISE++","originalKeyword":"LISE++"}],"language":"zh","publisherId":"yzhwlpl200903006","title":"RIBLL传输<span style=\"color:red\">效率</span>研究","volume":"26","year":"2009"},{"abstractinfo":"建立了一种高效液相色谱-串联质谱(HPLC-MS/MS)测定泡沫<span style=\"color:red\">灭火</span>材料、洗涤剂以及织物整理剂中全氟辛烷磺酸及其盐(PFOS)的方法.对应产品中的PFOS用水超声提取后,经固相萃取柱淋洗萃取,萃取液以乙腈-10 mmol/L 乙酸铵溶液(80∶20,v/v)为流动相进行HPLC分离,在负离子模式和多级反应监测(MRM)方式下进行测定.用两个子离子的相对丰度定性,外标法定量.PFOS的测定在0.002～0.1 mg/L 范围内线性关系良好(r~2=0.998);泡沫<span style=\"color:red\">灭火</span>材料、洗涤剂以及织物整理剂中PFOS的加标回收率分别为93.4% ～103% ,93.2% ～102%和91.8% ～102% ,精密度(以相对标准偏差(RSD)计)分别为0.48% ～3.52% ,0.78% ～1.79%和0.47% ～3.47% ;方法的检出限均为2 mg/kg(0.000 2% )(信噪比(S/N)≥10),满足欧盟法规对泡沫<span style=\"color:red\">灭火</span>材料、洗涤剂以及织物整理剂中PFOS的限量检测要求.该方法准确度和灵敏度高,前处理简单,可用于泡沫<span style=\"color:red\">灭火</span>材料、洗涤剂以及织物整理剂中PFOS的检测.","authors":[{"authorName":"陈会明","id":"e67021cb-f95e-4f57-8c00-dce3b9327dd1","originalAuthorName":"陈会明"},{"authorName":"程艳","id":"6db35096-427b-4b7f-8858-c60932253b0c","originalAuthorName":"程艳"},{"authorName":"陈伟","id":"d3b59a9d-679b-4a84-ac76-ad53c5f61327","originalAuthorName":"陈伟"},{"authorName":"于文莲","id":"a3b3eab1-91ac-45a1-be76-382b4945c1fa","originalAuthorName":"于文莲"},{"authorName":"李晞","id":"e1fe715a-13f4-47e4-8528-260885d9becb","originalAuthorName":"李晞"},{"authorName":"王琤","id":"5739f8f3-fa7c-4f2b-b635-82b5efc59e2e","originalAuthorName":"王琤"}],"doi":"","fpage":"185","id":"17a4c9ef-47fb-420d-812c-2aa1fc0a2a32","issue":"2","journal":{"abbrevTitle":"SP","coverImgSrc":"journal/img/cover/SP.jpg","id":"58","issnPpub":"1000-8713","publisherId":"SP","title":"色谱 "},"keywords":[{"id":"009ccff8-58ab-46f0-9eba-61867029b287","keyword":"高效液相色谱-串联质谱法(HPLC-MS/MS)","originalKeyword":"高效液相色谱-串联质谱法(HPLC-MS/MS)"},{"id":"afc5154f-2137-4db1-9480-7351eeb8f95a","keyword":"固相萃取","originalKeyword":"固相萃取"},{"id":"c33870a1-ee52-4514-b137-376c781fe659","keyword":"全氟辛烷磺酰基化合物(PFOS)","originalKeyword":"全氟辛烷磺酰基化合物(PFOS)"},{"id":"1d094e87-6736-4d80-883c-0b160b75b899","keyword":"泡沫<span style=\"color:red\">灭火</span>材料","originalKeyword":"泡沫灭火材料"},{"id":"9fc15167-cb43-4620-a0ad-8487409b7927","keyword":"洗涤剂","originalKeyword":"洗涤剂"},{"id":"072ccf58-d1ff-4a52-b89d-bbc09d643791","keyword":"织物整理剂","originalKeyword":"织物整理剂"}],"language":"zh","publisherId":"sp201002015","title":"高效液相色谱-串联质谱法测定泡沫<span style=\"color:red\">灭火</span>材料及其他材料中的全氟辛烷磺酸及其盐","volume":"28","year":"2010"}],"totalpage":716,"totalrecord":7152}